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Synthesis and Characterization of Magnetic Functionalized Ni and Cu Nano Catalysts and Their Application in Oxidation, Oxidative Coupling and Various Multi-Component Reactions
Two magnetic nano catalysts of nickel and copper, Fe 3 O 4 @SiO 2 @DOP-BenPyr-M(II), (M=Ni and Cu) have been synthesized. These catalysts were applied as recoverable, efficient and new heterogeneous catalysts for the high yielding and room temperature one-pot procedure of selective oxidation of sulf...
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| Published in: | Catalysis letters 2021-08, Vol.151 (8), p.2420-2435 |
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| Main Authors: | , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c392t-97c162270d762d908f4008e44623eda4db455f843a171ebffb1ce450b7478c9f3 |
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| cites | cdi_FETCH-LOGICAL-c392t-97c162270d762d908f4008e44623eda4db455f843a171ebffb1ce450b7478c9f3 |
| container_end_page | 2435 |
| container_issue | 8 |
| container_start_page | 2420 |
| container_title | Catalysis letters |
| container_volume | 151 |
| creator | Hajjami, Maryam Sheikhaei, Shiva Gholamian, Fatemeh Yousofvand, Zakieh |
| description | Two magnetic nano catalysts of nickel and copper, Fe
3
O
4
@SiO
2
@DOP-BenPyr-M(II), (M=Ni and Cu) have been synthesized. These catalysts were applied as recoverable, efficient and new heterogeneous catalysts for the high yielding and room temperature one-pot procedure of selective oxidation of sulfides to sulfoxides and oxidative coupling of thiols to disulfides. In addition, the catalytic activity of Fe
3
O
4
@SiO
2
@DOP-BenPyr-Ni(II) was investigated as heterogeneous nanocatalyst for synthesis of 2,3-dihydroquinazolin-4(1H)-ones, 5-substituted 1H-tetrazoles and polyhydroquinolines. The synthesized catalysts were characterized by FT-IR, TGA, XRD, VSM, EDX, ICP and SEM techniques. These catalysts were recovered by an external magnet and reused several times without significant loss of catalytic efficiency.
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| doi_str_mv | 10.1007/s10562-020-03495-3 |
| format | article |
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3
O
4
@SiO
2
@DOP-BenPyr-M(II), (M=Ni and Cu) have been synthesized. These catalysts were applied as recoverable, efficient and new heterogeneous catalysts for the high yielding and room temperature one-pot procedure of selective oxidation of sulfides to sulfoxides and oxidative coupling of thiols to disulfides. In addition, the catalytic activity of Fe
3
O
4
@SiO
2
@DOP-BenPyr-Ni(II) was investigated as heterogeneous nanocatalyst for synthesis of 2,3-dihydroquinazolin-4(1H)-ones, 5-substituted 1H-tetrazoles and polyhydroquinolines. The synthesized catalysts were characterized by FT-IR, TGA, XRD, VSM, EDX, ICP and SEM techniques. These catalysts were recovered by an external magnet and reused several times without significant loss of catalytic efficiency.
Graphic Abstract</description><identifier>ISSN: 1011-372X</identifier><identifier>EISSN: 1572-879X</identifier><identifier>DOI: 10.1007/s10562-020-03495-3</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Catalysis ; Catalysts ; Catalytic activity ; Chemical synthesis ; Chemistry ; Chemistry and Materials Science ; Copper ; Coupling ; Industrial Chemistry/Chemical Engineering ; Iron oxides ; Nickel ; Organometallic Chemistry ; Oxidation ; Oxidation-reduction reaction ; Physical Chemistry ; Room temperature ; Silicon dioxide ; Sulfides ; Tetrazoles ; Thiols</subject><ispartof>Catalysis letters, 2021-08, Vol.151 (8), p.2420-2435</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC part of Springer Nature 2021</rights><rights>COPYRIGHT 2021 Springer</rights><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC part of Springer Nature 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c392t-97c162270d762d908f4008e44623eda4db455f843a171ebffb1ce450b7478c9f3</citedby><cites>FETCH-LOGICAL-c392t-97c162270d762d908f4008e44623eda4db455f843a171ebffb1ce450b7478c9f3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27903,27904</link.rule.ids></links><search><creatorcontrib>Hajjami, Maryam</creatorcontrib><creatorcontrib>Sheikhaei, Shiva</creatorcontrib><creatorcontrib>Gholamian, Fatemeh</creatorcontrib><creatorcontrib>Yousofvand, Zakieh</creatorcontrib><title>Synthesis and Characterization of Magnetic Functionalized Ni and Cu Nano Catalysts and Their Application in Oxidation, Oxidative Coupling and Various Multi-Component Reactions</title><title>Catalysis letters</title><addtitle>Catal Lett</addtitle><description>Two magnetic nano catalysts of nickel and copper, Fe
3
O
4
@SiO
2
@DOP-BenPyr-M(II), (M=Ni and Cu) have been synthesized. These catalysts were applied as recoverable, efficient and new heterogeneous catalysts for the high yielding and room temperature one-pot procedure of selective oxidation of sulfides to sulfoxides and oxidative coupling of thiols to disulfides. In addition, the catalytic activity of Fe
3
O
4
@SiO
2
@DOP-BenPyr-Ni(II) was investigated as heterogeneous nanocatalyst for synthesis of 2,3-dihydroquinazolin-4(1H)-ones, 5-substituted 1H-tetrazoles and polyhydroquinolines. The synthesized catalysts were characterized by FT-IR, TGA, XRD, VSM, EDX, ICP and SEM techniques. These catalysts were recovered by an external magnet and reused several times without significant loss of catalytic efficiency.
