GermanIum array for non-destructive testing (GIANT) setup for muon-induced x-ray emission (MIXE) at the Paul Scherrer Institute

• Published in: Review of scientific instruments 2023-04, Vol.94 (4)
• Main Authors: Gerchow, Lars, Biswas, Sayani, Janka, Gianluca, Vigo, Carlos, Knecht, Andreas, Vogiatzi, Stergiani Marina, Ritjoho, Narongrit, Prokscha, Thomas, Luetkens, Hubertus, Amato, Alex
• Format: Article
• Language: English
• Subjects: Archaeology; Arrays; Charged particles; Decision making; Emission analysis; Energy resolution; Gamma rays; Germanium; Isotope ratios; Lithium-ion batteries; Muons; Nondestructive testing; Nuclear capture; Particle beams; Photopeak; Rechargeable batteries; Scientific apparatus & instruments; X-rays
• ISSN: 0034-6748; 1089-7623
• DOI: 10.1063/5.0136178

The usage of muonic x-rays to study elemental properties like nuclear radii ranges back to the seventies. This triggered the pioneering work at the Paul Scherrer Institute (PSI), during the eighties on the Muon-induced x-ray emission (MIXE) technique for a non-destructive assessment of elemental compositions. In recent years, this method has seen a rebirth, improvement, and adoption at most muon facilities around the world. Hereby, the PSI offers unique capabilities with its high-rate continuous muon beam at the Swiss Muon Source (SμS). We report here the decision-making, construction, and commissioning of a dedicated MIXE spectrometer at PSI, the GermanIum Array for Non-destructive Testing (GIANT) setup. Multiple campaigns highlighted the outstanding capabilities of MIXE at PSI, e.g., resolving down to 1 at. % elemental concentrations with as little as 1 h data taking, measuring isotopic ratios for elements from iron to lead, and characterizing gamma rays induced by muon nuclear capture. On-target beam spots were characterized with a dedicated charged particle tracker to be symmetric to 5% with an average σ = 22.80(25) and 14.41(8) mm for 25 and 45 MeV/c, respectively. Advanced analysis of the high-purity germanium signals further allows us to improve energy and timing resolutions to ∼1 keV and 20 ns at 1 MeV, respectively. Within the GIANT setup, an average detector has a photopeak efficiency of ϵĒ=0.11% and an energy resolution of σĒ=0.8keV at E = 1000 keV. The overall performance of the GIANT setup at SμS allowed us to start a rich user program with archaeological samples, Li-ion battery research, and collaboration with the industry. Future improvements will include a simulation-based analysis and a higher degree of automation, e.g., automatic scans of a series of muon momenta and automatic sample changing.