Incipient flow properties of two-component fine powder systems and their relationships with bulk density and particle contacts

• Published in: Powder technology 2012-09, Vol.228, p.359-370
• Main Authors: Kojima, Takehiro, Elliott, James A.
• Format: Article
• Language: English
• Subjects: Applied sciences; Bulk density; Chemical engineering; Cohesion; Coordination number; Density; Devices; Estimating; Exact sciences and technology; Flowability; friction; glass; Glass ballotini; Incipient flow properties; Miscellaneous; mixing; Mixing ratios; powders; Shear; Shear testing; Solid-solid systems; Toners; Two-component fine powders
• ISSN: 0032-5910; 1873-328X
• DOI: 10.1016/j.powtec.2012.05.052

The effect of incipient flow properties, such as cohesion and internal angle of friction, on the flowability of two-component fine powder systems is of great importance for controlling the process efficiency and quality of industrial products such as developers for electrophotographic (EP) printing devices. In this paper, we have studied the flow properties of model fine powders composed of glass ballotini (d50=69.4μm) and resin toners (d50=6–8μm), using different mixing ratios of the components under a low normal consolidation stress (2kPa) using a ring shear tester (RST). We have found that the dependence of the cohesion of the two-component mixtures on the mixing ratio can be reproduced by a linear superposition of the cohesions of each component weighted by the number of the three different types of interparticle contacts, which suggests that the bulk cohesive properties of fine powder mixtures are dominated by cohesion between particles and the number of each type of particle contacts in the system. Also, the frictional properties of the two-component mixtures are strongly related to the packing density of the mixture, and its dependence on the mixing ratio can be related to the densities of each type of particle contacts. Our results suggest that the dependence of the incipient flow properties of two-component fine powders on the ratio of the components can be predicted by measuring only the flow properties of each component and estimating the ease with which the mixture can be compacted. The cohesive and frictional properties of two-component fine powder mixtures of glass ballotini and resin toners can be predicted as a function of toner volume ratio using the inter-particle cohesions and coordination numbers of each component and packing density of the mixtures. The highest flowabilities correspond to the smallest cohesions obtained around the critical surface coverage of ballotini by toners. [Display omitted] ► We studied the incipient flow properties of two-component fine powders. ► Cohesion of mixture is governed by the particle cohesions and coordination number. ► Frictional properties are strongly related to the packing density. ► Flowability index depends strongly on the cohesive property of the powder. ► Incipient flow properties are predictable from those of each component.