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Magnetic attapulgite synthesized via Sonochemistry: an innovative strategy for efficient solid phase extraction of As3+ from simulated and unrefined crude oil samples

Magnetised attapulgite (ATP-Fe 3 O 4 ) adsorbent was synthesised using a sonochemistry approach for the solid phase extraction of As 3+ from stimulated and unrefined crude oil samples. The average size of the Fe 3 O 4 nanoparticles estimated from the Transmission Electron Microscopy (TEM) image was...

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Published in:Journal of porous materials 2024-08, Vol.31 (4), p.1183-1195
Main Authors: Ali, Ehab M., Iqbal, Anwar, Ibrahim, Mohamad Nasir Mohamad, Alheety, Mustafa A., Ahmed, Naser M., Yanto, Dede Heri Yuli, Zainul, Rahadian
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creator Ali, Ehab M.
Iqbal, Anwar
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Yanto, Dede Heri Yuli
Zainul, Rahadian
description Magnetised attapulgite (ATP-Fe 3 O 4 ) adsorbent was synthesised using a sonochemistry approach for the solid phase extraction of As 3+ from stimulated and unrefined crude oil samples. The average size of the Fe 3 O 4 nanoparticles estimated from the Transmission Electron Microscopy (TEM) image was 10 nm. The TEM analysis also showed that Fe 3 O 4 nanoparticles agglomerated in the ATP’s tube and on its surface. The X-ray diffraction analysis (XRD) indicates that the crystallinity of the ATP reduced after the magnetisation process. The saturation magnetisation of the ATP-Fe 3 O 4 was determined to be only 2.8 emu g -1 . Under the optimum conditions (pH = 7, adsorbent dosage = 0.6 g, contact time = 90 min and sample volume = 50 mL), the As 3+ removal was more than 98% for both types of oil. The limits of detection (LOD) and relative standard deviations (RSD%) were 2.88 ng mL -1 and 0.3423%, respectively. The adsorption process follows the pseudo-first-order kinetic model (R 2  = 0.9696) and adheres to the Langmuir isotherm model (R 2  = 0.9925). The reusability study showed that ATP-Fe 3 O 4 is highly stable and can be reused five times with almost 100% removal efficiency. This research outcome aligns with the United Nations Sustainable Goal 7, Affordable and Clean Energy.
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subjects Adsorbents
Arsenic ions
Catalysis
Characterization and Evaluation of Materials
Chemistry
Chemistry and Materials Science
Clean energy
Crude oil
Electrons
Iron oxides
Magnetization
Nanoparticles
Physical Chemistry
Solid phases
Transmission electron microscopy
title Magnetic attapulgite synthesized via Sonochemistry: an innovative strategy for efficient solid phase extraction of As3+ from simulated and unrefined crude oil samples
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