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Filler‐size‐dependent dynamic mechanical properties of polyethylene glycol/zircon composites
The thermomechanical properties of polyethylene glycol (PEG) composites filled with various zircon sizes were studied. The zircon powders were derived from natural (well‐known as puya) sand collected from Kereng Pangi, Central Kalimantan, Indonesia. The effects of the zircon size and content were ex...
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Published in: | Journal of applied polymer science 2022-02, Vol.139 (5), p.n/a |
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creator | Fauziyah, Nur Aini Nurmalasari, Muthia Diah Hilmi, Allif Rosyidy Triwikantoro, Triwikantoro Baqiya, Malik Anjelh Zainuri, Mochamad Pratapa, Suminar |
description | The thermomechanical properties of polyethylene glycol (PEG) composites filled with various zircon sizes were studied. The zircon powders were derived from natural (well‐known as puya) sand collected from Kereng Pangi, Central Kalimantan, Indonesia. The effects of the zircon size and content were examined to understand the thermomechanical properties of the composites using dynamic mechanical analysis in shear mode. Pure zircon powders with micron to nanometer sizes were prepared. The microzircon powders were prepared by heating zircon at 500, 1000, and 1200°C. Moreover, the nanozircon powders were prepared by a wet milling method with milling times of 5, 10, and 15 hours. Furthermore, the composites were prepared by a wet mixing method. According to elemental analysis of scanning electron microscopy/energy dispersive X‐Ray spectroscopy (SEM/EDX) data, it was found that the various zircon sizes caused different distribution effects, that is, in general, the smaller the size was, the better the distribution. Filler size variation also affected the thermomechanical properties of the composites. The addition of microzircon heated at 1200°C had the lowest storage moduli (G'), that is, 154.90 MPa and 155.55 MPa for 5 wt.% and 10 wt.%, respectively. Moreover, the maximum value of G' was obtained for the composite with the addition of nanozircon milled for 10 h (Z10h), that is, 679.27 MPa and 706.37 MPa for 5 and 10 wt.%, respectively. The addition of nanozircon slightly reduced room‐temperature G', presumably due to the agglomerated filler, as confirmed by the SEM/EDX data. Moreover, a decrease in zircon size caused an increase in the melting temperature (Tm) of the matrix. In contrast, 15 h of milling had a minor effect on Tm and G', whereas the loss modulus (G") decreased with the addition of nanozircon. The effects of filler size on the thermomechanical properties of PEG/zircon composites are discussed in detail. |
doi_str_mv | 10.1002/app.51565 |
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The zircon powders were derived from natural (well‐known as puya) sand collected from Kereng Pangi, Central Kalimantan, Indonesia. The effects of the zircon size and content were examined to understand the thermomechanical properties of the composites using dynamic mechanical analysis in shear mode. Pure zircon powders with micron to nanometer sizes were prepared. The microzircon powders were prepared by heating zircon at 500, 1000, and 1200°C. Moreover, the nanozircon powders were prepared by a wet milling method with milling times of 5, 10, and 15 hours. Furthermore, the composites were prepared by a wet mixing method. According to elemental analysis of scanning electron microscopy/energy dispersive X‐Ray spectroscopy (SEM/EDX) data, it was found that the various zircon sizes caused different distribution effects, that is, in general, the smaller the size was, the better the distribution. Filler size variation also affected the thermomechanical properties of the composites. The addition of microzircon heated at 1200°C had the lowest storage moduli (G'), that is, 154.90 MPa and 155.55 MPa for 5 wt.% and 10 wt.%, respectively. Moreover, the maximum value of G' was obtained for the composite with the addition of nanozircon milled for 10 h (Z10h), that is, 679.27 MPa and 706.37 MPa for 5 and 10 wt.%, respectively. The addition of nanozircon slightly reduced room‐temperature G', presumably due to the agglomerated filler, as confirmed by the SEM/EDX data. Moreover, a decrease in zircon size caused an increase in the melting temperature (Tm) of the matrix. In contrast, 15 h of milling had a minor effect on Tm and G', whereas the loss modulus (G") decreased with the addition of nanozircon. The effects of filler size on the thermomechanical properties of PEG/zircon composites are discussed in detail.