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Implication of initial grain size on DRX mechanism and grain refinement in super-304H SS in a wide range of strain rates during large-strain hot deformation

In this work, we studied the effect of initial grain size on the hot compression characteristics of super-304H austenitic stainless steel in a range of strain rates (0.001–1 s−1) at a fixed temperature of 1223 K. Analysis of the flow curves reveals that the flow stress is inversely proportional to t...

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Published in:Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2022-01, Vol.832, p.142269, Article 142269
Main Authors: Arun Babu, K., Mozumder, Yahya H., Athreya, C.N., Sarma, V.Subramanya, Mandal, Sumantra
Format: Article
Language:English
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Summary:In this work, we studied the effect of initial grain size on the hot compression characteristics of super-304H austenitic stainless steel in a range of strain rates (0.001–1 s−1) at a fixed temperature of 1223 K. Analysis of the flow curves reveals that the flow stress is inversely proportional to the average sub-grain diameter in both coarse and fine-grained specimens at higher strain (≥0.5) levels. Further, the fine-grained specimen following deformation at a low strain rate (0.001 s−1) reveals the occurrence of both continuous dynamic recrystallization (CDRX) and discontinuous dynamic recrystallization (DDRX) mechanisms. In this condition, the CDRX is characterized by a progressive increase of boundary misorientation, while the DDRX is characterized by bulging and strain-induced boundary migration. In contrast, the CDRX characterized by the formation of microbands is majorly responsible for the grain refinement in the fine-grained specimen at higher strain rates (∼1 s−1) and in the coarse-grained specimen at all strain rates (0.001–1 s−1). The superposition of different DRX mechanisms leads to significant variations in grain refinement kinetics with strain rates and initial grain sizes. The findings of this investigation provide a foundation for the accurate control of the microstructures in the studied alloy with different initial grain sizes during the hot working at various strain rates. [Display omitted] •Large strain hot compression in super-304H is conducted at 1223 K and 0.001–1 s−1.•Avrami exponent is weakly dependent on strain rate but varies with initial grain size.•Fine-grained specimen at 0.001 s−1 reveals both DDRX and CDRX mechanisms.•Fine and coarse-grained specimens at 1 s−1 reveal CDRX assisted by microbanding.•Superposition of DRX mechanisms leads to variations in grain refinement kinetics.
ISSN:0921-5093
1873-4936
DOI:10.1016/j.msea.2021.142269