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The impact of different surfactants on the structure, surface area, and electrochemical properties of hydrothermally synthesized spinel NiCo2O4 nanoparticles
NiCo 2 O 4 Nanoparticles have been synthesized by a facile hydrothermal method followed by annealing at a temperature decided based on differential thermal (DTA). Different additives and surfactants were used in preparation under the same synthesis conditions and their effects on the physical proper...
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| Published in: | Journal of materials science. Materials in electronics 2023-03, Vol.34 (7), p.584, Article 584 |
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| Main Authors: | , , , , |
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| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c293t-4f9a5b6619f392bb300ae64fe9f5d477fdb133514254defae7a33e6c4c6887b23 |
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| cites | cdi_FETCH-LOGICAL-c293t-4f9a5b6619f392bb300ae64fe9f5d477fdb133514254defae7a33e6c4c6887b23 |
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| container_issue | 7 |
| container_start_page | 584 |
| container_title | Journal of materials science. Materials in electronics |
| container_volume | 34 |
| creator | Abu El-Fadl, A. Mohammed, Mohaned M. M. Mansour, Heba R. Nashaat, A. M. Abbady, Gh |
| description | NiCo
2
O
4
Nanoparticles have been synthesized by a facile hydrothermal method followed by annealing at a temperature decided based on differential thermal (DTA). Different additives and surfactants were used in preparation under the same synthesis conditions and their effects on the physical properties of spinel nickel cobaltite nanoparticles have been investigated in a fair comparison study. The synthesis products have been characterized by using DTA and TGA measurements, X-ray diffraction, scanning electron microscopy, transmission electron microscopy, and Fourier transform infrared spectroscopy. Modification on the synthesis of the spinel nanoparticles provided high specific capacitance of 2253 F g
−1
at 1 A g
−1
and long-term cyclic stability for 10,000 cycles with 90% capacitance retention. |
| doi_str_mv | 10.1007/s10854-023-09890-x |
| format | article |
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2
O
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Nanoparticles have been synthesized by a facile hydrothermal method followed by annealing at a temperature decided based on differential thermal (DTA). Different additives and surfactants were used in preparation under the same synthesis conditions and their effects on the physical properties of spinel nickel cobaltite nanoparticles have been investigated in a fair comparison study. The synthesis products have been characterized by using DTA and TGA measurements, X-ray diffraction, scanning electron microscopy, transmission electron microscopy, and Fourier transform infrared spectroscopy. Modification on the synthesis of the spinel nanoparticles provided high specific capacitance of 2253 F g
−1
at 1 A g
−1
and long-term cyclic stability for 10,000 cycles with 90% capacitance retention.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-023-09890-x</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Additives ; Capacitance ; Carbon ; Characterization and Evaluation of Materials ; Chemical synthesis ; Chemistry and Materials Science ; Differential thermal analysis ; Electrochemical analysis ; Electrodes ; Electrolytes ; Electron microscopy ; Energy storage ; Fluorides ; Fourier transforms ; Graphene ; Investigations ; Materials Science ; Nanoparticles ; Nickel compounds ; Optical and Electronic Materials ; Physical properties ; Polyethylene glycol ; Scanning electron microscopy ; Spectrum analysis ; Spinel ; Surfactants</subject><ispartof>Journal of materials science. Materials in electronics, 2023-03, Vol.34 (7), p.584, Article 584</ispartof><rights>The Author(s) 2023</rights><rights>The Author(s) 2023. This work is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c293t-4f9a5b6619f392bb300ae64fe9f5d477fdb133514254defae7a33e6c4c6887b23</citedby><cites>FETCH-LOGICAL-c293t-4f9a5b6619f392bb300ae64fe9f5d477fdb133514254defae7a33e6c4c6887b23</cites><orcidid>0000-0003-2413-5965</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Abu El-Fadl, A.</creatorcontrib><creatorcontrib>Mohammed, Mohaned M. M.</creatorcontrib><creatorcontrib>Mansour, Heba R.</creatorcontrib><creatorcontrib>Nashaat, A. M.</creatorcontrib><creatorcontrib>Abbady, Gh</creatorcontrib><title>The impact of different surfactants on the structure, surface area, and electrochemical properties of hydrothermally synthesized spinel NiCo2O4 nanoparticles</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>NiCo
