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Synthesis, morpho-structural properties, and catalytic performances of Pt-APA@Fe3O4/GO nanocomposite based on magnetical graphene in C–C coupling reactions and photoinactivation of E. coli
Herein, a novel Pt-APA composite (APA = pyridinium bromide salt) based on magnetic graphene oxide was synthesized and used as an effective catalyst. In this way, Fe 3 O 4 nanoparticles are grown on graphene oxide (GO) nanosheets by a simple and practical method which creates a unique nanostructure (...
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| Published in: | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology 2021-08, Vol.23 (8), Article 192 |
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| container_title | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology |
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| creator | Moniriyan, Faezeh Sabounchei, Seyyed Javad Yousefi, Abed Akhavan, Omid |
| description | Herein, a novel Pt-APA composite (APA = pyridinium bromide salt) based on magnetic graphene oxide was synthesized and used as an effective catalyst. In this way, Fe
3
O
4
nanoparticles are grown on graphene oxide (GO) nanosheets by a simple and practical method which creates a unique nanostructure (Fe
3
O
4
/GO) through dispersing uniformly among graphene nanosheets. The resulted Pt-APA composite was obtained via adding PtCl
2
to an ethanol solution of Fe
3
O
4
/GO and α-keto stabilized pyridinium ylide in related conditions. The synthesized nanocomposite structure was identified using field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), energy dispersive spectral analysis (EDS), inductively coupled plasma spectrometry (ICP-MS), powder X-ray diffraction (XRD), Fourier transform infrared (FT-IR), vibrating-sample magnetometer (VSM), and UV − Vis spectroscopy. To investigate the catalytic properties of the synthesized Pt-APA@Fe
3
O
4
/GO nanocomposite, it was firstly used as an efficient nano-magnetic catalyst in C–C cross-coupling reaction, Suzuki–Miyaura, with excellent results. Second, the Pt-APA@Fe
3
O
4
/GO nanocomposite has been used as a magnetic photocatalyst to inactivate
E. coli
bacteria on a nutrient agar plate under visible light irradiation, which showed excellent results. By examining the results, the antibacterial durability of nanocomposites Pt-APA@GO/Fe
3
O
4
related to Fe
3
O
4
/GO shows a more significant inhibition against bacteria cell in both dark and visible light.
Graphical abstract
In this study a novel pyridinium complex-functionalized magnetic graphene oxide composite was synthesized and used in photoinactivation of Escherichia coli bacteria under visible light irradiation. It was also used as a promising catalyst in Suzuki–Miyaura C–C coupling reaction. The nanocomposite was characterized by field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), energy dispersive spectral analysis (EDS), powder X-ray diffraction (XRD), Fourier transform infrared (FT-IR), Inductively coupled plasma mass spectrometry (ICP-MS), UV − vis spectroscopy and vibrating-sample magnetometer (VSM). |
| doi_str_mv | 10.1007/s11051-021-05278-2 |
| format | article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2563225830</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2563225830</sourcerecordid><originalsourceid>FETCH-LOGICAL-c319t-e73674ef52da48cefb947c57785116dbb09e6d471f9f1c6c05c5b8d5fb2e5fcc3</originalsourceid><addsrcrecordid>eNp9Uctq3DAUNSWB5vUDXQm6rRJJtix7l2FI0kJgAkkgOyHLVzMKtuRIcmB2-Yf8Tz8mX1JNptBdF-KKc89D6BTFN0rOKSHiIlJKOMWE5cOZaDD7UhxRLhhu2vrpIN_LpsFE1NXX4jjGZ0JozVp2VPy-37q0gWjjDzT6MG08jinMOs1BDWgKfoKQLOStcj3SKqlhm6xGGTY-jMppiMgbdJfw4m5xeQ3lqrq4WSGnnNd-nHy0CVCnIvTIOzSqtYOsz97roKYNOEDWoeXH2_sSaT9Pg3VrFEDpZL2Ln6H5Tclbt4Ne1Q7e5V2dZ_pgT4tDo4YIZ3_nSfF4ffWw_IlvVze_lotbrEvaJgyirEUFhrNeVY0G07WV0FyIhlNa911HWqj7SlDTGqprTbjmXdNz0zHgRuvypPi-980_8jJDTPLZz8HlSMl4XTLGm5JkFtuzdPAxBjByCnZUYSspkbue5L4nmXuSnz1JlkXlXhQz2a0h_LP-j-oPLqya8Q</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2563225830</pqid></control><display><type>article</type><title>Synthesis, morpho-structural