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Nano-indentation testing of new and fractured nickel-titanium endodontic instruments

Jamleh A, Sadr A, Nomura N, Yahata Y, Ebihara A, Hanawa T, Tagami J, Suda H. Nano‐indentation testing of new and fractured nickel‐titanium endodontic instruments. International Endodontic Journal, 45, 462–468, 2012. Aim  To investigate the effect of cyclic fatigue on nickel‐titanium (NiTi) endodonti...

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Published in:International endodontic journal 2012-05, Vol.45 (5), p.462-468
Main Authors: Jamleh, A., Sadr, A., Nomura, N., Yahata, Y., Ebihara, A., Hanawa, T., Tagami, J., Suda, H.
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container_title International endodontic journal
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description Jamleh A, Sadr A, Nomura N, Yahata Y, Ebihara A, Hanawa T, Tagami J, Suda H. Nano‐indentation testing of new and fractured nickel‐titanium endodontic instruments. International Endodontic Journal, 45, 462–468, 2012. Aim  To investigate the effect of cyclic fatigue on nickel‐titanium (NiTi) endodontic instruments using a nano‐indentation test. Methodology  Eight ProFile NiTi rotary instruments (size 30, taper 0.06; Dentsply Maillefer, Ballaigues, Switzerland) were tested using a cyclic fatigue set‐up until fracture. The fractured instruments and eight new NiTi instruments of the same size and taper were used for a nano‐indentation test on the internal surfaces of a NiTi instruments in the region just adjacent to their fractured edge (group I) and in the same region of the new group (group II), and the cutting part beside the shaft for both instruments [group III (fractured) and group IV (new)]. Data were statistically analyzed using one‐way analysis of variance and Games–Howell post hoc test. The alpha‐type error was set at 0.05. Results  Significant differences in terms of hardness and elastic modulus for each group (P 
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Nano‐indentation testing of new and fractured nickel‐titanium endodontic instruments. International Endodontic Journal, 45, 462–468, 2012. Aim  To investigate the effect of cyclic fatigue on nickel‐titanium (NiTi) endodontic instruments using a nano‐indentation test. Methodology  Eight ProFile NiTi rotary instruments (size 30, taper 0.06; Dentsply Maillefer, Ballaigues, Switzerland) were tested using a cyclic fatigue set‐up until fracture. The fractured instruments and eight new NiTi instruments of the same size and taper were used for a nano‐indentation test on the internal surfaces of a NiTi instruments in the region just adjacent to their fractured edge (group I) and in the same region of the new group (group II), and the cutting part beside the shaft for both instruments [group III (fractured) and group IV (new)]. Data were statistically analyzed using one‐way analysis of variance and Games–Howell post hoc test. The alpha‐type error was set at 0.05. Results  Significant differences in terms of hardness and elastic modulus for each group (P &lt; 0.05) were found, with group I having the lowest mean values followed by group III. Additionally, standard deviations increased remarkably after failure, as represented by groups I and III. Conclusion  The nano‐indentation technique can be applied to determine the performance and the failure mechanism of NiTi instruments. The fatigue process revealed a significant decrease in the hardness and elastic modulus of the NiTi instrument. As indicated by the low hardness, the fatigue process did not result in work hardening but rather work softening.</description><identifier>ISSN: 0143-2885</identifier><identifier>EISSN: 1365-2591</identifier><identifier>DOI: 10.1111/j.1365-2591.2011.01997.x</identifier><identifier>PMID: 22211861</identifier><language>eng</language><publisher>Oxford, UK: Blackwell Publishing Ltd</publisher><subject>cyclic fatigue ; Dental Alloys - chemistry ; Dental Stress Analysis - instrumentation ; Dentistry ; Elastic Modulus ; Equipment Design ; Equipment Failure ; Hardness ; Humans ; Materials Testing ; nano-indentation ; Nanotechnology ; Nickel - chemistry ; nickel-titanium instruments ; Root Canal Preparation - instrumentation ; Rotation ; Stress, Mechanical ; Surface Properties ; Time Factors ; Titanium - chemistry</subject><ispartof>International endodontic journal, 2012-05, Vol.45 (5), p.462-468</ispartof><rights>2011 International Endodontic Journal</rights><rights>2011 International Endodontic Journal.