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Magnetic attapulgite synthesized via Sonochemistry: an innovative strategy for efficient solid phase extraction of As3+ from simulated and unrefined crude oil samples
Magnetised attapulgite (ATP-Fe 3 O 4 ) adsorbent was synthesised using a sonochemistry approach for the solid phase extraction of As 3+ from stimulated and unrefined crude oil samples. The average size of the Fe 3 O 4 nanoparticles estimated from the Transmission Electron Microscopy (TEM) image was...
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Published in: | Journal of porous materials 2024-08, Vol.31 (4), p.1183-1195 |
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container_title | Journal of porous materials |
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creator | Ali, Ehab M. Iqbal, Anwar Ibrahim, Mohamad Nasir Mohamad Alheety, Mustafa A. Ahmed, Naser M. Yanto, Dede Heri Yuli Zainul, Rahadian |
description | Magnetised attapulgite (ATP-Fe
3
O
4
) adsorbent was synthesised using a sonochemistry approach for the solid phase extraction of As
3+
from stimulated and unrefined crude oil samples. The average size of the Fe
3
O
4
nanoparticles estimated from the Transmission Electron Microscopy (TEM) image was 10 nm. The TEM analysis also showed that Fe
3
O
4
nanoparticles agglomerated in the ATP’s tube and on its surface. The X-ray diffraction analysis (XRD) indicates that the crystallinity of the ATP reduced after the magnetisation process. The saturation magnetisation of the ATP-Fe
3
O
4
was determined to be only 2.8 emu g
-1
. Under the optimum conditions (pH = 7, adsorbent dosage = 0.6 g, contact time = 90 min and sample volume = 50 mL), the As
3+
removal was more than 98% for both types of oil. The limits of detection (LOD) and relative standard deviations (RSD%) were 2.88 ng mL
-1
and 0.3423%, respectively. The adsorption process follows the pseudo-first-order kinetic model (R
2
= 0.9696) and adheres to the Langmuir isotherm model (R
2
= 0.9925). The reusability study showed that ATP-Fe
3
O
4
is highly stable and can be reused five times with almost 100% removal efficiency. This research outcome aligns with the United Nations Sustainable Goal 7, Affordable and Clean Energy. |
doi_str_mv | 10.1007/s10934-024-01581-0 |
format | article |
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3
O
4
) adsorbent was synthesised using a sonochemistry approach for the solid phase extraction of As
3+
from stimulated and unrefined crude oil samples. The average size of the Fe
3
O
4
nanoparticles estimated from the Transmission Electron Microscopy (TEM) image was 10 nm. The TEM analysis also showed that Fe
3
O
4
nanoparticles agglomerated in the ATP’s tube and on its surface. The X-ray diffraction analysis (XRD) indicates that the crystallinity of the ATP reduced after the magnetisation process. The saturation magnetisation of the ATP-Fe
3
O
4
was determined to be only 2.8 emu g
-1
. Under the optimum conditions (pH = 7, adsorbent dosage = 0.6 g, contact time = 90 min and sample volume = 50 mL), the As
3+
removal was more than 98% for both types of oil. The limits of detection (LOD) and relative standard deviations (RSD%) were 2.88 ng mL
-1
and 0.3423%, respectively. The adsorption process follows the pseudo-first-order kinetic model (R
2
= 0.9696) and adheres to the Langmuir isotherm model (R
2
= 0.9925). The reusability study showed that ATP-Fe
3
O
4
