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Synthesis of sulfonated melamine-functionalized Fe3O4@SiO2@Si–(CH2)3@melamine nanoparticles and its application in the synthesis of 4,4’-(aryl methylene)bis(3-methyl-1H-pyrazol-5-ol)s and hexahydroquinolines
In this work, sulfonated melamine-functionalized Fe 3 O 4 @SiO 2 @Si-(CH 2 ) 3 @melamine nanoparticles were prepared through a simple approach and characterized by energy dispersive X-ray analysis (EDX), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), the...
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| Published in: | Journal of the Iranian Chemical Society 2022-05, Vol.19 (5), p.1849-1863 |
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| Main Authors: | , , , |
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| cited_by | cdi_FETCH-LOGICAL-c2348-a4510405ff8d99a910953e7a004bcf792fb632c18607bd441bc0a3ffa25861473 |
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| cites | cdi_FETCH-LOGICAL-c2348-a4510405ff8d99a910953e7a004bcf792fb632c18607bd441bc0a3ffa25861473 |
| container_end_page | 1863 |
| container_issue | 5 |
| container_start_page | 1849 |
| container_title | Journal of the Iranian Chemical Society |
| container_volume | 19 |
| creator | Soleimani, Maryam Khazaei, Ardeshir Sarmasti, Negin Akbarpour, Tahereh |
| description | In this work, sulfonated melamine-functionalized Fe
3
O
4
@SiO
2
@Si-(CH
2
)
3
@melamine nanoparticles were prepared through a simple approach and characterized by energy dispersive X-ray analysis (EDX), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), thermal gravimetric analysis (TGA), vibrating sample magnetometer (VSM), and infrared (IR). The catalytic activity of the synthesized catalyst was investigated in the synthesis of 4,4'-(aryl methylene)bis(3-methyl-1
H
-pyrazol-5-ol)s and hexahydroquinolines (HHQs) via the one-pot reactions under solvent-free conditions. Short reaction time, waste to wealth, high yield, and solvent-free conditions are the most important benefits of the present work. |
| doi_str_mv | 10.1007/s13738-021-02420-8 |
| format | article |
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3
O
4
@SiO
2
@Si-(CH
2
)
3
@melamine nanoparticles were prepared through a simple approach and characterized by energy dispersive X-ray analysis (EDX), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), thermal gravimetric analysis (TGA), vibrating sample magnetometer (VSM), and infrared (IR). The catalytic activity of the synthesized catalyst was investigated in the synthesis of 4,4'-(aryl methylene)bis(3-methyl-1
H
-pyrazol-5-ol)s and hexahydroquinolines (HHQs) via the one-pot reactions under solvent-free conditions. Short reaction time, waste to wealth, high yield, and solvent-free conditions are the most important benefits of the present work.</description><identifier>ISSN: 1735-207X</identifier><identifier>EISSN: 1735-2428</identifier><identifier>DOI: 10.1007/s13738-021-02420-8</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Analytical Chemistry ; Aromatic compounds ; Biochemistry ; Catalytic activity ; Chemical synthesis ; Chemistry ; Chemistry and Materials Science ; Electron microscopy ; Emission analysis ; Energy dispersive X ray analysis ; Field emission microscopy ; Gravimetric analysis ; Infrared analysis ; Inorganic Chemistry ; Iron oxides ; Melamine ; Methylene ; Microscopy ; Nanoparticles ; Organic Chemistry ; Original Paper ; Physical Chemistry ; Reaction time ; Silicon dioxide ; Solvents ; Thermal analysis ; X ray analysis</subject><ispartof>Journal of the Iranian Chemical Society, 2022-05, Vol.19 (5), p.1849-1863</ispartof><rights>Iranian Chemical Society 2021</rights><rights>Iranian Chemical Society 