Three-component reaction between phenanthridine, acetylenic ketones and bis(polyfluoroalkyl) H-phosphonates: synthesis of E-N-acylethenyl-6-bis(polyfluoroalkyl)phosphoryl-5,6-dihydrophenanthridines

A solvent-free three-component reaction between phenanthridine, acetylenic ketones, and bis(polyfluoroalkyl) H -phosphonates proceeded at room temperature for 20–24 h to stereoselectively give the corresponding E - N -acylethenyl-6-bis(polyfluoroalkyl)phosphoryl-5,6-dihydrophenanthridines in up to 8...

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Bibliographic Details
Published in:Russian chemical bulletin 2024, Vol.73 (1), p.221-226
Main Authors: Volkov, P. A., Khrapova, K. O., Telezhkin, A. A., Albanov, A. I., Trofimov, B. A.
Format: Article
Language:English
Subjects:
Brief Communications
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Inorganic Chemistry
Ketones
Organic Chemistry
Phosphonates
Room temperature
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Summary:A solvent-free three-component reaction between phenanthridine, acetylenic ketones, and bis(polyfluoroalkyl) H -phosphonates proceeded at room temperature for 20–24 h to stereoselectively give the corresponding E - N -acylethenyl-6-bis(polyfluoroalkyl)phosphoryl-5,6-dihydrophenanthridines in up to 82% yield.
ISSN:1066-5285
1573-9171
DOI:10.1007/s11172-024-4134-9