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Diethylene triamine penta methylene phosphonic acid encountered silver ions: a convenient method for preparation of flame retardant and antibacterial lyocell fabric
Ammonium salt of diethylene triamine penta methylene phosphonic acid (ADTPMPA), a novel flame retardant, was synthesized and grafted on the lyocell fabric to obtain a kind of flame retardant lyocell fabric (FR-lyocell). Then FR-lyocell was coated by Ag nanoparticles (Ag NPs) to fabricate flame retar...
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| Published in: | Cellulose (London) 2021-07, Vol.28 (11), p.7465-7481 |
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| Main Authors: | , , , , , |
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| container_title | Cellulose (London) |
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| creator | Xiao, Mengyuan Guo, Yingbin Zhang, Jiayue Liu, Yansong Ren, Yuanlin Liu, Xiaohui |
| description | Ammonium salt of diethylene triamine penta methylene phosphonic acid (ADTPMPA), a novel flame retardant, was synthesized and grafted on the lyocell fabric to obtain a kind of flame retardant lyocell fabric (FR-lyocell). Then FR-lyocell was coated by Ag nanoparticles (Ag NPs) to fabricate flame retardant and antibacterial lyocell fabric (FR-Ag-lyocell). The elemental composition, surface morphology, combustion behavior and antibacterial activity of the lyocell fabric before and after modification were investigated. The flame retardant and antibacterial mechanism of FR-Ag-lyocell fabric was also analyzed. The limiting oxygen index (LOI) values of FR-Ag-lyocell fabric before and after 20 laundering cycles (LCs) reached 44.8% and 31.3%, respectively. The treated lyocell fabric possessed lower peak of heat release rate (pHRR) and total heat release (THR) values compared with control lyocell fabric. The FR-Ag-lyocell fabric exhibited excellent antimicrobial ability against Staphylococcus aureus (
S. aureus
) and Escherichia coli (
E. coli
), even after 10 LCs. These results indicated that FR-Ag-lyocell fabric had durable flame retardant and antibacterial properties.
Graphic abstract |
| doi_str_mv | 10.1007/s10570-021-04000-8 |
| format | article |
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S. aureus
) and Escherichia coli (
E. coli
), even after 10 LCs. These results indicated that FR-Ag-lyocell fabric had durable flame retardant and antibacterial properties.
Graphic abstract</description><identifier>ISSN: 0969-0239</identifier><identifier>EISSN: 1572-882X</identifier><identifier>DOI: 10.1007/s10570-021-04000-8</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Bioorganic Chemistry ; Ceramics ; Chemistry ; Chemistry and Materials Science ; Composites ; Diethylene triamine ; E coli ; Enthalpy ; Flame retardants ; Glass ; Heat release rate ; Methylene ; Morphology ; Nanoparticles ; Natural Materials ; Organic Chemistry ; Original Research ; Phosphonic acids ; Physical Chemistry ; Polymer Sciences ; Silver ; Sustainable Development</subject><ispartof>Cellulose (London), 2021-07, Vol.28 (11), p.7465-7481</ispartof><rights>The Author(s), under exclusive licence to Springer Nature B.V. 2021</rights><rights>The Author(s), under exclusive licence to Springer Nature B.V. 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-53abc2083d35c462088577c3c10ec63b4ebc1c60f79572af438296d5232e6d943</citedby><cites>FETCH-LOGICAL-c319t-53abc2083d35c462088577c3c10ec63b4ebc1c60f79572af438296d5232e6d943</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><creatorcontrib>Xiao, Mengyuan</creatorcontrib><creatorcontrib>Guo, Yingbin</creatorcontrib><creatorcontrib>Zhang, Jiayue</creatorcontrib><creatorcontrib>Liu, Yansong</creatorcontrib><creatorcontrib>Ren, Yuanlin</creatorcontrib><creatorcontrib>Liu, Xiaohui</creatorcontrib><title>Diethylene triamine penta methylene phosphonic acid encountered silver ions: a convenient method for preparation of flame retardant and antibacterial lyocell fabric</title><title>Cellulose (London)</title><addtitle>Cellulose</addtitle><description>Ammonium salt of diethylene triamine penta methylene phosphonic acid (ADTPMPA), a novel flame retardant, was synthesized and grafted on the lyocell fabric to obtain a kind of flame retardant lyocell fabric (FR-lyocell). Then FR-lyocell was coated by Ag nanoparticles (Ag NPs) to fabricate flame retardant and antibacterial lyocell fabric (FR-Ag-lyocell). The elemental composition, surface morphology, combustion behavior and antibacterial activity of the lyocell fabric before and after modification were investigated. The flame retardant and antibacterial mechanism of FR-Ag-lyocell fabric was also analyzed. The limiting oxygen index (LOI) values of FR-Ag-lyocell fabric before and after 20 laundering cycles (LCs) reached 44.8% and 31.3%, respectively. The treated lyocell fabric possessed lower peak of heat release rate (pHRR) and total heat release (THR) values compared with control lyocell fabric. The FR-Ag-lyocell fabric exhibited excellent antimicrobial ability against Staphylococcus aureus (
S. aureus
) and Escherichia coli (
E. coli
), even after 10 LCs. These results indicated that FR-Ag-lyocell fabric had durable flame retardant and antibacterial properties.
