Modification of ultrasonic transducers to study crack propagation in vinyl polymers, supported by SEM technique

• Published in: Journal of vinyl & additive technology 2023-01, Vol.29 (1), p.84-99
• Main Authors: Barakat, Mirham A. Y., El‐Wakil, Abd El‐Aziz A., Hasan, Ebtisam H.
• Format: Article
• Language: English
• Subjects: Annealing; Beams (radiation); cone; crack; Crack propagation; Cracks; crosshead speed; Defects; Diameters; Flaw detection; MDPE; Plates; PMMA; Polyethylenes; Propagation (polymerization); Scanning electron microscopy; SEM; Stress intensity factors; Transducers; ultrasonic; Ultrasonic attenuation; Ultrasonic testing; Ultrasonic transducers; Vinyl polymers; Wave reflection
• ISSN: 1083-5601; 1548-0585
• DOI: 10.1002/vnl.21945

Detecting defects in various industrial products remains a challenging task in the industry. Researchers are constantly working to improve detection techniques and tools for various defects, particularly cracks. Many industrial structures suffer from cracks. The selection of a suitable technique and/or tool is based upon the tested structures and the accuracy of the technique and/or tool. The work's novelty is the development of a fully accurate, simple, and safe ultrasonic tool for precisely scanning cracks. A pen‐shaped cone was added to the ultrasonic transducers to improve their performance. Different crosshead speeds and annealing techniques were used to cause cracks on medium density polyethylene (MDPE) and poly‐methyl‐methacrylate (PMMA) polymer plates with specific dimensions. Cone reduced the front diameter of the transducers from 12 to 2 mm (cone tip diameter). It improved the transducers by giving them new properties such as a small near field, a collimated beam, high sensitivity, and high wave reflection. The modified transducers tracked the cracks at discrete sequential sites, where the ultrasonic velocity was measured to determine the crack speed, critical crack speed, dynamic stress intensity factor, and crack branching phenomenon. Additionally, ultrasonic attenuation was measured in order to accurately determine crack growth behavior, the crack's neck zone, and the crack growth dependency on both plate thickness and annealing. Scanning electron microscope (SEM) images revealed crack propagation in polymer plates. The results of ultrasonic testing and SEM evaluations were consistent. This guaranteed that the modified transducers could scan cracks accurately. Crack speed (a*) versus crack path in both PMMA and MDPE plates that subjected to different crosshead speeds.