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Ceramics Based on CaSO4⋅2H2O Powder Synthesized from Ca(NO3)2 and (NH4)2SO4
— Ceramics consisting of anhydrous calcium sulfate, CaSO 4 , after firing in the range 800–1000°C have been prepared from calcium sulfate dihydrate (CaSO 4 ⋅2H 2 O) powder synthesized using aqueous 1 M calcium nitrate (Ca(NO 3 ) 2 ) and ammonium sulfate ((NH 4 ) 2 SO 4 ) solutions. In the preparatio...
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| Published in: | Inorganic materials 2021-08, Vol.57 (8), p.867-873 |
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| Main Authors: | , , , , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c2312-55d1989bfaafd913f33863d564187defbdb9609575cd990b752bfcfc39948a7e3 |
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| cites | cdi_FETCH-LOGICAL-c2312-55d1989bfaafd913f33863d564187defbdb9609575cd990b752bfcfc39948a7e3 |
| container_end_page | 873 |
| container_issue | 8 |
| container_start_page | 867 |
| container_title | Inorganic materials |
| container_volume | 57 |
| creator | Safronova, T. V. Belokozenko, M. A. Yahyoev, Sh. O. Shatalova, T. B. Kazakova, G. K. Peranidze, K. Kh Toshev, O. U. Khasanova, S. S. |
| description | —
Ceramics consisting of anhydrous calcium sulfate, CaSO
4
, after firing in the range 800–1000°C have been prepared from calcium sulfate dihydrate (CaSO
4
⋅2H
2
O) powder synthesized using aqueous 1 M calcium nitrate (Ca(NO
3
)
2
) and ammonium sulfate ((NH
4
)
2
SO
4
) solutions. In the preparation of the powder, the precipitate was washed four times with distilled water to remove ammonium nitrate, NH
4
NO
3
, a reaction by-product and, after drying, the powder was disaggregated in acetone. The synthesized CaSO
4
⋅2H
2
O powder particles had an elongated prismatic shape both before and after disaggregation. After firing at 800, 900, and 1000°C, the microstructure of the ceramics based on the synthesized CaSO
4
⋅2H
2
O powder free of reaction by-products contained sintered elongated polycrystalline structures, confirming that the ceramics inherited the microstructure of the starting powder. Ceramics consisting of anhydrous calcium sulfate, CaSO
4
, can be recommended for the fabrication of implants for bone tissue defect repair by regenerative medicine methods because they are biocompatible and bioresorbable. |
| doi_str_mv | 10.1134/S0020168521080112 |
| format | article |
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Ceramics consisting of anhydrous calcium sulfate, CaSO
4
, after firing in the range 800–1000°C have been prepared from calcium sulfate dihydrate (CaSO
4
⋅2H
2
O) powder synthesized using aqueous 1 M calcium nitrate (Ca(NO
3
)
2
) and ammonium sulfate ((NH
4
)
2
SO
4
) solutions. In the preparation of the powder, the precipitate was washed four times with distilled water to remove ammonium nitrate, NH
4
NO
3
, a reaction by-product and, after drying, the powder was disaggregated in acetone. The synthesized CaSO
4
⋅2H
2
O powder particles had an elongated prismatic shape both before and after disaggregation. After firing at 800, 900, and 1000°C, the microstructure of the ceramics based on the synthesized CaSO
4
⋅2H
2
O powder free of reaction by-products contained sintered elongated polycrystalline structures, confirming that the ceramics inherited the microstructure of the starting powder. Ceramics consisting of anhydrous calcium sulfate, CaSO
4
, can be recommended for the fabrication of implants for bone tissue defect repair by regenerative medicine methods because they are biocompatible and bioresorbable.</description><identifier>ISSN: 0020-1685</identifier><identifier>EISSN: 1608-3172</identifier><identifier>DOI: 10.1134/S0020168521080112</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Ammonium nitrate ; Ammonium sulfate ; Biocompatibility ; Biomedical materials ; Byproducts ; Calcium nitrate ; Calcium sulfate ; Calcium sulfate dihydrate ; Ceramic powders ; Ceramics ; Chemistry ; Chemistry and Materials Science ; Distilled water ; Elongated structure ; Industrial Chemistry/Chemical Engineering ; Inorganic Chemistry ; Materials Science ; Microstructure ; Nitrates ; Sintering (powder metallurgy) ; Tissue engineering</subject><ispartof>Inorganic materials, 2021-08, Vol.57 (8), p.867-873</ispartof><rights>Pleiades Publishing, Ltd. 2021. ISSN 0020-1685, Inorganic Materials, 2021, Vol. 57, No. 8, pp. 867–873. © Pleiades Publishing, Ltd., 2021. Russian Text © The Author(s), 2021, published in Neorganicheskie Materialy, 2021, Vol. 57, No. 8, pp. 910–917.