Synthesis of Substituted Cyclohexenones by Reaction of Chalcones with Acetoacetic Acid Amides

New 4-aryl-2-oxo-6-phenyl-3-cyclohexene-1-carboxamides were obtained by the reaction of N -substituted acetoacetic acid amides with benzalacetophenone and 4-methoxybenzalacetophenone in alcohol in the presence of potassium hydroxide. Structure of the prepared compounds was proved using IR, 1 H and 1...

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Bibliographic Details
Published in:Russian journal of general chemistry 2023-11, Vol.93 (11), p.2742-2748
Main Authors: Nosova, N. V., Sokolov, A. A., Gein, V. L., Dmitriev, M. V., Mokrushin, I. G.
Format: Article
Language:English
Subjects:
Amides
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Hydroxides
Mass spectrometry
NMR spectroscopy
Nuclear magnetic resonance spectroscopy
Potassium hydroxides
Substitutes
Tetracycline
Tetracyclines
X ray analysis
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Summary:New 4-aryl-2-oxo-6-phenyl-3-cyclohexene-1-carboxamides were obtained by the reaction of N -substituted acetoacetic acid amides with benzalacetophenone and 4-methoxybenzalacetophenone in alcohol in the presence of potassium hydroxide. Structure of the prepared compounds was proved using IR, 1 H and 13 C NMR spectroscopy, mass spectrometry and X-ray analysis data.
ISSN:1070-3632
1608-3350
DOI:10.1134/S1070363223110026