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Influence of the microstructure on the deuterium retention in tungsten
The microstructure of tungsten samples is systematically modified by recrystallization to investigate the structure dependence of deuterium (D) retention. After a thorough characterization by scanning and transmission electron microscopy, non-recrystallized samples and samples recrystallized by diff...
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Published in: | Journal of nuclear materials 2011-08, Vol.415 (1), p.S632-S635 |
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container_end_page | S635 |
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container_start_page | S632 |
container_title | Journal of nuclear materials |
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creator | Manhard, A. Schmid, K. Balden, M. Jacob, W. |
description | The microstructure of tungsten samples is systematically modified by recrystallization to investigate the structure dependence of deuterium (D) retention. After a thorough characterization by scanning and transmission electron microscopy, non-recrystallized samples and samples recrystallized by different degrees are loaded with deuterium in a low-temperature plasma device. The deuterium inventory is measured by nuclear reaction analysis and thermal desorption spectroscopy. The post implantation surface morphology is investigated by scanning electron, optical and atomic force microscopy. The modification by recrystallization allows a wide variation in the crystallite size and has a strong impact on the measured D retention. Both the total amount and the binding state of the retained D are changed. |
doi_str_mv | 10.1016/j.jnucmat.2010.10.045 |
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After a thorough characterization by scanning and transmission electron microscopy, non-recrystallized samples and samples recrystallized by different degrees are loaded with deuterium in a low-temperature plasma device. The deuterium inventory is measured by nuclear reaction analysis and thermal desorption spectroscopy. The post implantation surface morphology is investigated by scanning electron, optical and atomic force microscopy. The modification by recrystallization allows a wide variation in the crystallite size and has a strong impact on the measured D retention. 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After a thorough characterization by scanning and transmission electron microscopy, non-recrystallized samples and samples recrystallized by different degrees are loaded with deuterium in a low-temperature plasma device. The deuterium inventory is measured by nuclear reaction analysis and thermal desorption spectroscopy. The post implantation surface morphology is investigated by scanning electron, optical and atomic force microscopy. The modification by recrystallization allows a wide variation in the crystallite size and has a strong impact on the measured D retention. Both the total amount and the binding state of the retained D are changed.</description><subject>Applied sciences</subject><subject>Controled nuclear fusion plants</subject><subject>Crystallites</subject><subject>Deuterium</subject><subject>Energy</subject><subject>Energy. Thermal use of fuels</subject><subject>Exact sciences and technology</subject><subject>Fission nuclear power plants</subject><subject>Fuels</subject><subject>Implantation</subject><subject>Installations for energy generation and conversion: thermal and electrical energy</subject><subject>Microstructure</subject><subject>Nuclear fuels</subject><subject>Nuclear reactions</subject><subject>Recrystallization</subject><subject>Scanning electron microscopy</subject><subject>Tungsten</subject><issn>0022-3115</issn><issn>1873-4820</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFkE1LxDAQhoMouK7-BKEXwUtrkiZN9iSyuCoseNFzaNOJpvRjzYfgvzfdXbx6GvLknZl3XoSuCS4IJtVdV3Rj1EMdCor3rMCMn6AFkaLMmaT4FC0wpjQvCeHn6ML7DmPMV5gv0OZlNH2EUUM2mSx8QjZY7SYfXNQhukTHPW0hBnA2DpmDAGOwidv0FccPn96X6MzUvYerY12i983j2_o5374-vawftrlmkoeccN5I0rAVFVQa0bQAIEveMMOS2WSei0oYaXDFRFvStixXUoJY1bwFASWUS3R7mLtz01cEH9RgvYa-r0eYoleEVYzLqhI0SflBOp_jHRi1c3ao3Y8iWM25qU4dc1NzbjNOuaW-m-OK2uu6N64etfV_zZQJWSW3SXd_0EG699uCU17bOcjWOtBBtZP9Z9Mv7U2GBw</recordid><startdate>20110801</startdate><enddate>20110801</enddate><creator>Manhard, A.</creator><creator>Schmid, K.</creator><creator>Balden, M.</creator><creator>Jacob, W.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7TB</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>FR3</scope><scope>H8D</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20110801</creationdate><title>Influence of the microstructure on the deuterium retention in tungsten</title><author>Manhard, A. ; Schmid, K. ; Balden, M. ; Jacob, W.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c485t-155b81b492728f7bdeee835b4f41870105767f8f0647d32d33988e79a5de7e3e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Applied sciences</topic><topic>Controled nuclear fusion plants</topic><topic>Crystallites</topic><topic>Deuterium</topic><topic>Energy</topic><topic>Energy. 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source | Elsevier ScienceDirect Freedom Collection 2023 |
subjects | Applied sciences Controled nuclear fusion plants Crystallites Deuterium Energy Energy. Thermal use of fuels Exact sciences and technology Fission nuclear power plants Fuels Implantation Installations for energy generation and conversion: thermal and electrical energy Microstructure Nuclear fuels Nuclear reactions Recrystallization Scanning electron microscopy Tungsten |
title | Influence of the microstructure on the deuterium retention in tungsten |
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