properties, and catalytic performances of Pt-APA@Fe3O4/GO nanocomposite based on magnetical graphene in C–C coupling reactions and photoinactivation of E. coli</title><source>Springer Nature</source><creator>Moniriyan, Faezeh ; Sabounchei, Seyyed Javad ; Yousefi, Abed ; Akhavan, Omid</creator><creatorcontrib>Moniriyan, Faezeh ; Sabounchei, Seyyed Javad ; Yousefi, Abed ; Akhavan, Omid</creatorcontrib><description>Herein, a novel Pt-APA composite (APA = pyridinium bromide salt) based on magnetic graphene oxide was synthesized and used as an effective catalyst. In this way, Fe
3
O
4
nanoparticles are grown on graphene oxide (GO) nanosheets by a simple and practical method which creates a unique nanostructure (Fe
3
O
4
/GO) through dispersing uniformly among graphene nanosheets. The resulted Pt-APA composite was obtained via adding PtCl
2
to an ethanol solution of Fe
3
O
4
/GO and α-keto stabilized pyridinium ylide in related conditions. The synthesized nanocomposite structure was identified using field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), energy dispersive spectral analysis (EDS), inductively coupled plasma spectrometry (ICP-MS), powder X-ray diffraction (XRD), Fourier transform infrared (FT-IR), vibrating-sample magnetometer (VSM), and UV − Vis spectroscopy. To investigate the catalytic properties of the synthesized Pt-APA@Fe
3
O
4
/GO nanocomposite, it was firstly used as an efficient nano-magnetic catalyst in C–C cross-coupling reaction, Suzuki–Miyaura, with excellent results. Second, the Pt-APA@Fe
3
O
4
/GO nanocomposite has been used as a magnetic photocatalyst to inactivate
E. coli
bacteria on a nutrient agar plate under visible light irradiation, which showed excellent results. By examining the results, the antibacterial durability of nanocomposites Pt-APA@GO/Fe
3
O
4
related to Fe
3
O
4
/GO shows a more significant inhibition against bacteria cell in both dark and visible light.
Graphical abstract
In this study a novel pyridinium complex-functionalized magnetic graphene oxide composite was synthesized and used in photoinactivation of Escherichia coli bacteria under visible light irradiation. It was also used as a promising catalyst in Suzuki–Miyaura C–C coupling reaction. The nanocomposite was characterized by field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), energy dispersive spectral analysis (EDS), powder X-ray diffraction (XRD), Fourier transform infrared (FT-IR), Inductively coupled plasma mass spectrometry (ICP-MS), UV − vis spectroscopy and vibrating-sample magnetometer (VSM).</description><identifier>ISSN: 1388-0764</identifier><identifier>EISSN: 1572-896X</identifier><identifier>DOI: 10.1007/s11051-021-05278-2</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Antiinfectives and antibacterials ; Bacteria ; Catalysts ; Characterization and Evaluation of Materials ; Chemical reactions ; Chemical synthesis ; Chemistry and Materials Science ; Coliforms ; Cross coupling ; Dispersion ; E coli ; Escherichia coli ; Ethanol ; Field emission microscopy ; Fourier analysis ; Fourier transforms ; Graphene ; Inductively coupled plasma mass spectrometry ; Infrared analysis ; Infrared spectroscopy ; Inorganic Chemistry ; Iron oxides ; Irradiation ; Lasers ; Light irradiation ; Magnetic properties ; Magnetometers ; Mass spectrometry ; Mass spectroscopy ; Materials Science ; Nanocomposites ; Nanoparticles ; Nanostructure ; Nanotechnology ; Optical Devices ; Optics ; Photoinactivation ; Photonics ; Physical Chemistry ; Platinum ; Pyridinium ; Research Paper ; Scanning electron microscopy ; Scientific imaging ; Spectral analysis ; Spectroscopy ; Spectrum analysis ; Transmission electron microscopy ; X-ray diffraction</subject><ispartof>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology, 2021-08, Vol.23 (8), Article 192</ispartof><rights>The Author(s), under exclusive licence to Springer Nature B.V. 2021</rights><rights>The Author(s), under exclusive licence to Springer Nature B.V. 2021.