</description><identifier>ISSN: 0021-8995</identifier><identifier>EISSN: 1097-4628</identifier><identifier>DOI: 10.1002/app.51565</identifier><language>eng</language><publisher>Hoboken, USA: John Wiley & Sons, Inc</publisher><subject>Composite materials ; Dynamic mechanical analysis ; Dynamic mechanical properties ; Fillers ; Loss modulus ; Materials science ; Mechanical properties ; Melt temperature ; nano‐ and micron‐sized filler ; PEG ; Polyethylene glycol ; Polymers ; Scanning electron microscopy ; Thermomechanical properties ; Wet milling ; Zircon</subject><ispartof>Journal of applied polymer science, 2022-02, Vol.139 (5), p.n/a</ispartof><rights>2021 Wiley Periodicals LLC.</rights><rights>2022 Wiley Periodicals LLC.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c2975-de7689a7d2bae4e281734bd4f259b52124df3e53a124e6d1fd8c04d5f05bd753</citedby><cites>FETCH-LOGICAL-c2975-de7689a7d2bae4e281734bd4f259b52124df3e53a124e6d1fd8c04d5f05bd753</cites><orcidid>0000-0003-2337-3566 ; 0000-0002-9603-9828</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Fauziyah, Nur Aini</creatorcontrib><creatorcontrib>Nurmalasari, Muthia Diah</creatorcontrib><creatorcontrib>Hilmi, Allif Rosyidy</creatorcontrib><creatorcontrib>Triwikantoro, Triwikantoro</creatorcontrib><creatorcontrib>Baqiya, Malik Anjelh</creatorcontrib><creatorcontrib>Zainuri, Mochamad</creatorcontrib><creatorcontrib>Pratapa, Suminar</creatorcontrib><title>Filler‐size‐dependent dynamic mechanical properties of polyethylene glycol/zircon composites</title><title>Journal of applied polymer science</title><description>The thermomechanical properties of polyethylene glycol (PEG) composites filled with various zircon sizes were studied. The zircon powders were derived from natural (well‐known as puya) sand collected from Kereng Pangi, Central Kalimantan, Indonesia. The effects of the zircon size and content were examined to understand the thermomechanical properties of the composites using dynamic mechanical analysis in shear mode. Pure zircon powders with micron to nanometer sizes were prepared. The microzircon powders were prepared by heating zircon at 500, 1000, and 1200°C. Moreover, the nanozircon powders were prepared by a wet milling method with milling times of 5, 10, and 15 hours. Furthermore, the composites were prepared by a wet mixing method. According to elemental analysis of scanning electron microscopy/energy dispersive X‐Ray spectroscopy (SEM/EDX) data, it was found that the various zircon sizes caused different distribution effects, that is, in general, the smaller the size was, the better the distribution. Filler size variation also affected the thermomechanical properties of the composites. The addition of microzircon heated at 1200°C had the lowest storage moduli (G'), that is, 154.90 MPa and 155.55 MPa for 5 wt.% and 10 wt.%, respectively. Moreover, the maximum value of G' was obtained for the composite with the addition of nanozircon milled for 10 h (Z10h), that is, 679.27 MPa and 706.37 MPa for 5 and 10 wt.%, respectively. The addition of nanozircon slightly reduced room‐temperature G', presumably due to the agglomerated filler, as confirmed by the SEM/EDX data. Moreover, a decrease in zircon size caused an increase in the melting temperature (Tm) of the matrix. In contrast, 15 h of milling had a minor effect on Tm and G', whereas the loss modulus (G") decreased with the addition of nanozircon. The effects of filler size on the thermomechanical properties of PEG/zircon composites are discussed in detail.</description><subject>Composite materials</subject><subject>Dynamic mechanical analysis</subject><subject>Dynamic mechanical properties</subject><subject>Fillers</subject><subject>Loss modulus</subject><subject>Materials science</subject><subject>Mechanical properties</subject><subject>Melt temperature</subject><subject>nano‐ and micron‐sized filler</subject><subject>PEG</subject><subject>Polyethylene glycol</subject><subject>Polymers</subject><subject>Scanning electron microscopy</subject><subject>Thermomechanical properties</subject><subject>Wet milling</subject><subject>Zircon</subject><issn>0021-8995</issn><issn>1097-4628</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp1kE1OwzAQhS0EEqWw4AaRWLFIaztxfpZVxZ9UiS66N449oa6c2NipULriCJyRk2AoW1ZvpPlm3tND6JrgGcGYzoVzM0ZYwU7QhOC6TPOCVqdoEnckreqanaOLEHYYE8JwMUEv99oY8F8fn0EfIIoCB72CfkjU2ItOy6QDuRW9lsIkzlsHftAQEtsmzpoRhu1ooIfk1YzSmvlBe2n7RNrO2aAHCJforBUmwNWfTtHm_m6zfExXzw9Py8UqlbQuWaqgLKpalIo2AnKgFSmzvFF5S1ndMEportoMWCbiBIUiraokzhVrMWtUybIpujm-jRHf9hAGvrN730dHTlmV4WhSl5G6PVLS2xA8tNx53Qk_coL5T3889sd_-4vs_Mi-awPj_yBfrNfHi29cMHXY</recordid><startdate>20220205</startdate><enddate>20220205</enddate><creator>Fauziyah, Nur Aini</creator><creator>Nurmalasari, Muthia Diah</creator><creator>Hilmi, Allif Rosyidy</creator><creator>Triwikantoro, Triwikantoro</creator><creator>Baqiya, Malik Anjelh</creator><creator>Zainuri, Mochamad</creator><creator>Pratapa, Suminar</creator><general>John Wiley & Sons, Inc</general><general>Wiley Subscription