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Reductive Ullmann-Type Homocoupling of Aryl Halides Catalysed by Mixed Metal Oxide Nanocomposite (Pd/MnFe2O4) Under Aqueous Condition
A highly efficient magnetic nanocomposite, Pd/MnFe 2 O 4 has been prepared by citrate gel auto combustion and deposition precipitation method for reductive Ullmann homocoupling of aryl halides in an aqueous medium. The physical and chemical properties of the synthesized composite were characterized...
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| Published in: | Catalysis letters 2024-03, Vol.154 (3), p.1209-1218 |
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| Main Authors: | , , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c319t-e198ad30c6295214de7599cbda0002f36c27dfa4048ac4487e709e55cafcb6db3 |
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| cites | cdi_FETCH-LOGICAL-c319t-e198ad30c6295214de7599cbda0002f36c27dfa4048ac4487e709e55cafcb6db3 |
| container_end_page | 1218 |
| container_issue | 3 |
| container_start_page | 1209 |
| container_title | Catalysis letters |
| container_volume | 154 |
| creator | Sutar, Damodar J. Zende, Sunil N. Mhaldar, Pradeep M. Pore, Dattaprasad M. Tapase, Asmita S. Gokavi, Gavisiddappa S. |
| description | A highly efficient magnetic nanocomposite, Pd/MnFe
2
O
4
has been prepared by citrate gel auto combustion and deposition precipitation method for reductive Ullmann homocoupling of aryl halides in an aqueous medium. The physical and chemical properties of the synthesized composite were characterized by XRD, TEM, SEM, EDAX, VSM, and BET analysis. The synthesis of symmetrical biaryls has been achieved at admirable reaction conditions with high yield in a short reaction time. The nanocomposite catalyst could be easily separated by magnetic separation and recycled up to six reaction cycles with appreciable yields of desired products. The synthesized nanocomposite was found to be a best alternative catalyst for carbon–carbon bond formation in Ullmann-type homocoupling.
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| doi_str_mv | 10.1007/s10562-023-04378-z |
| format | article |
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2
O
4
has been prepared by citrate gel auto combustion and deposition precipitation method for reductive Ullmann homocoupling of aryl halides in an aqueous medium. The physical and chemical properties of the synthesized composite were characterized by XRD, TEM, SEM, EDAX, VSM, and BET analysis. The synthesis of symmetrical biaryls has been achieved at admirable reaction conditions with high yield in a short reaction time. The nanocomposite catalyst could be easily separated by magnetic separation and recycled up to six reaction cycles with appreciable yields of desired products. The synthesized nanocomposite was found to be a best alternative catalyst for carbon–carbon bond formation in Ullmann-type homocoupling.
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2
O
4
has been prepared by citrate gel auto combustion and deposition precipitation method for reductive Ullmann homocoupling of aryl halides in an aqueous medium. The physical and chemical properties of the synthesized composite were characterized by XRD, TEM, SEM, EDAX, VSM, and BET analysis. The synthesis of symmetrical biaryls has been achieved at admirable reaction conditions with high yield in a short reaction time. The nanocomposite catalyst could be easily separated by magnetic separation and recycled up to six reaction cycles with appreciable yields of desired products. The synthesized nanocomposite was found to be a best alternative catalyst for carbon–carbon bond formation in Ullmann-type homocoupling.
