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On Investigating the Microstructural Evolution of Hot-Pressed TiB2-Reinforced Steel Composites
In the current work, TiB 2 reinforced steel matrix composites were synthesized by a technically feasible and cost-effective hot pressing route. A detailed microstructural analysis of the resultant composite was studied. Using a field emission scanning electron microscope (FESEM) and transmission ele...
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| Published in: | Transactions of the Indian Institute of Metals 2022-03, Vol.75 (3), p.789-796 |
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| Main Authors: | , , , |
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| container_end_page | 796 |
| container_issue | 3 |
| container_start_page | 789 |
| container_title | Transactions of the Indian Institute of Metals |
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| creator | Sahoo, Silani Jha, Bharat Bhushan Panigrahi, Ajit Mandal, Animesh |
| description | In the current work, TiB
2
reinforced steel matrix composites were synthesized by a technically feasible and cost-effective hot pressing route. A detailed microstructural analysis of the resultant composite was studied. Using a field emission scanning electron microscope (FESEM) and transmission electron microscopy (TEM), the microstructure evolution of the composite was studied. FESEM observations indicated the homogeneous distribution of TiB
2
particles in the matrix. The results also revealed the formation of elongated Cr–Fe–Ni phases (fcc:
a
= 3.5537 Å space group = Fm
3
¯
m) in a sympathetic fashion. The size of this phase ranges from 200 to 400 nm. TEM observations indicated a clear interface between steel matrix and TiB
2
particles. |
| doi_str_mv | 10.1007/s12666-021-02496-z |
| format | article |
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2
reinforced steel matrix composites were synthesized by a technically feasible and cost-effective hot pressing route. A detailed microstructural analysis of the resultant composite was studied. Using a field emission scanning electron microscope (FESEM) and transmission electron microscopy (TEM), the microstructure evolution of the composite was studied. FESEM observations indicated the homogeneous distribution of TiB
2
particles in the matrix. The results also revealed the formation of elongated Cr–Fe–Ni phases (fcc:
a
= 3.5537 Å space group = Fm
3
¯
m) in a sympathetic fashion. The size of this phase ranges from 200 to 400 nm. TEM observations indicated a clear interface between steel matrix and TiB
2
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2
reinforced steel matrix composites were synthesized by a technically feasible and cost-effective hot pressing route. A detailed microstructural analysis of the resultant composite was studied. Using a field emission scanning electron microscope (FESEM) and transmission electron microscopy (TEM), the microstructure evolution of the composite was studied. FESEM observations indicated the homogeneous distribution of TiB
2
particles in the matrix. The results also revealed the formation of elongated Cr–Fe–Ni phases (fcc:
a
= 3.5537 Å space group = Fm
3
¯
m) in a sympathetic fashion. The size of this phase ranges from 200 to 400 nm. TEM observations indicated a clear interface between steel matrix and TiB
2
particles.</description><subject>Chemistry and Materials Science</subject><subject>Corrosion and Coatings</subject><subject>Cost analysis</subject><subject>Electron microscopes</subject><subject>Emission analysis</subject><subject>Evolution</subject><subject>Field emission microscopy</subject><subject>Hot pressing</subject><subject>Materials Science</subject><subject>Metal matrix composites</subject><subject>Metallic Materials</subject><subject>Microstructural analysis</subject><subject>Microstructure</subject><subject>Original Article</subject><subject>Reinforcing steels</subject><subject>Titanium diboride</subject><subject>Transmission electron