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Structure and dielectric properties of ZnMn2O4/NiFe2O4 nanocomposite

(1-x)ZnMn 2 O 4 /xNiFe 2 O 4 ( x  = 0, 0.05, 0.1, 0.15, 0.2) nanocomposite system was prepared using the sol–gel technique. Rietveld analysis revealed the presence of two phases ZnMn 2 O 4 and NiFe 2 O 4 for all composites, but with phase percentages different from nominated values of ( x ). The eff...

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Published in:Applied physics. A, Materials science & processing Materials science & processing, 2021-08, Vol.127 (8), Article 577
Main Authors: Heiba, Zein K., Mohamed, Mohamed Bakr, El-naggar, A. M., Altowairqi, Y.
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description (1-x)ZnMn 2 O 4 /xNiFe 2 O 4 ( x  = 0, 0.05, 0.1, 0.15, 0.2) nanocomposite system was prepared using the sol–gel technique. Rietveld analysis revealed the presence of two phases ZnMn 2 O 4 and NiFe 2 O 4 for all composites, but with phase percentages different from nominated values of ( x ). The effect of alloying parameter ( x ) on the lattice parameters and crystallite size of the obtained phases was also examined. The oxidation states of different ions were determined using X-ray photoelectron spectroscopy (XPS) technique. For the prepared nanocomposite samples, the dependence of dielectric constant, impedance and electric modulus on the frequency and temperature was performed using complex impedance technique. It was found that the obtained samples have ferroelectric characteristics. The degree of correlation for the different nanocomposite samples was explored using ac conductivity.
doi_str_mv 10.1007/s00339-021-04731-2
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subjects Alloying effects
Applied physics
Characterization and Evaluation of Materials
Condensed Matter Physics
Crystallites
Dielectric properties
Ferroelectricity
Impedance
Lattice parameters
Machines
Manufacturing
Materials science
Nanocomposites
Nanotechnology
Nickel ferrites
Optical and Electronic Materials
Oxidation
Photoelectrons
Physics
Physics and Astronomy
Processes
Sol-gel processes
Surfaces and Interfaces
Thin Films
X ray photoelectron spectroscopy
Zinc compounds
title Structure and dielectric properties of ZnMn2O4/NiFe2O4 nanocomposite
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