Instant MOFs: continuous synthesis of metal-organic frameworks by rapid solvent mixing

A continuous flow reactor allows the preparation of porous metal-organic framework materials with crystallisation induced by rapid mixing of streams of preheated water and solutions of reagents in organic solvent: this gives high volume production (132 g h(-1)) with crystallite size of the products...

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Bibliographic Details
Published in:Chemical communications (Cambridge, England) England), 2012-01, Vol.48 (86), p.10642-10644
Main Authors: Gimeno-Fabra, Miquel, Munn, Alexis S, Stevens, Lee A, Drage, Trevor C, Grant, David M, Kashtiban, Reza J, Sloan, Jeremy, Lester, Edward, Walton, Richard I
Format: Article
Language:English
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Summary:A continuous flow reactor allows the preparation of porous metal-organic framework materials with crystallisation induced by rapid mixing of streams of preheated water and solutions of reagents in organic solvent: this gives high volume production (132 g h(-1)) with crystallite size of the products from nanoscale to micron.
ISSN:1359-7345
1364-548X
DOI:10.1039/c2cc34493a