Synthesis of nanostructured FePt systems

The paper compares some characteristics of nanoparticles of the FePt system obtained by the method of joint reduction of solutions of metal precursors using different reducing agents: an alkaline solution of hydrazine hydrate and sodium tetrahydroborate. The method of transmission electron microscop...

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Bibliographic Details
Published in:Journal of physics. Conference series 2021-01, Vol.1749 (1), p.12012
Main Authors: Zakharov, N S, Popova, A N, Zakharov, Yu A, Pugachev, V M
Format: Article
Language:English
Subjects:
Hydrazines
Intermetallic compounds
Iron compounds
Mass spectrometry
Morphology
Nanoparticles
Physics
Platinum compounds
Reducing agents
Reduction (metal working)
Thermal analysis
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Summary:The paper compares some characteristics of nanoparticles of the FePt system obtained by the method of joint reduction of solutions of metal precursors using different reducing agents: an alkaline solution of hydrazine hydrate and sodium tetrahydroborate. The method of transmission electron microscopy is used to analyze the shape and morphology of the obtained nanosized particles, according to the data obtained by the methods of X-ray diffraction, phase analysis is carried out and the main X-ray structural parameters are evaluated. Thermal analysis in combination with mass spectrometry is used to characterize the state and purity of the surface of nanoparticles. It is shown in the work that nanoscale FePt systems obtained using the reductants selected in the work have similar physicochemical characteristics.
ISSN:1742-6588
1742-6596
DOI:10.1088/1742-6596/1749/1/012012