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Low-Temperature Synthesis of Barium Titanate in a Mesoporous Polyethylene Matrix
— A nanocomposite based on high-density polyethylene with 13–15 wt % of barium titanate was obtained by the low-temperature synthesis of the inorganic component directly in the mesopores of an oriented polymer matrix using the sol-gel method followed by hydrothermal treatment in an alkaline medium....
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| Published in: | Inorganic materials : applied research 2022-10, Vol.13 (5), p.1391-1397 |
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| Main Authors: | , , , |
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| Language: | English |
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| container_end_page | 1397 |
| container_issue | 5 |
| container_start_page | 1391 |
| container_title | Inorganic materials : applied research |
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| creator | Trofimchuk, E. S. Moskvina, M. A. Shevchenko, V. G. Nikonorova, N. I. |
| description | —
A nanocomposite based on high-density polyethylene with 13–15 wt % of barium titanate was obtained by the low-temperature synthesis of the inorganic component directly in the mesopores of an oriented polymer matrix using the sol-gel method followed by hydrothermal treatment in an alkaline medium. Crystallization of barium titanate in nanopores was detected by X-ray powder diffraction and electron microscopy to occur mainly in a cubic crystalline modification with an average crystallite size of 16 nm, where crystallites form chain structures. The dielectric properties of the polymer nanocomposite and barium titanate synthesized under similar conditions were comparatively assessed. |
| doi_str_mv | 10.1134/S2075113322050422 |
| format | article |
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A nanocomposite based on high-density polyethylene with 13–15 wt % of barium titanate was obtained by the low-temperature synthesis of the inorganic component directly in the mesopores of an oriented polymer matrix using the sol-gel method followed by hydrothermal treatment in an alkaline medium. Crystallization of barium titanate in nanopores was detected by X-ray powder diffraction and electron microscopy to occur mainly in a cubic crystalline modification with an average crystallite size of 16 nm, where crystallites form chain structures. The dielectric properties of the polymer nanocomposite and barium titanate synthesized under similar conditions were comparatively assessed.</description><identifier>ISSN: 2075-1133</identifier><identifier>EISSN: 2075-115X</identifier><identifier>DOI: 10.1134/S2075113322050422</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Barium titanates ; Chemistry ; Chemistry and Materials Science ; Crystallites ; Crystallization ; Dielectric properties ; High density polyethylenes ; Hydrothermal treatment ; Industrial Chemistry/Chemical Engineering ; Inorganic Chemistry ; Low temperature ; Materials Science ; Nanocomposites ; New Technologies for Obtaining and Processing Materials ; Polymers ; Sol-gel processes ; X ray powder diffraction</subject><ispartof>Inorganic materials : applied research, 2022-10, Vol.13 (5), p.1391-1397</ispartof><rights>Pleiades Publishing, Ltd. 2022. ISSN 2075-1133, Inorganic Materials: Applied Research, 2022, Vol. 13, No. 5, pp. 1391–1397. © Pleiades Publishing, Ltd., 2022. Russian Text © The Author(s), 2022, published in Perspektivnye Materialy, 2022, No. 3, pp. 78–86.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c198t-4d80e60e30995299b54aaa2f25a19e30d764a96ef7d77af3487867f8a024e5883</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Trofimchuk, E. S.</creatorcontrib><creatorcontrib>Moskvina, M. A.</creatorcontrib><creatorcontrib>Shevchenko, V. G.</creatorcontrib><creatorcontrib>Nikonorova, N. I.</creatorcontrib><title>Low-Temperature Synthesis of Barium Titanate in a Mesoporous Polyethylene Matrix</title><title>Inorganic materials : applied research</title><addtitle>Inorg. Mater. Appl. Res</addtitle><description>—
