Mitigation of autogenous shrinkage of high-strength concrete using rice husk ashes with distinct pore structures

• Published in: Advances in cement research 2022-04, Vol.34 (4), p.151-160
• Main Authors: Vieira, Amanda Pereira, Toledo Filho, Romildo Dias, Tavares, Luís Marcelo, Cordeiro, Guilherme Chagas
• Format: Article
• Language: English
• Subjects: Ashes; Compressive strength; Concrete; Factorial analysis; High strength concretes; Hydration; Nucleation; Porosity; Pozzolans; Shrinkage; Statistical methods
• ISSN: 0951-7197; 1751-7605
• DOI: 10.1680/jadcr.21.00031

The effect of particle size (50% passing size (D 50 ) of 20 μm, 14 μm and 7 μm) and content (8%, 10% and 12% by mass) of rice husk ash (RHA) on the autogenous shrinkage evolution of high-strength concrete was investigated. RHA samples were selected based on differences in their pore structures, which were investigated by means of nitrogen adsorption isotherms, scanning electron microscopy and absorbency tests. Cement–pozzolan hydration development was studied using isothermal calorimetry. The concretes were subjected to mercury intrusion porosimetry and compressive strength tests. Considering a statistical 2 2 factorial analysis with a central point, the results showed that D 50 and the interaction between D 50 and RHA content influenced the autogenous shrinkage at 28 and 100 days. The water absorbed internally by the preserved RHA pore structure (D 50  ≈ 20 μm) in the high cement replacement (12% RHA) mixes reduced the final autogenous shrinkage of concrete without a decrease in compressive strength. In addition, the RHA with a more preserved pore structure accelerated the hydration kinetics by heterogeneous nucleation. However, this behaviour did not influence the early autogenous shrinkage results.