</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-e73674ef52da48cefb947c57785116dbb09e6d471f9f1c6c05c5b8d5fb2e5fcc3</citedby><cites>FETCH-LOGICAL-c319t-e73674ef52da48cefb947c57785116dbb09e6d471f9f1c6c05c5b8d5fb2e5fcc3</cites><orcidid>0000-0001-9000-5304</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27903,27904</link.rule.ids></links><search><creatorcontrib>Moniriyan, Faezeh</creatorcontrib><creatorcontrib>Sabounchei, Seyyed Javad</creatorcontrib><creatorcontrib>Yousefi, Abed</creatorcontrib><creatorcontrib>Akhavan, Omid</creatorcontrib><title>Synthesis, morpho-structural properties, and catalytic performances of Pt-APA@Fe3O4/GO nanocomposite based on magnetical graphene in C–C coupling reactions and photoinactivation of E. coli</title><title>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology</title><addtitle>J Nanopart Res</addtitle><description>Herein, a novel Pt-APA composite (APA = pyridinium bromide salt) based on magnetic graphene oxide was synthesized and used as an effective catalyst. In this way, Fe
3
O
4
nanoparticles are grown on graphene oxide (GO) nanosheets by a simple and practical method which creates a unique nanostructure (Fe
3
O
4
/GO) through dispersing uniformly among graphene nanosheets. The resulted Pt-APA composite was obtained via adding PtCl
2
to an ethanol solution of Fe
3
O
4
/GO and α-keto stabilized pyridinium ylide in related conditions. The synthesized nanocomposite structure was identified using field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), energy dispersive spectral analysis (EDS), inductively coupled plasma spectrometry (ICP-MS), powder X-ray diffraction (XRD), Fourier transform infrared (FT-IR), vibrating-sample magnetometer (VSM), and UV − Vis spectroscopy. To investigate the catalytic properties of the synthesized Pt-APA@Fe
3
O
4
/GO nanocomposite, it was firstly used as an efficient nano-magnetic catalyst in C–C cross-coupling reaction, Suzuki–Miyaura, with excellent results. Second, the Pt-APA@Fe
3
O
4
/GO nanocomposite has been used as a magnetic photocatalyst to inactivate
E. coli
bacteria on a nutrient agar plate under visible light irradiation, which showed excellent results. By examining the results, the antibacterial durability of nanocomposites Pt-APA@GO/Fe
3
O
4
related to Fe
3
O
4
/GO shows a more significant inhibition against bacteria cell in both dark and visible light.
Graphical abstract
In this study a novel pyridinium complex-functionalized magnetic graphene oxide composite was synthesized and used in photoinactivation of Escherichia coli bacteria under visible light irradiation. It was also used as a promising catalyst in Suzuki–Miyaura C–C coupling reaction. The nanocomposite was characterized by field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), energy dispersive spectral analysis (EDS), powder X-ray diffraction (XRD), Fourier transform infrared (FT-IR), Inductively coupled plasma mass spectrometry (ICP-MS), UV − vis spectroscopy and vibrating-sample magnetometer (VSM).</description><subject>Antiinfectives and antibacterials</subject><subject>Bacteria</subject><subject>Catalysts</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical reactions</subject><subject>Chemical synthesis</subject><subject>Chemistry and Materials Science</subject><subject>Coliforms</subject><subject>Cross coupling</subject><subject>Dispersion</subject><subject>E coli</subject><subject>Escherichia coli</subject><subject>Ethanol</subject><subject>Field emission microscopy</subject><subject>Fourier analysis</subject><subject>Fourier transforms</subject><subject>Graphene</subject><subject>Inductively coupled plasma mass spectrometry</subject><subject>Infrared analysis</subject><subject>Infrared spectroscopy</subject><subject>Inorganic Chemistry</subject><subject>Iron oxides</subject><subject>Irradiation</subject><subject>Lasers</subject><subject>Light irradiation</subject><subject>Magnetic properties</subject><subject>Magnetometers</subject><subject>Mass spectrometry</subject><subject>Mass spectroscopy</subject><subject>Materials