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c2312-55d1989bfaafd913f33863d564187defbdb9609575cd990b752bfcfc39948a7e3</citedby><cites>FETCH-LOGICAL-c2312-55d1989bfaafd913f33863d564187defbdb9609575cd990b752bfcfc39948a7e3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,777,781,27905,27906</link.rule.ids></links><search><creatorcontrib>Safronova, T. V.</creatorcontrib><creatorcontrib>Belokozenko, M. A.</creatorcontrib><creatorcontrib>Yahyoev, Sh. O.</creatorcontrib><creatorcontrib>Shatalova, T. B.</creatorcontrib><creatorcontrib>Kazakova, G. K.</creatorcontrib><creatorcontrib>Peranidze, K. Kh</creatorcontrib><creatorcontrib>Toshev, O. U.</creatorcontrib><creatorcontrib>Khasanova, S. S.</creatorcontrib><title>Ceramics Based on CaSO4⋅2H2O Powder Synthesized from Ca(NO3)2 and (NH4)2SO4</title><title>Inorganic materials</title><addtitle>Inorg Mater</addtitle><description>—
Ceramics consisting of anhydrous calcium sulfate, CaSO
4
, after firing in the range 800–1000°C have been prepared from calcium sulfate dihydrate (CaSO
4
⋅2H
2
O) powder synthesized using aqueous 1 M calcium nitrate (Ca(NO
3
)
2
) and ammonium sulfate ((NH
4
)
2
SO
4
) solutions. In the preparation of the powder, the precipitate was washed four times with distilled water to remove ammonium nitrate, NH
4
NO
3
, a reaction by-product and, after drying, the powder was disaggregated in acetone. The synthesized CaSO
4
⋅2H
2
O powder particles had an elongated prismatic shape both before and after disaggregation. After firing at 800, 900, and 1000°C, the microstructure of the ceramics based on the synthesized CaSO
4
⋅2H
2
O powder free of reaction by-products contained sintered elongated polycrystalline structures, confirming that the ceramics inherited the microstructure of the starting powder. Ceramics consisting of anhydrous calcium sulfate, CaSO
4
, can be recommended for the fabrication of implants for bone tissue defect repair by regenerative medicine methods because they are biocompatible and bioresorbable.</description><subject>Ammonium nitrate</subject><subject>Ammonium sulfate</subject><subject>Biocompatibility</subject><subject>Biomedical materials</subject><subject>Byproducts</subject><subject>Calcium nitrate</subject><subject>Calcium sulfate</subject><subject>Calcium sulfate dihydrate</subject><subject>Ceramic powders</subject><subject>Ceramics</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Distilled water</subject><subject>Elongated structure</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Inorganic Chemistry</subject><subject>Materials Science</subject><subject>Microstructure</subject><subject>Nitrates</subject><subject>Sintering (powder metallurgy)</subject><subject>Tissue engineering</subject><issn>0020-1685</issn><issn>1608-3172</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp1kLFOwzAURS0EEqXwAWyWWNoh4PccJ_YIEVCkQpAKc-TENrSiSbFbobIz8Zd8Ca6KxICY3nDPuU-6hBwDOwXg6dmEMWSQSYHAJAPAHdKDjMmEQ467pLeJk02-Tw5CmDHGUiFVj9wW1uv5tAn0QgdraNfSQk_K9OvzA0dY0vvuzVhPJ-t2-WzD9D0iznfzCA3uSj5EqltDB3ejdIjROiR7Tr8Ee_Rz--Tx6vKhGCXj8vqmOB8nDXLARAgDSqraae2MAu44lxk3IktB5sa62tQqY0rkojFKsToXWLvGNVypVOrc8j452fYufPe6smFZzbqVb-PLCkUGiisJeaRgSzW-C8FbVy38dK79ugJWbVar_qwWHdw6IbLtk_W_zf9L32KAamM</recordid><startdate>20210801</startdate><enddate>20210801</enddate><creator>Safronova, T. V.</creator><creator>Belokozenko, M. A.</creator><creator>Yahyoev, Sh. O.</creator><creator>Shatalova, T. B.</creator><creator>Kazakova, G. K.</creator><creator>Peranidze, K. Kh</creator><creator>Toshev, O. U.</creator><creator>Khasanova, S. S.