A Simple Approach to the Synthesis of 5-Aroyl-2-imino-2,3-dihydrothiazoles

A simple approach was proposed to the synthesis 5-benzoyl-2-imino-4-thiazolines by the reaction of α-thiocynatoacetophenone with various aryl amines and triethyl orthoformate. Structure of the prepared compounds was confirmed by IR spectrophotometry and NMR spectroscopy, including two-dimensional HM...

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Bibliographic Details
Published in:Russian journal of general chemistry 2024-02, Vol.94 (2), p.292-296
Main Authors: Kindop, V. K., Bespalov, A. V., Dotsenko, V. V., Kindop, Vl. K., Volnyanskaya, Ya. M., Aksenov, N. A., Aksenova, I. V.
Format: Article
Language:English
Subjects:
Amines
Aromatic amines
Chemical synthesis
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
NMR spectroscopy
Nuclear magnetic resonance spectroscopy
Spectrophotometry
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Summary:A simple approach was proposed to the synthesis 5-benzoyl-2-imino-4-thiazolines by the reaction of α-thiocynatoacetophenone with various aryl amines and triethyl orthoformate. Structure of the prepared compounds was confirmed by IR spectrophotometry and NMR spectroscopy, including two-dimensional HMBC and HSQC experiments.
ISSN:1070-3632
1608-3350
DOI:10.1134/S107036322402004X