microscopy</subject><subject>Tribology</subject><issn>0972-2815</issn><issn>0975-1645</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp9UE1LAzEQDaJgrf4BTwHP0Xx0J7tHLdUWKorWq2E3JnXLdlOTbMH-etOu4M3DMDPw3pt5D6FLRq8ZpfImMA4AhHKWalQA2R2hAS1kRhiMsuPDzAnPWXaKzkJYUSoKLsQAvT-1eNZuTYj1sox1u8Tx0-DHWnsXou907HzZ4MnWNV2sXYudxVMXybM3IZgPvKjvOHkxdWud12l_jcY0eOzWGxfqaMI5OrFlE8zFbx-it_vJYjwl86eH2fh2TjSXNBLQFeSy1BJYwSppqC20LU36WRgroQLQlmVFDlLwPBNcSF5pnee0MBWFUSmG6KrX3Xj31SU3auU636aTioOgiQQCEor3qL274I1VG1-vS_-tGFX7HFWfo0o5qkOOapdIoieFBG6Xxv9J_8P6AfuKdrc</recordid><startdate>202203</startdate><enddate>202203</enddate><creator>Sahoo, Silani</creator><creator>Jha, Bharat Bhushan</creator><creator>Panigrahi, Ajit</creator><creator>Mandal, Animesh</creator><general>Springer India</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>202203</creationdate><title>On Investigating the Microstructural Evolution of Hot-Pressed TiB2-Reinforced Steel Composites</title><author>Sahoo, Silani ; Jha, Bharat Bhushan ; Panigrahi, Ajit ; Mandal, Animesh</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c270t-6cb687ac76191b7e0f9cfae9723ef76b66cf159867328532372bcc8809eb064a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Chemistry and Materials Science</topic><topic>Corrosion and Coatings</topic><topic>Cost analysis</topic><topic>Electron microscopes</topic><topic>Emission analysis</topic><topic>Evolution</topic><topic>Field emission microscopy</topic><topic>Hot pressing</topic><topic>Materials Science</topic><topic>Metal matrix composites</topic><topic>Metallic Materials</topic><topic>Microstructural analysis</topic><topic>Microstructure</topic><topic>Original Article</topic><topic>Reinforcing steels</topic><topic>Titanium diboride</topic><topic>Transmission electron microscopy</topic><topic>Tribology</topic><toplevel>online_resources</toplevel><creatorcontrib>Sahoo, Silani</creatorcontrib><creatorcontrib>Jha, Bharat Bhushan</creatorcontrib><creatorcontrib>Panigrahi, Ajit</creatorcontrib><creatorcontrib>Mandal, Animesh</creatorcontrib><collection>CrossRef</collection><jtitle>Transactions of the Indian Institute of Metals</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sahoo, Silani</au><au>Jha, Bharat Bhushan</au><au>Panigrahi, Ajit</au><au>Mandal, Animesh</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>On Investigating the Microstructural Evolution of Hot-Pressed TiB2-Reinforced Steel Composites</atitle><jtitle>Transactions of the Indian Institute of Metals</jtitle><stitle>Trans Indian Inst Met</stitle><date>2022-03</date><risdate>2022</risdate><volume>75</volume><issue>3</issue><spage>789</spage><epage>796</epage><pages>789-796</pages><issn>0972-2815</issn><eissn>0975-1645</eissn><abstract>In the current work, TiB
2
reinforced steel matrix composites were synthesized by a technically feasible and cost-effective hot pressing route. A detailed microstructural analysis of the resultant composite was studied. Using a field emission scanning electron microscope (FESEM) and transmission electron microscopy (TEM), the microstructure evolution of the composite was studied. FESEM observations indicated the homogeneous distribution of TiB
2
particles in the matrix. The results also revealed the formation of elongated Cr–Fe–Ni phases (fcc:
a
= 3.5537 Å space group = Fm
3
¯
m) in a sympathetic fashion. The size of this phase ranges from 200 to 400 nm. TEM observations indicated a clear interface between steel matrix and TiB
2
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| ispartof | Transactions of the Indian Institute of Metals, 2022-03, Vol.75 (3), p.789-796 |
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| subjects | Chemistry and Materials Science Corrosion and Coatings Cost analysis Electron microscopes Emission analysis Evolution Field emission microscopy Hot pressing Materials Science Metal matrix composites Metallic Materials Microstructural analysis Microstructure Original Article Reinforcing steels Titanium diboride Transmission electron microscopy Tribology |
| title | On Investigating the Microstructural Evolution of Hot-Pressed TiB2-Reinforced Steel Composites |
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