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20210801</creationdate><title>Ceramics Based on CaSO4⋅2H2O Powder Synthesized from Ca(NO3)2 and (NH4)2SO4</title><author>Safronova, T. V. ; Belokozenko, M. A. ; Yahyoev, Sh. O. ; Shatalova, T. B. ; Kazakova, G. K. ; Peranidze, K. Kh ; Toshev, O. U. ; Khasanova, S. S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2312-55d1989bfaafd913f33863d564187defbdb9609575cd990b752bfcfc39948a7e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Ammonium nitrate</topic><topic>Ammonium sulfate</topic><topic>Biocompatibility</topic><topic>Biomedical materials</topic><topic>Byproducts</topic><topic>Calcium nitrate</topic><topic>Calcium sulfate</topic><topic>Calcium sulfate dihydrate</topic><topic>Ceramic powders</topic><topic>Ceramics</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Distilled water</topic><topic>Elongated structure</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>Inorganic Chemistry</topic><topic>Materials Science</topic><topic>Microstructure</topic><topic>Nitrates</topic><topic>Sintering (powder metallurgy)</topic><topic>Tissue engineering</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Safronova, T. V.</creatorcontrib><creatorcontrib>Belokozenko, M. A.</creatorcontrib><creatorcontrib>Yahyoev, Sh. O.</creatorcontrib><creatorcontrib>Shatalova, T. B.</creatorcontrib><creatorcontrib>Kazakova, G. K.</creatorcontrib><creatorcontrib>Peranidze, K. Kh</creatorcontrib><creatorcontrib>Toshev, O. U.</creatorcontrib><creatorcontrib>Khasanova, S. S.</creatorcontrib><collection>CrossRef</collection><jtitle>Inorganic materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Safronova, T. V.</au><au>Belokozenko, M. A.</au><au>Yahyoev, Sh. O.</au><au>Shatalova, T. B.</au><au>Kazakova, G. K.</au><au>Peranidze, K. Kh</au><au>Toshev, O. U.</au><au>Khasanova, S. S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Ceramics Based on CaSO4⋅2H2O Powder Synthesized from Ca(NO3)2 and (NH4)2SO4</atitle><jtitle>Inorganic materials</jtitle><stitle>Inorg Mater</stitle><date>2021-08-01</date><risdate>2021</risdate><volume>57</volume><issue>8</issue><spage>867</spage><epage>873</epage><pages>867-873</pages><issn>0020-1685</issn><eissn>1608-3172</eissn><abstract>—
Ceramics consisting of anhydrous calcium sulfate, CaSO
4
, after firing in the range 800–1000°C have been prepared from calcium sulfate dihydrate (CaSO
4
⋅2H
2
O) powder synthesized using aqueous 1 M calcium nitrate (Ca(NO
3
)
2
) and ammonium sulfate ((NH
4
)
2
SO
4
) solutions. In the preparation of the powder, the precipitate was washed four times with distilled water to remove ammonium nitrate, NH
4
NO
3
, a reaction by-product and, after drying, the powder was disaggregated in acetone. The synthesized CaSO
4
⋅2H
2
O powder particles had an elongated prismatic shape both before and after disaggregation. After firing at 800, 900, and 1000°C, the microstructure of the ceramics based on the synthesized CaSO
4
⋅2H
2
O powder free of reaction by-products contained sintered elongated polycrystalline structures, confirming that the ceramics inherited the microstructure of the starting powder. Ceramics consisting of anhydrous calcium sulfate, CaSO
4
, can be recommended for the fabrication of implants for bone tissue defect repair by regenerative medicine methods because they are biocompatible and bioresorbable.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S0020168521080112</doi><tpages>7</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0020-1685 |
| ispartof | Inorganic materials, 2021-08, Vol.57 (8), p.867-873 |
| issn | 0020-1685 1608-3172 |
| language | eng |
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| source | Springer Link |
| subjects | Ammonium nitrate Ammonium sulfate Biocompatibility Biomedical materials Byproducts Calcium nitrate Calcium sulfate Calcium sulfate dihydrate Ceramic powders Ceramics Chemistry Chemistry and Materials Science Distilled water Elongated structure Industrial Chemistry/Chemical Engineering Inorganic Chemistry Materials Science Microstructure Nitrates Sintering (powder metallurgy) Tissue engineering |
| title | Ceramics Based on CaSO4⋅2H2O Powder Synthesized from Ca(NO3)2 and (NH4)2SO4 |
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