Science</subject><subject>Nanocomposites</subject><subject>Nanoparticles</subject><subject>Nanostructure</subject><subject>Nanotechnology</subject><subject>Optical Devices</subject><subject>Optics</subject><subject>Photoinactivation</subject><subject>Photonics</subject><subject>Physical Chemistry</subject><subject>Platinum</subject><subject>Pyridinium</subject><subject>Research Paper</subject><subject>Scanning electron microscopy</subject><subject>Scientific imaging</subject><subject>Spectral analysis</subject><subject>Spectroscopy</subject><subject>Spectrum analysis</subject><subject>Transmission electron microscopy</subject><subject>X-ray diffraction</subject><issn>1388-0764</issn><issn>1572-896X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp9Uctq3DAUNSWB5vUDXQm6rRJJtix7l2FI0kJgAkkgOyHLVzMKtuRIcmB2-Yf8Tz8mX1JNptBdF-KKc89D6BTFN0rOKSHiIlJKOMWE5cOZaDD7UhxRLhhu2vrpIN_LpsFE1NXX4jjGZ0JozVp2VPy-37q0gWjjDzT6MG08jinMOs1BDWgKfoKQLOStcj3SKqlhm6xGGTY-jMppiMgbdJfw4m5xeQ3lqrq4WSGnnNd-nHy0CVCnIvTIOzSqtYOsz97roKYNOEDWoeXH2_sSaT9Pg3VrFEDpZL2Ln6H5Tclbt4Ne1Q7e5V2dZ_pgT4tDo4YIZ3_nSfF4ffWw_IlvVze_lotbrEvaJgyirEUFhrNeVY0G07WV0FyIhlNa911HWqj7SlDTGqprTbjmXdNz0zHgRuvypPi-980_8jJDTPLZz8HlSMl4XTLGm5JkFtuzdPAxBjByCnZUYSspkbue5L4nmXuSnz1JlkXlXhQz2a0h_LP-j-oPLqya8Q</recordid><startdate>20210801</startdate><enddate>20210801</enddate><creator>Moniriyan, 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morpho-structural properties, and catalytic performances of Pt-APA@Fe3O4/GO nanocomposite based on magnetical graphene in C–C coupling reactions and photoinactivation of E. coli</title><author>Moniriyan, Faezeh ; Sabounchei, Seyyed Javad ; Yousefi, Abed ; Akhavan, Omid</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-e73674ef52da48cefb947c57785116dbb09e6d471f9f1c6c05c5b8d5fb2e5fcc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Antiinfectives and antibacterials</topic><topic>Bacteria</topic><topic>Catalysts</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical reactions</topic><topic>Chemical synthesis</topic><topic>Chemistry and Materials Science</topic><topic>Coliforms</topic><topic>Cross coupling</topic><topic>Dispersion</topic><topic>E coli</topic><topic>Escherichia coli</topic><topic>Ethanol</topic><topic>Field emission microscopy</topic><topic>Fourier analysis</topic><topic>Fourier transforms</topic><topic>Graphene</topic><topic>Inductively coupled plasma mass spectrometry</topic><topic>Infrared analysis</topic><topic>Infrared spectroscopy</topic><topic>Inorganic Chemistry</topic><topic>Iron oxides</topic><topic>Irradiation</topic><topic>Lasers</topic><topic>Light irradiation</topic><topic>Magnetic properties</topic><topic>Magnetometers</topic><topic>Mass spectrometry</topic><topic>Mass spectroscopy</topic><topic>Materials Science</topic><topic>Nanocomposites</topic><topic>Nanoparticles</topic><topic>Nanostructure</topic><topic>Nanotechnology</topic><topic>Optical Devices</topic><topic>Optics</topic><topic>Photoinactivation</topic><topic>Photonics</topic><topic>Physical Chemistry</topic><topic>Platinum</topic><topic>Pyridinium</topic><topic>Research Paper</topic><topic>Scanning electron microscopy</topic><topic>Scientific imaging</topic><topic>Spectral analysis</topic><topic>Spectroscopy</topic><topic>Spectrum analysis</topic><topic>Transmission electron microscopy</topic><topic>X-ray diffraction</topic><toplevel>online_resources</toplevel><creatorcontrib>Moniriyan, Faezeh</creatorcontrib><creatorcontrib>Sabounchei, Seyyed Javad</creatorcontrib><creatorcontrib>Yousefi, Abed</creatorcontrib><creatorcontrib>Akhavan, Omid</creatorcontrib><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Biotechnology Research Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Toxicology Abstracts</collection><collection>Health & Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>ProQuest Pharma Collection</collection><collection>METADEX</collection><collection>Technology 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properties, and catalytic performances of Pt-APA@Fe3O4/GO nanocomposite based on magnetical graphene in C–C coupling reactions and photoinactivation of E. coli</atitle><jtitle>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology</jtitle><stitle>J Nanopart Res</stitle><date>2021-08-01</date><risdate>2021</risdate><volume>23</volume><issue>8</issue><artnum>192</artnum><issn>1388-0764</issn><eissn>1572-896X</eissn><abstract>Herein, a novel Pt-APA composite (APA = pyridinium bromide salt) based on magnetic graphene oxide was synthesized and used as an effective catalyst. In this way, Fe
