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Effect of calcination time on biosynthesised SnO2 nanoparticles using bioactive compound from leaves extract of Chromolaena Odorata
Bioactive compounds contain in local medicinal plant found in Malaysia namely as Kapal Terbang or Chromolaena Odorata (C. Odorata) is used in performing biosynthesis of tin (iv) oxide nanoparticles (SnO2 NPs) which act as reducing and stabilizing agent. In this paper, we report for the first time th...
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creator | Buniyamin, Irmaizatussyehdany Akhir, Rabiatuladawiyah Md Asli, Noor Asnida Khusaimi, Zuraida Mahmood, Mohamad Rusop |
description | Bioactive compounds contain in local medicinal plant found in Malaysia namely as Kapal Terbang or Chromolaena Odorata (C. Odorata) is used in performing biosynthesis of tin (iv) oxide nanoparticles (SnO2 NPs) which act as reducing and stabilizing agent. In this paper, we report for the first time the biosynthesis of SnO2 NPs using non-toxic aqueous mixture of C. Odorata. The biosynthesis of SnO2 NPs was performed at room temperature and later underwent calcination process at 700°C within four different calcination time; 2 hours, 3 hours, 4 hours and 5-hours respectively. The synthesized SnO2 NPs were characterized using Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive X-ray analysis (EDX) and UV-visible diffuse reflectance spectroscopy (DRS). The results from FT-IR spectra confirmed the presence of functional groups of SnO2 NPs for sample calcined within two to four-hours. X-ray diffraction results shows that the average crystallite size are 8.8 nm with tetragonal structure. The morphology of the nanoparticles synthesized with uniform distribution of agglomerated spherical shape. The change in calcination time has definitely affect the energy band-gap as shown from the DRS absorption spectrum from 3.15 to 3.47 eV, respectively. This biosynthesized SnO2 NPs are proposed to have valuable application in catalysis and optoelectronic devices. |
doi_str_mv | 10.1063/5.0057784 |
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Odorata) is used in performing biosynthesis of tin (iv) oxide nanoparticles (SnO2 NPs) which act as reducing and stabilizing agent. In this paper, we report for the first time the biosynthesis of SnO2 NPs using non-toxic aqueous mixture of C. Odorata. The biosynthesis of SnO2 NPs was performed at room temperature and later underwent calcination process at 700°C within four different calcination time; 2 hours, 3 hours, 4 hours and 5-hours respectively. The synthesized SnO2 NPs were characterized using Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive X-ray analysis (EDX) and UV-visible diffuse reflectance spectroscopy (DRS). The results from FT-IR spectra confirmed the presence of functional groups of SnO2 NPs for sample calcined within two to four-hours. X-ray diffraction results shows that the average crystallite size are 8.8 nm with tetragonal structure. The morphology of the nanoparticles synthesized with uniform distribution of agglomerated spherical shape. The change in calcination time has definitely affect the energy band-gap as shown from the DRS absorption spectrum from 3.15 to 3.47 eV, respectively. This biosynthesized SnO2 NPs are proposed to have valuable application in catalysis and optoelectronic devices.</description><identifier>ISSN: 0094-243X</identifier><identifier>EISSN: 1551-7616</identifier><identifier>DOI: 10.1063/5.0057784</identifier><identifier>CODEN: APCPCS</identifier><language>eng</language><publisher>Melville: American Institute of Physics</publisher><subject>Absorption spectra ; Biocompatibility ; Biological activity ; Biosynthesis ; Crystallites ; Emission analysis ; Energy bands ; Energy dispersive X ray analysis ; Energy gap ; Field emission microscopy ; Fourier transforms ; Functional groups ; Herbal medicine ; Infrared spectroscopy ; Morphology ; Nanoparticles ; Optoelectronic devices ; Roasting ; Room temperature ; Spectrum analysis ; Stabilizers (agents) ; Tin dioxide ; X ray analysis ; X-ray diffraction</subject><ispartof>AIP conference proceedings, 2021, Vol.2368 (1)</ispartof><rights>Author(s)</rights><rights>2021 Author(s). Published by AIP Publishing.