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O
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Nanoparticles have been synthesized by a facile hydrothermal method followed by annealing at a temperature decided based on differential thermal (DTA). Different additives and surfactants were used in preparation under the same synthesis conditions and their effects on the physical properties of spinel nickel cobaltite nanoparticles have been investigated in a fair comparison study. The synthesis products have been characterized by using DTA and TGA measurements, X-ray diffraction, scanning electron microscopy, transmission electron microscopy, and Fourier transform infrared spectroscopy. Modification on the synthesis of the spinel nanoparticles provided high specific capacitance of 2253 F g
−1
at 1 A g
−1
and long-term cyclic stability for 10,000 cycles with 90% capacitance retention.</description><subject>Additives</subject><subject>Capacitance</subject><subject>Carbon</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical synthesis</subject><subject>Chemistry and Materials Science</subject><subject>Differential thermal analysis</subject><subject>Electrochemical analysis</subject><subject>Electrodes</subject><subject>Electrolytes</subject><subject>Electron microscopy</subject><subject>Energy storage</subject><subject>Fluorides</subject><subject>Fourier transforms</subject><subject>Graphene</subject><subject>Investigations</subject><subject>Materials Science</subject><subject>Nanoparticles</subject><subject>Nickel compounds</subject><subject>Optical and Electronic Materials</subject><subject>Physical properties</subject><subject>Polyethylene glycol</subject><subject>Scanning electron microscopy</subject><subject>Spectrum analysis</subject><subject>Spinel</subject><subject>Surfactants</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp9kc9KAzEQxoMoWKsv4CngtavZJLvZPUrxHxR7qeAtZLMTu2WbrEkWrO_iu5pawZunYWa-7zcDH0KXObnOCRE3ISdVwTNCWUbqqibZxxGa5IVgGa_o6zGakLoQGS8oPUVnIWwIISVn1QR9rdaAu-2gdMTO4LYzBjzYiMPoTRoqGwN2FsckC9GPOo4eZr9bwMqDmmFlWww96OidXsO206rHg3cD-NhB2HPXu9a7xPBb1fc7HHY2NaH7hBaHobPQ4-du7uiSY6usG1Qy6h7COToxqg9w8Vun6OX-bjV_zBbLh6f57SLTtGYx46ZWRVOWeW1YTZuGEaKg5AZqU7RcCNM2OWNFzmnBWzAKhGIMSs11WVWioWyKrg7c9PX7CCHKjRu9TSclFaJKCMHKpKIHlfYuBA9GDr7bKr-TOZH7GOQhBplikD8xyI9kYgdTSGL7Bv4P_Y_rGzqbj-I</recordid><startdate>20230301</startdate><enddate>20230301</enddate><creator>Abu El-Fadl, A.</creator><creator>Mohammed, Mohaned M. 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M. ; Mansour, Heba R. ; Nashaat, A. 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Nanoparticles have been synthesized by a facile hydrothermal method followed by annealing at a temperature decided based on differential thermal (DTA). Different additives and surfactants were used in preparation under the same synthesis conditions and their effects on the physical properties of spinel nickel cobaltite nanoparticles have been investigated in a fair comparison study. The synthesis products have been characterized by using DTA and TGA measurements, X-ray diffraction, scanning electron microscopy, transmission electron microscopy, and Fourier transform infrared spectroscopy. Modification on the synthesis of the spinel nanoparticles provided high specific capacitance of 2253 F g
−1
at 1 A g
−1
and long-term cyclic stability for 10,000 cycles with 90% capacitance retention.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-023-09890-x</doi><orcidid>https://orcid.org/0000-0003-2413-5965</orcidid><oa>free_for_read</oa></addata></record> |
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| ispartof | Journal of materials science. Materials in electronics, 2023-03, Vol.34 (7), p.584, Article 584 |
| issn | 0957-4522 1573-482X |
| language | eng |
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| subjects | Additives Capacitance Carbon Characterization and Evaluation of Materials Chemical synthesis Chemistry and Materials Science Differential thermal analysis Electrochemical analysis Electrodes Electrolytes Electron microscopy Energy storage Fluorides Fourier transforms Graphene Investigations Materials Science Nanoparticles Nickel compounds Optical and Electronic Materials Physical properties Polyethylene glycol Scanning electron microscopy Spectrum analysis Spinel Surfactants |
| title | The impact of different surfactants on the structure, surface area, and electrochemical properties of hydrothermally synthesized spinel NiCo2O4 nanoparticles |
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