is highly stable and can be reused five times with almost 100% removal efficiency. This research outcome aligns with the United Nations Sustainable Goal 7, Affordable and Clean Energy.</description><identifier>ISSN: 1380-2224</identifier><identifier>EISSN: 1573-4854</identifier><identifier>DOI: 10.1007/s10934-024-01581-0</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Adsorbents ; Arsenic ions ; Catalysis ; Characterization and Evaluation of Materials ; Chemistry ; Chemistry and Materials Science ; Clean energy ; Crude oil ; Electrons ; Iron oxides ; Magnetization ; Nanoparticles ; Physical Chemistry ; Solid phases ; Transmission electron microscopy</subject><ispartof>Journal of porous materials, 2024-08, Vol.31 (4), p.1183-1195</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c200t-74277901b44216b760ecc507c83b07006f278d1f66f74a3bba3dbc737af37b2b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Ali, Ehab M.</creatorcontrib><creatorcontrib>Iqbal, Anwar</creatorcontrib><creatorcontrib>Ibrahim, Mohamad Nasir Mohamad</creatorcontrib><creatorcontrib>Alheety, Mustafa A.</creatorcontrib><creatorcontrib>Ahmed, Naser M.</creatorcontrib><creatorcontrib>Yanto, Dede Heri Yuli</creatorcontrib><creatorcontrib>Zainul, Rahadian</creatorcontrib><title>Magnetic attapulgite synthesized via Sonochemistry: an innovative strategy for efficient solid phase extraction of As3+ from simulated and unrefined crude oil samples</title><title>Journal of porous materials</title><addtitle>J Porous Mater</addtitle><description>Magnetised attapulgite (ATP-Fe
3
O
4
) adsorbent was synthesised using a sonochemistry approach for the solid phase extraction of As
3+
from stimulated and unrefined crude oil samples. The average size of the Fe
3
O
4
nanoparticles estimated from the Transmission Electron Microscopy (TEM) image was 10 nm. The TEM analysis also showed that Fe
3
O
4
nanoparticles agglomerated in the ATP’s tube and on its surface. The X-ray diffraction analysis (XRD) indicates that the crystallinity of the ATP reduced after the magnetisation process. The saturation magnetisation of the ATP-Fe
3
O
4
was determined to be only 2.8 emu g
-1
. Under the optimum conditions (pH = 7, adsorbent dosage = 0.6 g, contact time = 90 min and sample volume = 50 mL), the As
3+
removal was more than 98% for both types of oil. The limits of detection (LOD) and relative standard deviations (RSD%) were 2.88 ng mL
-1
and 0.3423%, respectively. The adsorption process follows the pseudo-first-order kinetic model (R
2
= 0.9696) and adheres to the Langmuir isotherm model (R
2
= 0.9925). The reusability study showed that ATP-Fe
3
O
4
is highly stable and can be reused five times with almost 100% removal efficiency. This research outcome aligns with the United Nations Sustainable Goal 7, Affordable and Clean Energy.</description><subject>Adsorbents</subject><subject>Arsenic ions</subject><subject>Catalysis</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Clean energy</subject><subject>Crude oil</subject><subject>Electrons</subject><subject>Iron oxides</subject><subject>Magnetization</subject><subject>Nanoparticles</subject><subject>Physical Chemistry</subject><subject>Solid phases</subject><subject>Transmission electron microscopy</subject><issn>1380-2224</issn><issn>1573-4854</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNp9kc9u1DAQxiNEJUrhBTiNxBGFju1s7OVWVfyTijgUzpbj2LuuEjt4nBXbB-I567KVuHEYzYz0-74Z6WuaNwzfM0R5SQy3omuR12IbxVp81pyzjRRtpzbd8zoLhS3nvHvRvCS6Q8StkvK8-fPN7KIrwYIpxSzrtAvFAR1j2TsK926EQzBwm2KyezcHKvn4AUyEEGM6mBIOFS7ZFLc7gk8ZnPfBBhcLUJrCCMvekAP3uzK2hBQhebgi8Q58TjNQmNepisdqOcIas_Mh1s3mdXSQwgRk5mVy9Ko582Yi9_qpXzQ_P338cf2lvfn--ev11U1rOWJpZcel3CIbuo6zfpA9Oms3KK0SA0rE3nOpRub73svOiGEwYhysFNJ4IQc-iIvm7cl3yenX6qjou7TmWE9qgYpz1aseK8VPlM2JqD6tlxxmk4-aoX7MQ5_y0DUP_TcP_SgSJxFVOO5c_mf9H9UD7T-RXw</recordid><startdate>20240801</startdate><enddate>20240801</enddate><creator>Ali, Ehab M.</creator><creator>Iqbal, Anwar</creator><creator>Ibrahim, Mohamad Nasir Mohamad</creator><creator>Alheety, Mustafa A.</creator><creator>Ahmed, Naser M.