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4737-5a2654f7686fc25e07491d06669ababe1e2998b9c82124f4931c1a0408f59fa53</citedby><cites>FETCH-LOGICAL-c4737-5a2654f7686fc25e07491d06669ababe1e2998b9c82124f4931c1a0408f59fa53</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/22211861$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Jamleh, A.</creatorcontrib><creatorcontrib>Sadr, A.</creatorcontrib><creatorcontrib>Nomura, N.</creatorcontrib><creatorcontrib>Yahata, Y.</creatorcontrib><creatorcontrib>Ebihara, A.</creatorcontrib><creatorcontrib>Hanawa, T.</creatorcontrib><creatorcontrib>Tagami, J.</creatorcontrib><creatorcontrib>Suda, H.</creatorcontrib><title>Nano-indentation testing of new and fractured nickel-titanium endodontic instruments</title><title>International endodontic journal</title><addtitle>Int Endod J</addtitle><description>Jamleh A, Sadr A, Nomura N, Yahata Y, Ebihara A, Hanawa T, Tagami J, Suda H. Nano‐indentation testing of new and fractured nickel‐titanium endodontic instruments. International Endodontic Journal, 45, 462–468, 2012. Aim  To investigate the effect of cyclic fatigue on nickel‐titanium (NiTi) endodontic instruments using a nano‐indentation test. Methodology  Eight ProFile NiTi rotary instruments (size 30, taper 0.06; Dentsply Maillefer, Ballaigues, Switzerland) were tested using a cyclic fatigue set‐up until fracture. The fractured instruments and eight new NiTi instruments of the same size and taper were used for a nano‐indentation test on the internal surfaces of a NiTi instruments in the region just adjacent to their fractured edge (group I) and in the same region of the new group (group II), and the cutting part beside the shaft for both instruments [group III (fractured) and group IV (new)]. Data were statistically analyzed using one‐way analysis of variance and Games–Howell post hoc test. The alpha‐type error was set at 0.05. Results  Significant differences in terms of hardness and elastic modulus for each group (P &lt; 0.05) were found, with group I having the lowest mean values followed by group III. Additionally, standard deviations increased remarkably after failure, as represented by groups I and III. Conclusion  The nano‐indentation technique can be applied to determine the performance and the failure mechanism of NiTi instruments. The fatigue process revealed a significant decrease in the hardness and elastic modulus of the NiTi instrument. As indicated by the low hardness, the fatigue process did not result in work hardening but rather work softening.</description><subject>cyclic fatigue</subject><subject>Dental Alloys - chemistry</subject><subject>Dental Stress Analysis - instrumentation</subject><subject>Dentistry</subject><subject>Elastic Modulus</subject><subject>Equipment Design</subject><subject>Equipment Failure</subject><subject>Hardness</subject><subject>Humans</subject><subject>Materials Testing</subject><subject>nano-indentation</subject><subject>Nanotechnology</subject><subject>Nickel - chemistry</subject><subject>nickel-titanium instruments</subject><subject>Root Canal Preparation - instrumentation</subject><subject>Rotation</subject><subject>Stress, Mechanical</subject><subject>Surface Properties</subject><subject>Time Factors</subject><subject>Titanium - chemistry</subject><issn>0143-2885</issn><issn>1365-2591</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqNkEFvFCEYhonR2LX6FwxHLzPyMQMDBw_adNtua73UeCQsA4btDFOBSbf_Xsatey6Xj-R73hfyIISB1FDO510NDWcVZRJqSgBqAlJ29f4VWh0Xr9GKQNtUVAh2gt6ltCOEMNLAW3RCKQUQHFbo7laHqfKhtyHr7KeAs03Zh994cjjYR6xDj13UJs_R9jh4c2-HKvusg59HbEM_9VPI3mAfUo7zWHrSe_TG6SHZD8_zFP1cn9-dXVY3Py6uzr7eVKbtmq5imnLWuo4L7gxllnSthJ5wzqXe6q0FS6UUW2kEBdq6VjZgQJOWCMek06w5RZ8OvQ9x-jOXf6vRJ2OHQQc7zUkBgUaCEEIWVBxQE6eUonXqIfpRx6cCqcWp2qlFnVrUqcWp-udU7Uv04_Mr83a0_TH4X2IBvhyARz_YpxcXq6vzzXIr-eqQ9ynb_TGv473ixRNTv24v1LfvG7q-hrXaNH8BxGqUXw</recordid><startdate>201205</startdate><enddate>201205</enddate><creator>Jamleh, A.</creator><creator>Sadr, A.</creator><creator>Nomura, N.</creator><creator>Yahata, Y.</creator><creator>Ebihara, A.</creator><creator>Hanawa, T.</creator><creator>Tagami, J.</creator><creator>Suda, H.</creator><general>Blackwell Publishing Ltd</general><scope>BSCLL</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>201205</creationdate><title>Nano-indentation testing of new and fractured nickel-titanium endodontic instruments</title><author>Jamleh, A. ; Sadr, A. ; Nomura, N. ; Yahata, Y. ; Ebihara, A. ; Hanawa, T. ; Tagami, J. ; Suda, H.