Services, Inc</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope><orcidid>https://orcid.org/0000-0003-2337-3566</orcidid><orcidid>https://orcid.org/0000-0002-9603-9828</orcidid></search><sort><creationdate>20220205</creationdate><title>Filler‐size‐dependent dynamic mechanical properties of polyethylene glycol/zircon composites</title><author>Fauziyah, Nur Aini ; Nurmalasari, Muthia Diah ; Hilmi, Allif Rosyidy ; Triwikantoro, Triwikantoro ; Baqiya, Malik Anjelh ; Zainuri, Mochamad ; Pratapa, Suminar</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2975-de7689a7d2bae4e281734bd4f259b52124df3e53a124e6d1fd8c04d5f05bd753</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Composite materials</topic><topic>Dynamic mechanical analysis</topic><topic>Dynamic mechanical properties</topic><topic>Fillers</topic><topic>Loss modulus</topic><topic>Materials science</topic><topic>Mechanical properties</topic><topic>Melt temperature</topic><topic>nano‐ and micron‐sized filler</topic><topic>PEG</topic><topic>Polyethylene glycol</topic><topic>Polymers</topic><topic>Scanning electron microscopy</topic><topic>Thermomechanical properties</topic><topic>Wet milling</topic><topic>Zircon</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Fauziyah, Nur Aini</creatorcontrib><creatorcontrib>Nurmalasari, Muthia Diah</creatorcontrib><creatorcontrib>Hilmi, Allif Rosyidy</creatorcontrib><creatorcontrib>Triwikantoro, Triwikantoro</creatorcontrib><creatorcontrib>Baqiya, Malik Anjelh</creatorcontrib><creatorcontrib>Zainuri, Mochamad</creatorcontrib><creatorcontrib>Pratapa, Suminar</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of applied polymer science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Fauziyah, Nur Aini</au><au>Nurmalasari, Muthia Diah</au><au>Hilmi, Allif Rosyidy</au><au>Triwikantoro, Triwikantoro</au><au>Baqiya, Malik Anjelh</au><au>Zainuri, Mochamad</au><au>Pratapa, Suminar</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Filler‐size‐dependent dynamic mechanical properties of polyethylene glycol/zircon composites</atitle><jtitle>Journal of applied polymer science</jtitle><date>2022-02-05</date><risdate>2022</risdate><volume>139</volume><issue>5</issue><epage>n/a</epage><issn>0021-8995</issn><eissn>1097-4628</eissn><abstract>The thermomechanical properties of polyethylene glycol (PEG) composites filled with various zircon sizes were studied. The zircon powders were derived from natural (well‐known as puya) sand collected from Kereng Pangi, Central Kalimantan, Indonesia. The effects of the zircon size and content were examined to understand the thermomechanical properties of the composites using dynamic mechanical analysis in shear mode. Pure zircon powders with micron to nanometer sizes were prepared. The microzircon powders were prepared by heating zircon at 500, 1000, and 1200°C. Moreover, the nanozircon powders were prepared by a wet milling method with milling times of 5, 10, and 15 hours. Furthermore, the composites were prepared by a wet mixing method. According to elemental analysis of scanning electron microscopy/energy dispersive X‐Ray spectroscopy (SEM/EDX) data, it was found that the various zircon sizes caused different distribution effects, that is, in general, the smaller the size was, the better the distribution. Filler size variation also affected the thermomechanical properties of the composites. The addition of microzircon heated at 1200°C had the lowest storage moduli (G'), that is, 154.90 MPa and 155.55 MPa for 5 wt.% and 10 wt.%, respectively. Moreover, the maximum value of G' was obtained for the composite with the addition of nanozircon milled for 10 h (Z10h), that is, 679.27 MPa and 706.37 MPa for 5 and 10 wt.%, respectively. The addition of nanozircon slightly reduced room‐temperature G', presumably due to the agglomerated filler, as confirmed by the SEM/EDX data. Moreover, a decrease in zircon size caused an increase in the melting temperature (Tm) of the matrix. In contrast, 15 h of milling had a minor effect on Tm and G', whereas the loss modulus (G") decreased with the addition of nanozircon. The effects of filler size on the thermomechanical properties of PEG/zircon composites are discussed in detail.</abstract><cop>Hoboken, USA</cop><pub>John Wiley & Sons, Inc</pub><doi>10.1002/app.51565</doi><tpages>15</tpages><orcidid>https://orcid.org/0000-0003-2337-3566</orcidid><orcidid>https://orcid.org/0000-0002-9603-9828</orcidid></addata></record> |
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subjects | Composite materials Dynamic mechanical analysis Dynamic mechanical properties Fillers Loss modulus Materials science Mechanical properties Melt temperature nano‐ and micron‐sized filler PEG Polyethylene glycol Polymers Scanning electron microscopy Thermomechanical properties Wet milling Zircon |
title | Filler‐size‐dependent dynamic mechanical properties of polyethylene glycol/zircon composites |
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