Charged colloidal model systems under confinement in slit geometry: a new setup for optical microscopic studies

A new experimental setup for optical microscopic studies of charged colloidal model systems under confinement between two flat walls is presented. The measurement cell consists of optically flat quartz substrates attached to piezo actuators. Those facilitate fast and flexible adjustment of the confi...

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Bibliographic Details
Published in:Review of scientific instruments 2013-06, Vol.84 (6), p.063907-063907
Main Authors: Reinmüller, A, Palberg, T, Schöpe, H J
Format: Article
Language:English
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Summary:A new experimental setup for optical microscopic studies of charged colloidal model systems under confinement between two flat walls is presented. The measurement cell consists of optically flat quartz substrates attached to piezo actuators. Those facilitate fast and flexible adjustment of the confining geometry. Optionally, the local cell height can be quantitatively controlled by in situ interferometric measurements. Proper choice of materials guarantees sufficient chemical inertia against contamination with salt ions. For efficient preparation of charged colloidal suspensions under strongly deionized conditions, the cell can be connected to a conventional pump circuit including a mixed bed ion exchanger column. The usefulness of this setup, in particular for investigating the equilibrium phase behavior of colloids at low background salt concentrations, is demonstrated recalling recent experiments.
ISSN:0034-6748
1089-7623
DOI:10.1063/1.4811719