Rh(iii)-Catalyzed one-pot three-component cyclization reaction: rapid selective synthesis of monohydroxy polycyclic BINOL derivatives

A Rh(iii)-catalyzed three-component C–H bond functionalization protocol has been successfully applied to access complex polycyclic BINOL derivatives in which the formation of intermediate amides occurred in situ from aldehydes and amines. The high efficiency strategy allows the rapid selective synth...

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Published in:Organic chemistry frontiers an international journal of organic chemistry 2021-09, Vol.8 (18), p.4967-4973
Main Authors: Liu, Hao, Meng-Ling, Lin, Yin-Jun, Chen, Yin-Hui, Huang, Lin, Dong
Format: Article
Language:English
Subjects:
Aldehydes
Amides
Amines
Chemical synthesis
Crystallography
Hydrogen bonds
Organic chemistry
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container_title Organic chemistry frontiers an international journal of organic chemistry
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creator Liu, Hao
Meng-Ling, Lin
Yin-Jun, Chen
Yin-Hui, Huang
Lin, Dong
description A Rh(iii)-catalyzed three-component C–H bond functionalization protocol has been successfully applied to access complex polycyclic BINOL derivatives in which the formation of intermediate amides occurred in situ from aldehydes and amines. The high efficiency strategy allows the rapid selective synthesis of diverse BINOL compounds in a step-economical manner from three readily accessible starting materials in one-pot.
doi_str_mv 10.1039/d1qo00779c
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subjects Aldehydes
Amides
Amines
Chemical synthesis
Crystallography
Hydrogen bonds
Organic chemistry
title Rh(iii)-Catalyzed one-pot three-component cyclization reaction: rapid selective synthesis of monohydroxy polycyclic BINOL derivatives
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