Graphic abstract</description><subject>Bioorganic Chemistry</subject><subject>Ceramics</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Composites</subject><subject>Diethylene triamine</subject><subject>E coli</subject><subject>Enthalpy</subject><subject>Flame retardants</subject><subject>Glass</subject><subject>Heat release rate</subject><subject>Methylene</subject><subject>Morphology</subject><subject>Nanoparticles</subject><subject>Natural Materials</subject><subject>Organic Chemistry</subject><subject>Original Research</subject><subject>Phosphonic acids</subject><subject>Physical Chemistry</subject><subject>Polymer Sciences</subject><subject>Silver</subject><subject>Sustainable Development</subject><issn>0969-0239</issn><issn>1572-882X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp9kctKBDEQRYMoOD5-wFXAdWse_Yo78Q2CGwV3oTpd7WToSdokI8z_-KHGGdGdi6IK6txbUJeQE87OOGPNeeSsaljBBC9YyRgr2h0y41UjirYVr7tkxlSt8lqqfXIQ4yIjqhF8Rj6vLab5ekSHNAULS5uHCV0CuvxdTHMfczlrKBjbU3TGr1zCgD2NdvzAQK138YICNd59oLPZYKP3PR18oFPACQKkTFE_0GGEJdKACUIPmQTX50q2A5NNLYx0XHuD40gH6II1R2RvgDHi8U8_JC-3N89X98Xj093D1eVjYSRXqagkdEawVvayMmWdp7ZqGiMNZ2hq2ZXYGW5qNjQqfwaGUrZC1X0lpMC6V6U8JKdb3yn49xXGpBd-FVw-qUVV8ZaVXMlMiS1lgo8x4KCnYJcQ1poz_Z2G3qahcxp6k4Zus0huRTHD7g3Dn_U_qi8NcZC6</recordid><startdate>20210701</startdate><enddate>20210701</enddate><creator>Xiao, Mengyuan</creator><creator>Guo, Yingbin</creator><creator>Zhang, Jiayue</creator><creator>Liu, Yansong</creator><creator>Ren, Yuanlin</creator><creator>Liu, Xiaohui</creator><general>Springer Netherlands</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope></search><sort><creationdate>20210701</creationdate><title>Diethylene triamine penta methylene phosphonic acid encountered silver ions: a convenient method for preparation of flame retardant and antibacterial lyocell fabric</title><author>Xiao, Mengyuan ; 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Then FR-lyocell was coated by Ag nanoparticles (Ag NPs) to fabricate flame retardant and antibacterial lyocell fabric (FR-Ag-lyocell). The elemental composition, surface morphology, combustion behavior and antibacterial activity of the lyocell fabric before and after modification were investigated. The flame retardant and antibacterial mechanism of FR-Ag-lyocell fabric was also analyzed. The limiting oxygen index (LOI) values of FR-Ag-lyocell fabric before and after 20 laundering cycles (LCs) reached 44.8% and 31.3%, respectively. The treated lyocell fabric possessed lower peak of heat release rate (pHRR) and total heat release (THR) values compared with control lyocell fabric. The FR-Ag-lyocell fabric exhibited excellent antimicrobial ability against Staphylococcus aureus (
S. aureus
) and Escherichia coli (
E. coli
), even after 10 LCs. These results indicated that FR-Ag-lyocell fabric had durable flame retardant and antibacterial properties.
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| subjects | Bioorganic Chemistry Ceramics Chemistry Chemistry and Materials Science Composites Diethylene triamine E coli Enthalpy Flame retardants Glass Heat release rate Methylene Morphology Nanoparticles Natural Materials Organic Chemistry Original Research Phosphonic acids Physical Chemistry Polymer Sciences Silver Sustainable Development |
| title | Diethylene triamine penta methylene phosphonic acid encountered silver ions: a convenient method for preparation of flame retardant and antibacterial lyocell fabric |
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