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>309,310,314,780,784,789,790,23930,23931,25140,27924,27925</link.rule.ids></links><search><contributor>Muhammad Khir, Farah Liyana binti</contributor><contributor>Supardan, Siti Nurbaya</contributor><contributor>Mohamed, Zakiah</contributor><contributor>Mahat, Annie Maria</contributor><creatorcontrib>Buniyamin, Irmaizatussyehdany</creatorcontrib><creatorcontrib>Akhir, Rabiatuladawiyah Md</creatorcontrib><creatorcontrib>Asli, Noor Asnida</creatorcontrib><creatorcontrib>Khusaimi, Zuraida</creatorcontrib><creatorcontrib>Mahmood, Mohamad Rusop</creatorcontrib><title>Effect of calcination time on biosynthesised SnO2 nanoparticles using bioactive compound from leaves extract of Chromolaena Odorata</title><title>AIP conference proceedings</title><description>Bioactive compounds contain in local medicinal plant found in Malaysia namely as Kapal Terbang or Chromolaena Odorata (C. Odorata) is used in performing biosynthesis of tin (iv) oxide nanoparticles (SnO2 NPs) which act as reducing and stabilizing agent. In this paper, we report for the first time the biosynthesis of SnO2 NPs using non-toxic aqueous mixture of C. Odorata. The biosynthesis of SnO2 NPs was performed at room temperature and later underwent calcination process at 700°C within four different calcination time; 2 hours, 3 hours, 4 hours and 5-hours respectively. The synthesized SnO2 NPs were characterized using Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive X-ray analysis (EDX) and UV-visible diffuse reflectance spectroscopy (DRS). The results from FT-IR spectra confirmed the presence of functional groups of SnO2 NPs for sample calcined within two to four-hours. X-ray diffraction results shows that the average crystallite size are 8.8 nm with tetragonal structure. The morphology of the nanoparticles synthesized with uniform distribution of agglomerated spherical shape. The change in calcination time has definitely affect the energy band-gap as shown from the DRS absorption spectrum from 3.15 to 3.47 eV, respectively. This biosynthesized SnO2 NPs are proposed to have valuable application in catalysis and optoelectronic devices.</description><subject>Absorption spectra</subject><subject>Biocompatibility</subject><subject>Biological activity</subject><subject>Biosynthesis</subject><subject>Crystallites</subject><subject>Emission analysis</subject><subject>Energy bands</subject><subject>Energy dispersive X ray analysis</subject><subject>Energy gap</subject><subject>Field emission microscopy</subject><subject>Fourier transforms</subject><subject>Functional groups</subject><subject>Herbal medicine</subject><subject>Infrared spectroscopy</subject><subject>Morphology</subject><subject>Nanoparticles</subject><subject>Optoelectronic devices</subject><subject>Roasting</subject><subject>Room temperature</subject><subject>Spectrum analysis</subject><subject>Stabilizers (agents)</subject><subject>Tin dioxide</subject><subject>X ray analysis</subject><subject>X-ray diffraction</subject><issn>0094-243X</issn><issn>1551-7616</issn><fulltext>true</fulltext><rsrctype>conference_proceeding</rsrctype><creationdate>2021</creationdate><recordtype>conference_proceeding</recordtype><recordid>eNp9kUtLAzEUhYMoWKsL_0HAnTA1mcwrSyn1AYUu7MLdcJuHTZlJxiQtdu0fN7UFd64OXL57D-dchG4pmVBSsYdyQkhZ101xhka0LGlWV7Q6RyNCeJHlBXu_RFchbAjJeaJG6HumtRIRO40FdMJYiMZZHE2vcNKVcWFv41oFE5TEb3aRYwvWDeCjEZ0KeBuM_ThwIKLZKSxcP7itlVh71-NOwS5B6it6OLpM12nuOlAW8EI6DxGu0YWGLqibk47R8mm2nL5k88Xz6_Rxng280VnBWSlXgq4AUg5d54pTqBQvcqVqJklNBYMqpVnVktZSEMZVw3MqtUzhS8rG6O54dvDuc6tCbDdu621ybPOyqFjOm4Il6v5IBWHibxnt4E0Pft_unG_L9tRvO0j9H0xJe3jI3wL7AQNCf9g</recordid><startdate>20210629</startdate><enddate>20210629</enddate><creator>Buniyamin, Irmaizatussyehdany</creator><creator>Akhir, Rabiatuladawiyah Md</creator><creator>Asli, Noor Asnida</creator><creator>Khusaimi, Zuraida</creator><creator>Mahmood, Mohamad Rusop</creator><general>American Institute of Physics</general><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope></search><sort><creationdate>20210629</creationdate><title>Effect of calcination time on biosynthesised SnO2 nanoparticles using bioactive compound from leaves extract of Chromolaena Odorata</title><author>Buniyamin, Irmaizatussyehdany ; Akhir, Rabiatuladawiyah Md ; Asli, Noor Asnida ; Khusaimi, Zuraida ; Mahmood, Mohamad