Graphical abstract</description><subject>Aqueous solutions</subject><subject>Aromatic compounds</subject><subject>Carbon</subject><subject>Catalysis</subject><subject>Catalysts</subject><subject>Chemical properties</subject><subject>Chemical synthesis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Halides</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Magnetic separation</subject><subject>Metal oxides</subject><subject>Nanocomposites</subject><subject>Nanoparticles</subject><subject>Nitrates</subject><subject>Organometallic Chemistry</subject><subject>Palladium</subject><subject>Physical Chemistry</subject><issn>1011-372X</issn><issn>1572-879X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNp9UE1LxDAQLaLg5x_wFPCih2g-2qY5Lou6guuKuOAtZJOpVLpJTVqx3v3fRlfw5mkeM--9mXlZdkzJOSVEXERKipJhwjgmORcV_tjK9mghGK6EfNpOmFCKuWBPu9l-jC-EECmo3Ms-H8AOpm_eAC3bdq2dw49jB2jm1974oWsb94x8jSZhbNFMt42FiKa61-0YwaLViObNewJzSC20eE9zdKdd0q47H5se0Om9vZi7K2CL_AwtnYWAJq8D-CH5eGebvvHuMNupdRvh6LceZMury8fpDN8urm-mk1tsOJU9BiorbTkxJZMFo7kFUUhpVlanf1jNS8OErXVO8kqbPK8ECCKhKIyuzaq0K36QnWx8u-DTDbFXL34ILq1UTDJOS8opSSy2YZngYwxQqy40ax1GRYn6jltt4lYpbvUTt_pIIr4RxUR2zxD-rP9RfQFhaIRt</recordid><startdate>20240301</startdate><enddate>20240301</enddate><creator>Sutar, Damodar J.</creator><creator>Zende, Sunil N.</creator><creator>Mhaldar, Pradeep M.</creator><creator>Pore, Dattaprasad M.</creator><creator>Tapase, Asmita S.</creator><creator>Gokavi, Gavisiddappa S.</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20240301</creationdate><title>Reductive Ullmann-Type Homocoupling of Aryl Halides Catalysed by Mixed Metal Oxide Nanocomposite (Pd/MnFe2O4) Under Aqueous Condition</title><author>Sutar, Damodar J. ; Zende, Sunil N. ; Mhaldar, Pradeep M. ; Pore, Dattaprasad M. ; Tapase, Asmita S. ; Gokavi, Gavisiddappa S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-e198ad30c6295214de7599cbda0002f36c27dfa4048ac4487e709e55cafcb6db3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Aqueous solutions</topic><topic>Aromatic compounds</topic><topic>Carbon</topic><topic>Catalysis</topic><topic>Catalysts</topic><topic>Chemical properties</topic><topic>Chemical synthesis</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Halides</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>Magnetic separation</topic><topic>Metal oxides</topic><topic>Nanocomposites</topic><topic>Nanoparticles</topic><topic>Nitrates</topic><topic>Organometallic Chemistry</topic><topic>Palladium</topic><topic>Physical Chemistry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sutar, Damodar J.</creatorcontrib><creatorcontrib>Zende, Sunil N.</creatorcontrib><creatorcontrib>Mhaldar, Pradeep M.</creatorcontrib><creatorcontrib>Pore, Dattaprasad M.</creatorcontrib><creatorcontrib>Tapase, Asmita S.</creatorcontrib><creatorcontrib>Gokavi, Gavisiddappa S.</creatorcontrib><collection>CrossRef</collection><jtitle>Catalysis letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sutar, Damodar J.</au><au>Zende, Sunil N.</au><au>Mhaldar, Pradeep M.</au><au>Pore, Dattaprasad M.</au><au>Tapase, Asmita S.</au><au>Gokavi, Gavisiddappa S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Reductive Ullmann-Type Homocoupling of Aryl Halides Catalysed by Mixed Metal Oxide Nanocomposite (Pd/MnFe2O4) Under Aqueous Condition</atitle><jtitle>Catalysis letters</jtitle><stitle>Catal Lett</stitle><date>2024-03-01</date><risdate>2024</risdate><volume>154</volume><issue>3</issue><spage>1209</spage><epage>1218</epage><pages>1209-1218</pages><issn>1011-372X</issn><eissn>1572-879X</eissn><abstract>A highly efficient magnetic nanocomposite, Pd/MnFe
2
O
4
has been prepared by citrate gel auto combustion and deposition precipitation method for reductive Ullmann homocoupling of aryl halides in an aqueous medium. The physical and chemical properties of the synthesized composite were characterized by XRD, TEM, SEM, EDAX, VSM, and BET analysis. The synthesis of symmetrical biaryls has been achieved at admirable reaction conditions with high yield in a short reaction time. The nanocomposite catalyst could be easily separated by magnetic separation and recycled up to six reaction cycles with appreciable yields of desired products. The synthesized nanocomposite was found to be a best alternative catalyst for carbon–carbon bond formation in Ullmann-type homocoupling.
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| ispartof | Catalysis letters, 2024-03, Vol.154 (3), p.1209-1218 |
| issn | 1011-372X 1572-879X |
| language | eng |
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| source | Springer Nature |
| subjects | Aqueous solutions Aromatic compounds Carbon Catalysis Catalysts Chemical properties Chemical synthesis Chemistry Chemistry and Materials Science Halides Industrial Chemistry/Chemical Engineering Magnetic separation Metal oxides Nanocomposites Nanoparticles Nitrates Organometallic Chemistry Palladium Physical Chemistry |
| title | Reductive Ullmann-Type Homocoupling of Aryl Halides Catalysed by Mixed Metal Oxide Nanocomposite (Pd/MnFe2O4) Under Aqueous Condition |
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