One-Pot Conversion and Separation of Methyl Eugenol by Vacuum Fractionation

The conversion and direct separation of methyl eugenol (ME) in one-pot fractionation vacuum is presented. Mixtures containing eugenol (Eu), sodium hydroxide (NaOH) and dimethyl sulphate (DMS) as methylation agent were reacted in pot of fractionation vacuum. After finished methylation, the mixture di...

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Bibliographic Details
Published in:IOP conference series. Materials Science and Engineering 2019-03, Vol.494 (1), p.12056
Main Authors: Agustian, E., Tursiloadi, S., Sulaswatty, A., Rinaldi, N., Sudiyarmanto
Format: Article
Language:English
Subjects:
clove oil
Conversion
Dimethyl sulfate
eugenol
Fractionation
Methyl eugenol
Methylation
one pot
Process parameters
Separation
Sodium hydroxide
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Summary:The conversion and direct separation of methyl eugenol (ME) in one-pot fractionation vacuum is presented. Mixtures containing eugenol (Eu), sodium hydroxide (NaOH) and dimethyl sulphate (DMS) as methylation agent were reacted in pot of fractionation vacuum. After finished methylation, the mixture direct separation in same pot of fractionation vacuum. The parameter process is observed ratio Eu to DMS, time reaction and temperatures. The best results is obtained 1:3 of the ratio Eu to DMS, 6 hour of time reaction and 100oC of temperatures. Concentration methyl eugenol after separation gave 98.06%. The one-pot fractionation is good conversion directly separation to obtain ME from Eu of clove oil with high concentration and efficient process.
ISSN:1757-8981
1757-899X
1757-899X
DOI:10.1088/1757-899X/494/1/012056