Rusop</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p98f-4935dbc1baa243f72e91a6e942ee73d071c3a6ffeb7d17dc039e8921dfd009513</frbrgroupid><rsrctype>conference_proceedings</rsrctype><prefilter>conference_proceedings</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Absorption spectra</topic><topic>Biocompatibility</topic><topic>Biological activity</topic><topic>Biosynthesis</topic><topic>Crystallites</topic><topic>Emission analysis</topic><topic>Energy bands</topic><topic>Energy dispersive X ray analysis</topic><topic>Energy gap</topic><topic>Field emission microscopy</topic><topic>Fourier transforms</topic><topic>Functional groups</topic><topic>Herbal medicine</topic><topic>Infrared spectroscopy</topic><topic>Morphology</topic><topic>Nanoparticles</topic><topic>Optoelectronic devices</topic><topic>Roasting</topic><topic>Room temperature</topic><topic>Spectrum analysis</topic><topic>Stabilizers (agents)</topic><topic>Tin dioxide</topic><topic>X ray analysis</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Buniyamin, Irmaizatussyehdany</creatorcontrib><creatorcontrib>Akhir, Rabiatuladawiyah Md</creatorcontrib><creatorcontrib>Asli, Noor Asnida</creatorcontrib><creatorcontrib>Khusaimi, Zuraida</creatorcontrib><creatorcontrib>Mahmood, Mohamad Rusop</creatorcontrib><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Advanced Technologies Database with Aerospace</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Buniyamin, Irmaizatussyehdany</au><au>Akhir, Rabiatuladawiyah Md</au><au>Asli, Noor Asnida</au><au>Khusaimi, Zuraida</au><au>Mahmood, Mohamad Rusop</au><au>Muhammad Khir, Farah Liyana binti</au><au>Supardan, Siti Nurbaya</au><au>Mohamed, Zakiah</au><au>Mahat, Annie Maria</au><format>book</format><genre>proceeding</genre><ristype>CONF</ristype><atitle>Effect of calcination time on biosynthesised SnO2 nanoparticles using bioactive compound from leaves extract of Chromolaena Odorata</atitle><btitle>AIP conference proceedings</btitle><date>2021-06-29</date><risdate>2021</risdate><volume>2368</volume><issue>1</issue><issn>0094-243X</issn><eissn>1551-7616</eissn><coden>APCPCS</coden><abstract>Bioactive compounds contain in local medicinal plant found in Malaysia namely as Kapal Terbang or Chromolaena Odorata (C. Odorata) is used in performing biosynthesis of tin (iv) oxide nanoparticles (SnO2 NPs) which act as reducing and stabilizing agent. In this paper, we report for the first time the biosynthesis of SnO2 NPs using non-toxic aqueous mixture of C. Odorata. The biosynthesis of SnO2 NPs was performed at room temperature and later underwent calcination process at 700°C within four different calcination time; 2 hours, 3 hours, 4 hours and 5-hours respectively. The synthesized SnO2 NPs were characterized using Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive X-ray analysis (EDX) and UV-visible diffuse reflectance spectroscopy (DRS). The results from FT-IR spectra confirmed the presence of functional groups of SnO2 NPs for sample calcined within two to four-hours. X-ray diffraction results shows that the average crystallite size are 8.8 nm with tetragonal structure. The morphology of the nanoparticles synthesized with uniform distribution of agglomerated spherical shape. The change in calcination time has definitely affect the energy band-gap as shown from the DRS absorption spectrum from 3.15 to 3.47 eV, respectively. This biosynthesized SnO2 NPs are proposed to have valuable application in catalysis and optoelectronic devices.</abstract><cop>Melville</cop><pub>American Institute of Physics</pub><doi>10.1063/5.0057784</doi><tpages>6</tpages></addata></record> |
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subjects | Absorption spectra Biocompatibility Biological activity Biosynthesis Crystallites Emission analysis Energy bands Energy dispersive X ray analysis Energy gap Field emission microscopy Fourier transforms Functional groups Herbal medicine Infrared spectroscopy Morphology Nanoparticles Optoelectronic devices Roasting Room temperature Spectrum analysis Stabilizers (agents) Tin dioxide X ray analysis X-ray diffraction |
title | Effect of calcination time on biosynthesised SnO2 nanoparticles using bioactive compound from leaves extract of Chromolaena Odorata |
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