Facile Sol-Gel Synthesis of Calcium Phosphates: Influence of Ca/P Ratio and Calcination Temperature

Calcium phosphates (CP) have been synthesized by sol-gel method in various calcium to phosphorus molar ratio and calcination temperatures. The objective of this study was to understand the influence of molar ratio Ca/P and calcination temperature on crystalline phase of CP. Sol-gel synthesis of calc...

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Published in:IOP conference series. Earth and environmental science 2019-01, Vol.217 (1), p.12001
Main Authors: Permana, A J, Utami, A T, Handajani, U S, Setyawati, H
Format: Article
Language:English
Subjects:
calcination temperature
Calcium nitrate
Calcium phosphates
Calorimetry
Chemical bonds
Crystal structure
Crystallinity
Differential scanning calorimetry
Fourier analysis
Fourier transforms
Infrared spectrophotometers
molar ratio
Phosphoric acid
Phosphorus
Roasting
Room temperature
sol-gel
Sol-gel processes
Synthesis
Temperature
Thermal analysis
Thermogravimetric analysis
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cited_by cdi_FETCH-LOGICAL-c444t-3819b86150bd06730ba2f900c356ce93c3098228bc4afb51093d8e6950a1247f3
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creator Permana, A J
Utami, A T
Handajani, U S
Setyawati, H
description Calcium phosphates (CP) have been synthesized by sol-gel method in various calcium to phosphorus molar ratio and calcination temperatures. The objective of this study was to understand the influence of molar ratio Ca/P and calcination temperature on crystalline phase of CP. Sol-gel synthesis of calcium phosphates have been performed at room temperature by mixing calcium nitrate and phosphoric acid at Ca/P molar ratio 1.0, 1.3 and 1.5. Gel of synthesis products were dried at 110°C to produce powder then measured by thermal analysis of Differential Scanning Calorimetry-Thermogravimetric Analysis (DSC-TGA). Powders of CP were calcined at 110, 400 and 600°C based on thermal analysis result. Crystalline phase and chemical bonds of calcined CP powders were characterized by X-Ray Diffractometer (XRD) and Fourier Transform Infrared Spectrophotometer (FTIR).
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1755-1315
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subjects calcination temperature
Calcium nitrate
Calcium phosphates
Calorimetry
Chemical bonds
Crystal structure
Crystallinity
Differential scanning calorimetry
Fourier analysis
Fourier transforms
Infrared spectrophotometers
molar ratio
Phosphoric acid
Phosphorus
Roasting
Room temperature
sol-gel
Sol-gel processes
Synthesis
Temperature
Thermal analysis
Thermogravimetric analysis
title Facile Sol-Gel Synthesis of Calcium Phosphates: Influence of Ca/P Ratio and Calcination Temperature
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