A nanocomposite based on high-density polyethylene with 13–15 wt % of barium titanate was obtained by the low-temperature synthesis of the inorganic component directly in the mesopores of an oriented polymer matrix using the sol-gel method followed by hydrothermal treatment in an alkaline medium. Crystallization of barium titanate in nanopores was detected by X-ray powder diffraction and electron microscopy to occur mainly in a cubic crystalline modification with an average crystallite size of 16 nm, where crystallites form chain structures. The dielectric properties of the polymer nanocomposite and barium titanate synthesized under similar conditions were comparatively assessed.</description><subject>Barium titanates</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Crystallites</subject><subject>Crystallization</subject><subject>Dielectric properties</subject><subject>High density polyethylenes</subject><subject>Hydrothermal treatment</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Inorganic Chemistry</subject><subject>Low temperature</subject><subject>Materials Science</subject><subject>Nanocomposites</subject><subject>New Technologies for Obtaining and Processing Materials</subject><subject>Polymers</subject><subject>Sol-gel processes</subject><subject>X ray powder diffraction</subject><issn>2075-1133</issn><issn>2075-115X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp1UMtKAzEUDaJgqf0AdwHXo3lOkqUWX9BioRXcDdf2jp3STsYkg87fO6WiC_Fu7uFwHnAIOefsknOpruaCGd0jKQTTTAlxRAZ7KuNcvxz_YClPySjGDetPc-2UHpDZxH9kC9w1GCC1Aem8q9MaYxWpL-kNhKrd0UWVoIaEtKop0ClG3_jg20hnftthWndbrJFOIYXq84yclLCNOPr-Q_J8d7sYP2STp_vH8fUkW3JnU6ZWlmHOUDLntHDuVSsAEKXQwF3PrkyuwOVYmpUxUEpljc1NaYEJhdpaOSQXh9wm-PcWYyo2vg11X1kIw52R3DrWq_hBtQw-xoBl0YRqB6ErOCv22xV_tus94uCJvbZ-w_Cb_L_pC2U4bys</recordid><startdate>20221001</startdate><enddate>20221001</enddate><creator>Trofimchuk, E. S.</creator><creator>Moskvina, M. A.</creator><creator>Shevchenko, V. G.</creator><creator>Nikonorova, N. I.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20221001</creationdate><title>Low-Temperature Synthesis of Barium Titanate in a Mesoporous Polyethylene Matrix</title><author>Trofimchuk, E. S. ; Moskvina, M. A. ; Shevchenko, V. G. ; Nikonorova, N. I.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c198t-4d80e60e30995299b54aaa2f25a19e30d764a96ef7d77af3487867f8a024e5883</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Barium titanates</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Crystallites</topic><topic>Crystallization</topic><topic>Dielectric properties</topic><topic>High density polyethylenes</topic><topic>Hydrothermal treatment</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>Inorganic Chemistry</topic><topic>Low temperature</topic><topic>Materials Science</topic><topic>Nanocomposites</topic><topic>New Technologies for Obtaining and Processing Materials</topic><topic>Polymers</topic><topic>Sol-gel processes</topic><topic>X ray powder diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Trofimchuk, E. S.</creatorcontrib><creatorcontrib>Moskvina, M. A.</creatorcontrib><creatorcontrib>Shevchenko, V. G.</creatorcontrib><creatorcontrib>Nikonorova, N. I.</creatorcontrib><collection>CrossRef</collection><jtitle>Inorganic materials : applied research</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Trofimchuk, E. S.</au><au>Moskvina, M. A.</au><au>Shevchenko, V. G.</au><au>Nikonorova, N. I.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Low-Temperature Synthesis of Barium Titanate in a Mesoporous Polyethylene Matrix</atitle><jtitle>Inorganic materials : applied research</jtitle><stitle>Inorg. Mater. Appl. Res</stitle><date>2022-10-01</date><risdate>2022</risdate><volume>13</volume><issue>5</issue><spage>1391</spage><epage>1397</epage><pages>1391-1397</pages><issn>2075-1133</issn><eissn>2075-115X</eissn><abstract>—
A nanocomposite based on high-density polyethylene with 13–15 wt % of barium titanate was obtained by the low-temperature synthesis of the inorganic component directly in the mesopores of an oriented polymer matrix using the sol-gel method followed by hydrothermal treatment in an alkaline medium. Crystallization of barium titanate in nanopores was detected by X-ray powder diffraction and electron microscopy to occur mainly in a cubic crystalline modification with an average crystallite size of 16 nm, where crystallites form chain structures. The dielectric properties of the polymer nanocomposite and barium titanate synthesized under similar conditions were comparatively assessed.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S2075113322050422</doi><tpages>7</tpages></addata></record> |
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| identifier | ISSN: 2075-1133 |
| ispartof | Inorganic materials : applied research, 2022-10, Vol.13 (5), p.1391-1397 |
| issn | 2075-1133 2075-115X |
| language | eng |
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| subjects | Barium titanates Chemistry Chemistry and Materials Science Crystallites Crystallization Dielectric properties High density polyethylenes Hydrothermal treatment Industrial Chemistry/Chemical Engineering Inorganic Chemistry Low temperature Materials Science Nanocomposites New Technologies for Obtaining and Processing Materials Polymers Sol-gel processes X ray powder diffraction |
| title | Low-Temperature Synthesis of Barium Titanate in a Mesoporous Polyethylene Matrix |
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