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4737-5a2654f7686fc25e07491d06669ababe1e2998b9c82124f4931c1a0408f59fa53</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>cyclic fatigue</topic><topic>Dental Alloys - chemistry</topic><topic>Dental Stress Analysis - instrumentation</topic><topic>Dentistry</topic><topic>Elastic Modulus</topic><topic>Equipment Design</topic><topic>Equipment Failure</topic><topic>Hardness</topic><topic>Humans</topic><topic>Materials Testing</topic><topic>nano-indentation</topic><topic>Nanotechnology</topic><topic>Nickel - chemistry</topic><topic>nickel-titanium instruments</topic><topic>Root Canal Preparation - instrumentation</topic><topic>Rotation</topic><topic>Stress, Mechanical</topic><topic>Surface Properties</topic><topic>Time Factors</topic><topic>Titanium - chemistry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Jamleh, A.</creatorcontrib><creatorcontrib>Sadr, A.</creatorcontrib><creatorcontrib>Nomura, N.</creatorcontrib><creatorcontrib>Yahata, Y.</creatorcontrib><creatorcontrib>Ebihara, A.</creatorcontrib><creatorcontrib>Hanawa, T.</creatorcontrib><creatorcontrib>Tagami, J.</creatorcontrib><creatorcontrib>Suda, H.</creatorcontrib><collection>Istex</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>International endodontic journal</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Jamleh, A.</au><au>Sadr, A.</au><au>Nomura, N.</au><au>Yahata, Y.</au><au>Ebihara, A.</au><au>Hanawa, T.</au><au>Tagami, J.</au><au>Suda, H.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Nano-indentation testing of new and fractured nickel-titanium endodontic instruments</atitle><jtitle>International endodontic journal</jtitle><addtitle>Int Endod J</addtitle><date>2012-05</date><risdate>2012</risdate><volume>45</volume><issue>5</issue><spage>462</spage><epage>468</epage><pages>462-468</pages><issn>0143-2885</issn><eissn>1365-2591</eissn><abstract>Jamleh A, Sadr A, Nomura N, Yahata Y, Ebihara A, Hanawa T, Tagami J, Suda H. Nano‐indentation testing of new and fractured nickel‐titanium endodontic instruments. International Endodontic Journal, 45, 462–468, 2012. Aim  To investigate the effect of cyclic fatigue on nickel‐titanium (NiTi) endodontic instruments using a nano‐indentation test. Methodology  Eight ProFile NiTi rotary instruments (size 30, taper 0.06; Dentsply Maillefer, Ballaigues, Switzerland) were tested using a cyclic fatigue set‐up until fracture. The fractured instruments and eight new NiTi instruments of the same size and taper were used for a nano‐indentation test on the internal surfaces of a NiTi instruments in the region just adjacent to their fractured edge (group I) and in the same region of the new group (group II), and the cutting part beside the shaft for both instruments [group III (fractured) and group IV (new)]. Data were statistically analyzed using one‐way analysis of variance and Games–Howell post hoc test. The alpha‐type error was set at 0.05. Results  Significant differences in terms of hardness and elastic modulus for each group (P &lt; 0.05) were found, with group I having the lowest mean values followed by group III. Additionally, standard deviations increased remarkably after failure, as represented by groups I and III. Conclusion  The nano‐indentation technique can be applied to determine the performance and the failure mechanism of NiTi instruments. The fatigue process revealed a significant decrease in the hardness and elastic modulus of the NiTi instrument. As indicated by the low hardness, the fatigue process did not result in work hardening but rather work softening.</abstract><cop>Oxford, UK</cop><pub>Blackwell Publishing Ltd</pub><pmid>22211861</pmid><doi>10.1111/j.1365-2591.2011.01997.x</doi><tpages>7</tpages></addata></record>
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subjects cyclic fatigue
Dental Alloys - chemistry
Dental Stress Analysis - instrumentation
Dentistry
Elastic Modulus
Equipment Design
Equipment Failure
Hardness
Humans
Materials Testing
nano-indentation
Nanotechnology
Nickel - chemistry
nickel-titanium instruments
Root Canal Preparation - instrumentation
Rotation
Stress, Mechanical
Surface Properties
Time Factors
Titanium - chemistry
title Nano-indentation testing of new and fractured nickel-titanium endodontic instruments
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