N‐Iodosuccinimide (NIS) Promoted Synthesis of Unsymmetrical Disulfides Starting from Isothiocyanates Under Transition‐Metal‐Free Conditions

Under transition‐metal‐free conditions, a series of unsymmetrical disulfides could be quickly and conveniently obtained by NIS (N‐Iodosuccinimide)‐promotion in one pot manner. This method features mild conditions, easy operation, short reaction time and wide substrate scopes. It's noteworthy th...

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Bibliographic Details
Published in:European journal of organic chemistry 2022-10, Vol.2022 (37), p.n/a
Main Authors: Yang, Cheng‐Li, Xiao, Hua‐Qing, Dong, Zhi‐Bing
Format: Article
Language:English
Subjects:
Disulfides
N-Iodosuccinimide (NIS)
One-pot
Reaction time
Substrates
Synthesis
Transition-metal-free
Unsymmetrical disulfides
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Summary:Under transition‐metal‐free conditions, a series of unsymmetrical disulfides could be quickly and conveniently obtained by NIS (N‐Iodosuccinimide)‐promotion in one pot manner. This method features mild conditions, easy operation, short reaction time and wide substrate scopes. It's noteworthy that the desired products could be obtained in moderate to good yields from inexpensive and easily available starting materials, providing an alternative way to afford various unsymmetrical disulfides. Under transition‐metal‐free conditions, a series of unsymmetrical disulfides could be quickly and conveniently obtained by NIS (N‐Iodosuccinimide)‐promotion in one pot manner. It's noteworthy that the desired products could be obtained in moderate to good yields from inexpensive and easily available starting materials, providing an alternative way to afford various unsymmetrical disulfides.
ISSN:1434-193X
1099-0690
DOI:10.1002/ejoc.202200954