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Diazotization-iodination of aromatic amines in water mediated by crosslinked poly(4-vinylpyridine) supported sodium nitrite

An Efficient and simple method for the diazotization of a wide range of aryl amines has been developed by using a polymer‐supported sodium nitrite. The diazotization of aryl amines occurred with crosslinked poly(4‐vinylpyridine)‐supported sodium nitrite, in the presence of concentrated H2SO4, at low...

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Published in:	Journal of applied polymer science 2011-09, Vol.121 (5), p.2621-2625
Main Authors:	Karimi Zarchi, Mohammad Ali, Ebrahimi, Nahid
Format:	Article
Language:	English
Subjects:	Amines Applied sciences Aromatic compounds aryl amine aryl iodide Crosslinking diazonium salt diazotization Exact sciences and technology Iodides Materials science Organic polymers Physicochemistry of polymers Polymers Properties and characterization Sodium nitrite Special properties (catalyst, reagent or carrier)
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description	An Efficient and simple method for the diazotization of a wide range of aryl amines has been developed by using a polymer‐supported sodium nitrite. The diazotization of aryl amines occurred with crosslinked poly(4‐vinylpyridine)‐supported sodium nitrite, in the presence of concentrated H2SO4, at low temperature (0–5°C). The obtained diazonium salt, followed by treatment with KI in water at room temperature or at 60°C to produce a various of aryl iodides. The spent polymeric reagent can be regenerated and reused for several times without losing its activity. © 2011 Wiley Periodicals, Inc. J Appl Polym Sci, 2011
doi_str_mv	10.1002/app.34004
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J Appl Polym Sci, 2011</description><subject>Amines</subject><subject>Applied sciences</subject><subject>Aromatic compounds</subject><subject>aryl amine</subject><subject>aryl iodide</subject><subject>Crosslinking</subject><subject>diazonium salt</subject><subject>diazotization</subject><subject>Exact sciences and technology</subject><subject>Iodides</subject><subject>Materials science</subject><subject>Organic polymers</subject><subject>Physicochemistry of polymers</subject><subject>Polymers</subject><subject>Properties and characterization</subject><subject>Sodium nitrite</subject><subject>Special properties (catalyst, reagent or carrier)</subject><issn>0021-8995</issn><issn>1097-4628</issn><issn>1097-4628</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNp1kcFu1DAQhi0EEkvhwBtYQkjtIa2d2I59rFq6VGphQa16tBzHkaZN7GAnlJSXx90tPSBx8ozmm09j_Qi9p-SQElIemXE8rBgh7AVaUaLqgolSvkSrPKOFVIq_Rm9SuiWEUk7ECv0-BfMQJngwEwRfQGjBb0scOmxiGHJjsRnAu4TB43szuYgH10IuWtws2MaQUg_-Lrdj6Jd9VvwEv_TjEiHL3AFO8ziG-IinrJ8H7GGKMLm36FVn-uTePb176Prs09XJ5-Li6_r85PiisJWSrCiN4bISpG5rwRpDW-U4lzIPu4ab1jROMCJKKhS3HePKKtdI2TFiJRWyddUe2t95xxh-zC5NeoBkXd8b78KcNCVlKeuaKJXRD_-gt2GOPl-nKc82WnHKMnWwo7Z_j67TY4TBxCWr9GMMOsegtzFk9uOT0SRr-i4abyE9L5SsVExwkbmjHXcPvVv-L9THm81fc7HbgDS5X88bJt5pUVc11zdf1nrzrRbry7Pv-qr6A2pwp0o</recordid><startdate>20110905</startdate><enddate>20110905</enddate><creator>Karimi Zarchi, Mohammad Ali</creator><creator>Ebrahimi, Nahid</creator><general>Wiley Subscription Services, Inc., A Wiley Company</general><general>Wiley</general><general>Wiley Subscription Services, Inc</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20110905</creationdate><title>Diazotization-iodination of aromatic amines in water mediated by crosslinked poly(4-vinylpyridine) supported sodium nitrite</title><author>Karimi Zarchi, Mohammad Ali ; Ebrahimi, Nahid</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3984-2aa583607d764ba1d9e5588c39fb5adabe640621695cf459c9eb88f40c8168de3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Amines</topic><topic>Applied sciences</topic><topic>Aromatic compounds</topic><topic>aryl amine</topic><topic>aryl iodide</topic><topic>Crosslinking</topic><topic>diazonium salt</topic><topic>diazotization</topic><topic>Exact sciences and technology</topic><topic>Iodides</topic><topic>Materials science</topic><topic>Organic polymers</topic><topic>Physicochemistry of polymers</topic><topic>Polymers</topic><topic>Properties and characterization</topic><topic>Sodium nitrite</topic><topic>Special properties (catalyst, reagent or carrier)</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Karimi Zarchi, Mohammad Ali</creatorcontrib><creatorcontrib>Ebrahimi, Nahid</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of applied polymer science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Karimi Zarchi, Mohammad Ali</au><au>Ebrahimi, Nahid</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Diazotization-iodination of aromatic amines in water mediated by crosslinked poly(4-vinylpyridine) supported sodium nitrite</atitle><jtitle>Journal of applied polymer science</jtitle><addtitle>J. Appl. Polym. Sci</addtitle><date>2011-09-05</date><risdate>2011</risdate><volume>121</volume><issue>5</issue><spage>2621</spage><epage>2625</epage><pages>2621-2625</pages><issn>0021-8995</issn><issn>1097-4628</issn><eissn>1097-4628</eissn><coden>JAPNAB</coden><abstract>An Efficient and simple method for the diazotization of a wide range of aryl amines has been developed by using a polymer‐supported sodium nitrite. The diazotization of aryl amines occurred with crosslinked poly(4‐vinylpyridine)‐supported sodium nitrite, in the presence of concentrated H2SO4, at low temperature (0–5°C). The obtained diazonium salt, followed by treatment with KI in water at room temperature or at 60°C to produce a various of aryl iodides. The spent polymeric reagent can be regenerated and reused for several times without losing its activity. © 2011 Wiley Periodicals, Inc. J Appl Polym Sci, 2011</abstract><cop>Hoboken</cop><pub>Wiley Subscription Services, Inc., A Wiley Company</pub><doi>10.1002/app.34004</doi><tpages>5</tpages></addata></record>
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subjects	Amines Applied sciences Aromatic compounds aryl amine aryl iodide Crosslinking diazonium salt diazotization Exact sciences and technology Iodides Materials science Organic polymers Physicochemistry of polymers Polymers Properties and characterization Sodium nitrite Special properties (catalyst, reagent or carrier)
title	Diazotization-iodination of aromatic amines in water mediated by crosslinked poly(4-vinylpyridine) supported sodium nitrite
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