Graphic Abstract</description><subject>Catalysis</subject><subject>Catalysts</subject><subject>Catalytic activity</subject><subject>Chemical synthesis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Copper</subject><subject>Coupling</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Iron oxides</subject><subject>Nickel</subject><subject>Organometallic Chemistry</subject><subject>Oxidation</subject><subject>Oxidation-reduction reaction</subject><subject>Physical Chemistry</subject><subject>Room temperature</subject><subject>Silicon dioxide</subject><subject>Sulfides</subject><subject>Tetrazoles</subject><subject>Thiols</subject><issn>1011-372X</issn><issn>1572-879X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp9kc1u3CAUha2qkZomfYGukLqqVKeAsTHLkdW0kfIjJWmVHWLwxUPkARdwlMlL9RVLxq2qbCoWXK7Od7hwiuI9wScEY_45Elw3tMQUl7hioi6rV8UhqTktWy7uXucaE1JWnN69Kd7GeI8xFpyIw-LXzc6lDUQbkXI96jYqKJ0g2CeVrHfIG3ShBgfJanQ6O_3cVKN9gh5d2gWZ0aVyHnUqqXEX02J0uwEb0GqaRqsXJ-vQ1aPt94dPf8sHQJ2fs8gNe-yHCtbPEV3MY7Jl57eTd-ASuga1vzoeFwdGjRHe_dmPiu-nX267b-X51dezbnVe6krQVAquSUMpxz1vaC9waxjGLTDW0Ap6xfo1q2vTskoRTmBtzJpoYDVec8ZbLUx1VHxYfKfgf84Qk7z3c8hPj5LWjBMuaiGy6mRRDWoEaZ3xKX9fXj1src6jG5v7q6bJQMsxycDHF0DWJHhMg5pjlGc31y-1dNHq4GMMYOQU7FaFnSRYPqcul9RlTl3uU5dVhqoFilnsBgj_5v4P9Rv2w7GU</recordid><startdate>20210801</startdate><enddate>20210801</enddate><creator>Hajjami, Maryam</creator><creator>Sheikhaei, Shiva</creator><creator>Gholamian, Fatemeh</creator><creator>Yousofvand, Zakieh</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope></search><sort><creationdate>20210801</creationdate><title>Synthesis and Characterization of Magnetic Functionalized Ni and Cu Nano Catalysts and Their Application in Oxidation, Oxidative Coupling and Various Multi-Component Reactions</title><author>Hajjami, Maryam ; 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3
O
4
@SiO
2
@DOP-BenPyr-M(II), (M=Ni and Cu) have been synthesized. These catalysts were applied as recoverable, efficient and new heterogeneous catalysts for the high yielding and room temperature one-pot procedure of selective oxidation of sulfides to sulfoxides and oxidative coupling of thiols to disulfides. In addition, the catalytic activity of Fe
3
O
4
@SiO
2
@DOP-BenPyr-Ni(II) was investigated as heterogeneous nanocatalyst for synthesis of 2,3-dihydroquinazolin-4(1H)-ones, 5-substituted 1H-tetrazoles and polyhydroquinolines. The synthesized catalysts were characterized by FT-IR, TGA, XRD, VSM, EDX, ICP and SEM techniques. These catalysts were recovered by an external magnet and reused several times without significant loss of catalytic efficiency.
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| fulltext | fulltext |
| identifier | ISSN: 1011-372X |
| ispartof | Catalysis letters, 2021-08, Vol.151 (8), p.2420-2435 |
| issn | 1011-372X 1572-879X |
| language | eng |
| recordid | cdi_proquest_journals_2547179599 |
| source | Springer Nature |
| subjects | Catalysis Catalysts Catalytic activity Chemical synthesis Chemistry Chemistry and Materials Science Copper Coupling Industrial Chemistry/Chemical Engineering Iron oxides Nickel Organometallic Chemistry Oxidation Oxidation-reduction reaction Physical Chemistry Room temperature Silicon dioxide Sulfides Tetrazoles Thiols |
| title | Synthesis and Characterization of Magnetic Functionalized Ni and Cu Nano Catalysts and Their Application in Oxidation, Oxidative Coupling and Various Multi-Component Reactions |
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