Synthesis of γ-valerolactone using a continuous-flow reactor

This study describes the heterogeneous catalysed continuous synthesis of gamma -valerolactone (GVL) using a continuous-flow reactor, H-Cube registered and H-Cube Pro(TM), equipped with 5% Ru/C, 10% Pd/C and RANEY registered Ni CatCart registered . The highest yield of GVL was achieved by using 5% Ru...

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Bibliographic Details
Published in:RSC advances 2013-01, Vol.3 (37), p.16283-16287
Main Authors: Tukacs, József M., Jones, Richard V., Darvas, Ferenc, Dibó, Gábor, Lezsák, Gábor, Mika, László T.
Format: Article
Language:English
Subjects:
Ligands
Nickel
Palladium
Reactors
Synthesis
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Summary:This study describes the heterogeneous catalysed continuous synthesis of gamma -valerolactone (GVL) using a continuous-flow reactor, H-Cube registered and H-Cube Pro(TM), equipped with 5% Ru/C, 10% Pd/C and RANEY registered Ni CatCart registered . The highest yield of GVL was achieved by using 5% Ru/C in the presence of 0.015 mol L super(-1) Bu-P(C sub(6)H sub(4)-m-SO sub(3)Na) sub(2) ligand under 100 bar H sub(2) at 100 degree C.
ISSN:2046-2069
2046-2069
DOI:10.1039/c3ra43032d