Characterization Studies on New Cellulosic Fiber Extracted from Leucaena Leucocephala Tree

• Published in: Journal of natural fibers 2023-04, Vol.20 (1)
• Main Authors: Gopinath, R., Billigraham, P., Sathishkumar, T.P.
• Format: Article
• Language: English
• Subjects: Calorimetry; Cellulose; Cellulose fibers; chemical properties; Climate change; crystallinity index; Differential scanning calorimetry; Fibers; Field emission microscopy; Field emission spectroscopy; Fourier transforms; Global warming; Greenhouse effect; Greenhouse gases; Infrared spectroscopy; Leucaena leucocephala; Leucaena leucocephala fiber; Mechanical properties; Modulus of elasticity; Polymers; Scanning electron microscopy; Spectrum analysis; Surface properties; Synthetic fibers; Tensile strength; Thermal stability; Thermogravimetric analysis; X-ray diffraction; X-ray spectroscopy; 化学性质; 机械性能; 热稳定性; 纤维素; 结晶度指数; 银合欢纤维
• ISSN: 1544-0478; 1544-046X
• DOI: 10.1080/15440478.2022.2157922

The present world faces critical issues such as global warming, sea-level rise, and drastic change in the climate pattern due to the emission of greenhouse gases. Large-scale use and disposal of hazardous plastics contribute significantly to the present scenario and it becomes essential to use naturally derived materials for making plastics. Natural fibers were found to possess the inherent characteristics required for reinforcing the polymer. In this work, one such novel cellulosic fiber derived from the bast of Leucaena leucocephala was identified and characterized using tests such as chemical, tensile, X-ray diffraction, Fourier transform infrared spectroscopy, Thermogravimetric, Differential scanning calorimetry, Energy-dispersive X-ray spectroscopy, and Field emission scanning electron microscopy. The presence of high cellulose (59.03 wt.%) with high crystallinity index (63.10%) contributes to high tensile strength(415-693 MPa) and high tensile modulus (9.90-13.10 GPa) of the Leucaena leucocephala fiber (LLF). From thermogravimetric analysis, LLF was observed to be thermally stable up to 188.20°C and activation energy of 64.22 kJ/mol. The morphological analysis of LLF revealed the existence of honeycombed porous surface characterized with serrations, and this facilitates better bonding characteristics with polymer. Lower density, mechanical properties, and better thermal stability make LLF a suitable alternate for synthetic fibers while making composites.