3
O
4
nanoparticles are grown on graphene oxide (GO) nanosheets by a simple and practical method which creates a unique nanostructure (Fe
3
O
4
/GO) through dispersing uniformly among graphene nanosheets. The resulted Pt-APA composite was obtained via adding PtCl
2
to an ethanol solution of Fe
3
O
4
/GO and α-keto stabilized pyridinium ylide in related conditions. The synthesized nanocomposite structure was identified using field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), energy dispersive spectral analysis (EDS), inductively coupled plasma spectrometry (ICP-MS), powder X-ray diffraction (XRD), Fourier transform infrared (FT-IR), vibrating-sample magnetometer (VSM), and UV − Vis spectroscopy. To investigate the catalytic properties of the synthesized Pt-APA@Fe
3
O
4
/GO nanocomposite, it was firstly used as an efficient nano-magnetic catalyst in C–C cross-coupling reaction, Suzuki–Miyaura, with excellent results. Second, the Pt-APA@Fe
3
O
4
/GO nanocomposite has been used as a magnetic photocatalyst to inactivate
E. coli
bacteria on a nutrient agar plate under visible light irradiation, which showed excellent results. By examining the results, the antibacterial durability of nanocomposites Pt-APA@GO/Fe
3
O
4
related to Fe
3
O
4
/GO shows a more significant inhibition against bacteria cell in both dark and visible light.
Graphical abstract
In this study a novel pyridinium complex-functionalized magnetic graphene oxide composite was synthesized and used in photoinactivation of Escherichia coli bacteria under visible light irradiation. It was also used as a promising catalyst in Suzuki–Miyaura C–C coupling reaction. The nanocomposite was characterized by field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), energy dispersive spectral analysis (EDS), powder X-ray diffraction (XRD), Fourier transform infrared (FT-IR), Inductively coupled plasma mass spectrometry (ICP-MS), UV − vis spectroscopy and vibrating-sample magnetometer (VSM).</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s11051-021-05278-2</doi><orcidid>https://orcid.org/0000-0001-9000-5304</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1388-0764 |
| ispartof | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology, 2021-08, Vol.23 (8), Article 192 |
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| language | eng |
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| source | Springer Nature |
| subjects | Antiinfectives and antibacterials Bacteria Catalysts Characterization and Evaluation of Materials Chemical reactions Chemical synthesis Chemistry and Materials Science Coliforms Cross coupling Dispersion E coli Escherichia coli Ethanol Field emission microscopy Fourier analysis Fourier transforms Graphene Inductively coupled plasma mass spectrometry Infrared analysis Infrared spectroscopy Inorganic Chemistry Iron oxides Irradiation Lasers Light irradiation Magnetic properties Magnetometers Mass spectrometry Mass spectroscopy Materials Science Nanocomposites Nanoparticles Nanostructure Nanotechnology Optical Devices Optics Photoinactivation Photonics Physical Chemistry Platinum Pyridinium Research Paper Scanning electron microscopy Scientific imaging Spectral analysis Spectroscopy Spectrum analysis Transmission electron microscopy X-ray diffraction |
| title | Synthesis, morpho-structural properties, and catalytic performances of Pt-APA@Fe3O4/GO nanocomposite based on magnetical graphene in C–C coupling reactions and photoinactivation of E. coli |
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