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c2348-a4510405ff8d99a910953e7a004bcf792fb632c18607bd441bc0a3ffa25861473</citedby><cites>FETCH-LOGICAL-c2348-a4510405ff8d99a910953e7a004bcf792fb632c18607bd441bc0a3ffa25861473</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27922,27923</link.rule.ids></links><search><creatorcontrib>Soleimani, Maryam</creatorcontrib><creatorcontrib>Khazaei, Ardeshir</creatorcontrib><creatorcontrib>Sarmasti, Negin</creatorcontrib><creatorcontrib>Akbarpour, Tahereh</creatorcontrib><title>Synthesis of sulfonated melamine-functionalized Fe3O4@SiO2@Si–(CH2)3@melamine nanoparticles and its application in the synthesis of 4,4’-(aryl methylene)bis(3-methyl-1H-pyrazol-5-ol)s and hexahydroquinolines</title><title>Journal of the Iranian Chemical Society</title><addtitle>J IRAN CHEM SOC</addtitle><description>In this work, sulfonated melamine-functionalized Fe
3
O
4
@SiO
2
@Si-(CH
2
)
3
@melamine nanoparticles were prepared through a simple approach and characterized by energy dispersive X-ray analysis (EDX), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), thermal gravimetric analysis (TGA), vibrating sample magnetometer (VSM), and infrared (IR). The catalytic activity of the synthesized catalyst was investigated in the synthesis of 4,4'-(aryl methylene)bis(3-methyl-1
H
-pyrazol-5-ol)s and hexahydroquinolines (HHQs) via the one-pot reactions under solvent-free conditions. Short reaction time, waste to wealth, high yield, and solvent-free conditions are the most important benefits of the present work.</description><subject>Analytical Chemistry</subject><subject>Aromatic compounds</subject><subject>Biochemistry</subject><subject>Catalytic activity</subject><subject>Chemical synthesis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Electron microscopy</subject><subject>Emission analysis</subject><subject>Energy dispersive X ray analysis</subject><subject>Field emission microscopy</subject><subject>Gravimetric analysis</subject><subject>Infrared analysis</subject><subject>Inorganic Chemistry</subject><subject>Iron oxides</subject><subject>Melamine</subject><subject>Methylene</subject><subject>Microscopy</subject><subject>Nanoparticles</subject><subject>Organic Chemistry</subject><subject>Original Paper</subject><subject>Physical Chemistry</subject><subject>Reaction time</subject><subject>Silicon dioxide</subject><subject>Solvents</subject><subject>Thermal analysis</subject><subject>X ray analysis</subject><issn>1735-207X</issn><issn>1735-2428</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp9UU1uEzEUHiGQKIULsLLEJpEwPP_FM7uiiDZIlbIoSOwsz4xNXDn2YE-kTle9AyvO1Rv0JDgMFaxY2M_v6fux_VXVawLvCIB8nwmTrMZASVmcAq6fVCdEMoFLVz99PIP8-rx6kfM1gJAg-El1fzWFcWeyyyhalA_exqBH06O98XrvgsH2ELrRlal3t2V-btiWn125LS3bw92PxXpDl-zsEY6CDnHQaXSdNxnp0CM3ljoM3nX6qINcQMUR5X-N-Vv-cPcTL3SafLEed5M3wSxblxcMzz0mGzxMSd9GjwWOfjmr78yN3k19it8PLkRfrpBfVs-s9tm8-lNPqy_nHz-vN_hye_Fp_eESd5TxGmsuCHAQ1tZ90-iGQCOYkRqAt52VDbXtitGO1CuQbc85aTvQzFpNRb0iXLLT6s2sOxzdTR7VdTyk8lFZ0ZUghDeUkYKiM6pLMedkrBqS25eHKgLqGJ6aw1MlPPU7PFUXEptJuYDDN5P-Sv-H9Qt4M6Dh</recordid><startdate>20220501</startdate><enddate>20220501</enddate><creator>Soleimani, Maryam</creator><creator>Khazaei, Ardeshir</creator><creator>Sarmasti, Negin</creator><creator>Akbarpour, Tahereh</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20220501</creationdate><title>Synthesis of sulfonated melamine-functionalized Fe3O4@SiO2@Si–(CH2)3@melamine nanoparticles and its application in the synthesis of 4,4’-(aryl methylene)bis(3-methyl-1H-pyrazol-5-ol)s and hexahydroquinolines</title><author>Soleimani, Maryam ; Khazaei, Ardeshir ; Sarmasti, Negin ; Akbarpour, Tahereh</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2348-a4510405ff8d99a910953e7a004bcf792fb632c18607bd441bc0a3ffa25861473</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Analytical Chemistry</topic><topic>Aromatic compounds</topic><topic>Biochemistry</topic><topic>Catalytic activity</topic><topic>Chemical synthesis</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Electron microscopy</topic><topic>Emission analysis</topic><topic>Energy dispersive X ray analysis</topic><topic>Field emission microscopy</topic><topic>Gravimetric analysis</topic><topic>Infrared analysis</topic><topic>Inorganic Chemistry</topic><topic>Iron oxides</topic><topic>Melamine</topic><topic>Methylene</topic><topic>Microscopy</topic><topic>Nanoparticles</topic><topic>Organic Chemistry</topic><topic>Original Paper</topic><topic>Physical Chemistry</topic><topic>Reaction time</topic><topic>Silicon dioxide</topic><topic>Solvents</topic><topic>Thermal analysis</topic><topic>X ray analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Soleimani, Maryam</creatorcontrib><creatorcontrib>Khazaei, Ardeshir</creatorcontrib><creatorcontrib>Sarmasti, Negin</creatorcontrib><creatorcontrib>Akbarpour, Tahereh</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of the Iranian Chemical Society</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Soleimani, Maryam</au><au>Khazaei, Ardeshir</au><au>Sarmasti, Negin</au><au>Akbarpour, Tahereh</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of sulfonated melamine-functionalized Fe3O4@SiO2@Si–(CH2)3@melamine nanoparticles and its application in the synthesis of 4,4’-(aryl methylene)bis(3-methyl-1H-pyrazol-5-ol)s and hexahydroquinolines</atitle><jtitle>Journal of the Iranian Chemical Society</jtitle><stitle>J IRAN CHEM SOC</stitle><date>2022-05-01</date><risdate>2022</risdate><volume>19</volume><issue>5</issue><spage>1849</spage><epage>1863</epage><pages>1849-1863</pages><issn>1735-207X</issn><eissn>1735-2428</eissn><abstract>In this work, sulfonated melamine-functionalized Fe
3
O
4
@SiO
2
@Si-(CH
2
)
3
@melamine nanoparticles were prepared through a simple approach and characterized by energy dispersive X-ray analysis (EDX), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), thermal gravimetric analysis (TGA), vibrating sample magnetometer (VSM), and infrared (IR). The catalytic activity of the synthesized catalyst was investigated in the synthesis of 4,4'-(aryl methylene)bis(3-methyl-1
H
-pyrazol-5-ol)s and hexahydroquinolines (HHQs) via the one-pot reactions under solvent-free conditions. Short reaction time, waste to wealth, high yield, and solvent-free conditions are the most important benefits of the present work.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s13738-021-02420-8</doi><tpages>15</tpages></addata></record> |
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| ispartof | Journal of the Iranian Chemical Society, 2022-05, Vol.19 (5), p.1849-1863 |
| issn | 1735-207X 1735-2428 |
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| source | Springer Nature |
| subjects | Analytical Chemistry Aromatic compounds Biochemistry Catalytic activity Chemical synthesis Chemistry Chemistry and Materials Science Electron microscopy Emission analysis Energy dispersive X ray analysis Field emission microscopy Gravimetric analysis Infrared analysis Inorganic Chemistry Iron oxides Melamine Methylene Microscopy Nanoparticles Organic Chemistry Original Paper Physical Chemistry Reaction time Silicon dioxide Solvents Thermal analysis X ray analysis |
| title | Synthesis of sulfonated melamine-functionalized Fe3O4@SiO2@Si–(CH2)3@melamine nanoparticles and its application in the synthesis of 4,4’-(aryl methylene)bis(3-methyl-1H-pyrazol-5-ol)s and hexahydroquinolines |
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