</creator><creator>Yanto, Dede Heri Yuli</creator><creator>Zainul, Rahadian</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20240801</creationdate><title>Magnetic attapulgite synthesized via Sonochemistry: an innovative strategy for efficient solid phase extraction of As3+ from simulated and unrefined crude oil samples</title><author>Ali, Ehab M. ; Iqbal, Anwar ; Ibrahim, Mohamad Nasir Mohamad ; Alheety, Mustafa A. ; Ahmed, Naser M. ; Yanto, Dede Heri Yuli ; Zainul, Rahadian</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c200t-74277901b44216b760ecc507c83b07006f278d1f66f74a3bba3dbc737af37b2b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Adsorbents</topic><topic>Arsenic ions</topic><topic>Catalysis</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Clean energy</topic><topic>Crude oil</topic><topic>Electrons</topic><topic>Iron oxides</topic><topic>Magnetization</topic><topic>Nanoparticles</topic><topic>Physical Chemistry</topic><topic>Solid phases</topic><topic>Transmission electron microscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ali, Ehab M.</creatorcontrib><creatorcontrib>Iqbal, Anwar</creatorcontrib><creatorcontrib>Ibrahim, Mohamad Nasir Mohamad</creatorcontrib><creatorcontrib>Alheety, Mustafa A.</creatorcontrib><creatorcontrib>Ahmed, Naser M.</creatorcontrib><creatorcontrib>Yanto, Dede Heri Yuli</creatorcontrib><creatorcontrib>Zainul, Rahadian</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of porous materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ali, Ehab M.</au><au>Iqbal, Anwar</au><au>Ibrahim, Mohamad Nasir Mohamad</au><au>Alheety, Mustafa A.</au><au>Ahmed, Naser M.</au><au>Yanto, Dede Heri Yuli</au><au>Zainul, Rahadian</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Magnetic attapulgite synthesized via Sonochemistry: an innovative strategy for efficient solid phase extraction of As3+ from simulated and unrefined crude oil samples</atitle><jtitle>Journal of porous materials</jtitle><stitle>J Porous Mater</stitle><date>2024-08-01</date><risdate>2024</risdate><volume>31</volume><issue>4</issue><spage>1183</spage><epage>1195</epage><pages>1183-1195</pages><issn>1380-2224</issn><eissn>1573-4854</eissn><abstract>Magnetised attapulgite (ATP-Fe
3
O
4
) adsorbent was synthesised using a sonochemistry approach for the solid phase extraction of As
3+
from stimulated and unrefined crude oil samples. The average size of the Fe
3
O
4
nanoparticles estimated from the Transmission Electron Microscopy (TEM) image was 10 nm. The TEM analysis also showed that Fe
3
O
4
nanoparticles agglomerated in the ATP’s tube and on its surface. The X-ray diffraction analysis (XRD) indicates that the crystallinity of the ATP reduced after the magnetisation process. The saturation magnetisation of the ATP-Fe
3
O
4
was determined to be only 2.8 emu g
-1
. Under the optimum conditions (pH = 7, adsorbent dosage = 0.6 g, contact time = 90 min and sample volume = 50 mL), the As
3+
removal was more than 98% for both types of oil. The limits of detection (LOD) and relative standard deviations (RSD%) were 2.88 ng mL
-1
and 0.3423%, respectively. The adsorption process follows the pseudo-first-order kinetic model (R
2
= 0.9696) and adheres to the Langmuir isotherm model (R
2
= 0.9925). The reusability study showed that ATP-Fe
3
O
4
is highly stable and can be reused five times with almost 100% removal efficiency. This research outcome aligns with the United Nations Sustainable Goal 7, Affordable and Clean Energy.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10934-024-01581-0</doi><tpages>13</tpages></addata></record> |
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subjects | Adsorbents Arsenic ions Catalysis Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Clean energy Crude oil Electrons Iron oxides Magnetization Nanoparticles Physical Chemistry Solid phases Transmission electron microscopy |
title | Magnetic attapulgite synthesized via Sonochemistry: an innovative strategy for efficient solid phase extraction of As3+ from simulated and unrefined crude oil samples |
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