Detecting Carbon Nanotube Orientation with Topological Data Analysis of Scanning Electron Micrographs

As the aerospace industry becomes increasingly demanding for stronger lightweight materials, the ultra-strong carbon nanotube (CNT) composites with highly aligned CNT network structures could be the answer. In this work, a novel methodology applying topological data analysis (TDA) to the scanning el...

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Bibliographic Details
Published in:arXiv.org 2021-08
Main Authors: Dong, Liyu, Hang, Haibin, Park, Jin Gyu, Washington Mio, Liang, Richard
Format: Article
Language:English
Subjects:
Aerospace industry
Alignment
Bar codes
Carbon nanotubes
Data analysis
Electron micrographs
Nanofibers
Orientation
Raman spectroscopy
Scanning electron microscopy
Strain
Topology
X-ray scattering
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Summary:As the aerospace industry becomes increasingly demanding for stronger lightweight materials, the ultra-strong carbon nanotube (CNT) composites with highly aligned CNT network structures could be the answer. In this work, a novel methodology applying topological data analysis (TDA) to the scanning electron microscope (SEM) images was developed to detect CNT orientation. The CNT bundle extensions in certain directions were summarized algebraically and expressed as visible barcodes. The barcodes were then calculated and converted into the total spread function \(V(X,\theta)\), from which the alignment fraction and the preferred direction could be determined. For validation purposes, the random CNT sheets were mechanically stretched at various strain ratios ranging from \(0-40\%\), and quantitative TDA analysis was conducted based on the SEM images taken at random positions. The results showed high consistency (\(R^2=0.975\)) compared to the Herman's orientation factors derived from the polarized Raman spectroscopy and wide-angle X-ray scattering analysis. Additionally, the TDA method presented great robustness with varying SEM acceleration voltages and magnifications, which might alter the scope in alignment detection. With potential applications in nanofiber systems, this study offers a rapid and simple way to quantify CNT alignment, which plays a crucial role in transferring the CNT properties into engineering products.
ISSN:2331-8422