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The ferroelectric phase transition in a 500 nm sized single particle of BaTiO3 tracked by coherent X-ray diffraction
The shapes and sizes of grains influence the anisotropy of crystal structures and the configuration of ferroelectric domains. In order to better understand these effects, we introduce a method to observe a ferroelectric phase transition in a single ferroelectric particle of sub-micrometer size. The...
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Published in: | Japanese Journal of Applied Physics 2022-11, Vol.61 (SN), p.SN1008 |
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container_title | Japanese Journal of Applied Physics |
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creator | Oshime, Norihiro Ohwada, Kenji Machida, Akihiko Fukushima, Nagise Ueno, Shintaro Fujii, Ichiro Wada, Satoshi Sugawara, Kento Shimada, Ayumu Ueno, Tetsuro Watanuki, Tetsu Ishii, Kenji Toyokawa, Hidenori Momma, Koichi Kim, Sangwook Tsukada, Shinya Kuroiwa, Yoshihiro |
description | The shapes and sizes of grains influence the anisotropy of crystal structures and the configuration of ferroelectric domains. In order to better understand these effects, we introduce a method to observe a ferroelectric phase transition in a single ferroelectric particle of sub-micrometer size. The phase transition was observed by cooling the sample through its Curie temperature, and studying the pattern variations of Bragg coherent X-ray diffraction from a single particle of 500 nm sized BaTiO3. A change from a single 200 peak (cubic phase) to both 200 and 002 peaks (tetragonal phase); was seen, with fringes connecting them like a bridge. The pattern from the BaTiO3 particle in the cubic phase was also imaged using Bragg coherent diffraction imaging. The apparent strain distribution caused by dislocation internal to the BaTiO3 crystal was visible in the reconstructed image. |
doi_str_mv | 10.35848/1347-4065/ac7d94 |
format | article |
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In order to better understand these effects, we introduce a method to observe a ferroelectric phase transition in a single ferroelectric particle of sub-micrometer size. The phase transition was observed by cooling the sample through its Curie temperature, and studying the pattern variations of Bragg coherent X-ray diffraction from a single particle of 500 nm sized BaTiO3. A change from a single 200 peak (cubic phase) to both 200 and 002 peaks (tetragonal phase); was seen, with fringes connecting them like a bridge. The pattern from the BaTiO3 particle in the cubic phase was also imaged using Bragg coherent diffraction imaging. 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J. Appl. Phys</addtitle><description>The shapes and sizes of grains influence the anisotropy of crystal structures and the configuration of ferroelectric domains. In order to better understand these effects, we introduce a method to observe a ferroelectric phase transition in a single ferroelectric particle of sub-micrometer size. The phase transition was observed by cooling the sample through its Curie temperature, and studying the pattern variations of Bragg coherent X-ray diffraction from a single particle of 500 nm sized BaTiO3. A change from a single 200 peak (cubic phase) to both 200 and 002 peaks (tetragonal phase); was seen, with fringes connecting them like a bridge. The pattern from the BaTiO3 particle in the cubic phase was also imaged using Bragg coherent diffraction imaging. The apparent strain distribution caused by dislocation internal to the BaTiO3 crystal was visible in the reconstructed image.</description><subject>Anisotropy</subject><subject>Barium titanates</subject><subject>Coherence</subject><subject>coherent X-ray diffraction</subject><subject>Crystal dislocations</subject><subject>Crystal structure</subject><subject>crystalline fine particle</subject><subject>Curie temperature</subject><subject>Diffraction patterns</subject><subject>Ferroelectric domains</subject><subject>Ferroelectric materials</subject><subject>ferroelectric phase transition</subject><subject>Ferroelectricity</subject><subject>Image reconstruction</subject><subject>imaging</subject><subject>Phase transitions</subject><subject>Strain distribution</subject><subject>X-ray diffraction</subject><issn>0021-4922</issn><issn>1347-4065</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNptkDtPwzAQxy0EEqXwAdgsMTGE2vErHgHxkio6UCQ265LY1KEkwXGH8ulxKIIF6XTP391Jf4ROKblgouDFjDKuMk6kmEGlas330OS3tY8mhOQ04zrPD9HRMDSplILTCYrLlcXOhtDZta1i8BXuVzBYHAO0g4--a7FvMWBBCG7f8eA_bZ18-7q2uIcQfZWSzuErWPoFG9eqt0SUW1x1KxtsG_FLFmCLa-9cGo4Xj9GBg_VgT37iFD3f3iyv77P54u7h-nKeeSZ5zCQtSlCgBUitBK2cKkuZE6pByFo4Ll3JuS4tU1IVRGmSCMUsLYA4VztgU3S2u9uH7mNjh2iabhPa9NLkUjNKBCvyRGU7ynf9H0CJ-RbWjCqaUUWzEzbx5__wTQO9kdQ8PSajhBSmrx37AkJfeds</recordid><startdate>20221101</startdate><enddate>20221101</enddate><creator>Oshime, Norihiro</creator><creator>Ohwada, Kenji</creator><creator>Machida, Akihiko</creator><creator>Fukushima, Nagise</creator><creator>Ueno, Shintaro</creator><creator>Fujii, Ichiro</creator><creator>Wada, Satoshi</creator><creator>Sugawara, Kento</creator><creator>Shimada, Ayumu</creator><creator>Ueno, Tetsuro</creator><creator>Watanuki, Tetsu</creator><creator>Ishii, Kenji</creator><creator>Toyokawa, Hidenori</creator><creator>Momma, Koichi</creator><creator>Kim, Sangwook</creator><creator>Tsukada, Shinya</creator><creator>Kuroiwa, Yoshihiro</creator><general>IOP Publishing</general><general>Japanese Journal of Applied Physics</general><scope>7U5</scope><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope><orcidid>https://orcid.org/0000-0001-5963-513X</orcidid><orcidid>https://orcid.org/0000-0002-1762-1642</orcidid><orcidid>https://orcid.org/0000-0003-2134-1640</orcidid><orcidid>https://orcid.org/0000-0003-0207-6415</orcidid></search><sort><creationdate>20221101</creationdate><title>The ferroelectric phase transition in a 500 nm sized single particle of BaTiO3 tracked by coherent X-ray diffraction</title><author>Oshime, Norihiro ; 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subjects | Anisotropy Barium titanates Coherence coherent X-ray diffraction Crystal dislocations Crystal structure crystalline fine particle Curie temperature Diffraction patterns Ferroelectric domains Ferroelectric materials ferroelectric phase transition Ferroelectricity Image reconstruction imaging Phase transitions Strain distribution X-ray diffraction |
title | The ferroelectric phase transition in a 500 nm sized single particle of BaTiO3 tracked by coherent X-ray diffraction |
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