Thionation of carbonyl compounds using phosphorus pentasulfide and hexamethyldisiloxane under microwave irradiations

A novel and convenient microwave assisted thionation of carbonyl compounds using phosphorus pentasulfide and hexamethyldisiloxane is described. Thionation by this method gave the desired product in higher yield and shorter reaction time as compared to conventional methods.

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Bibliographic Details
Published in:Journal of chemical research 2004-07, Vol.2004 (7), p.474-476
Main Authors: Polshettiwar, Vivek, Nivsarkar, Manisha, Paradashani, Deepak, Kaushik, M P
Format: Article
Language:English
Subjects:
Carbonyl compounds
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Description
Summary:A novel and convenient microwave assisted thionation of carbonyl compounds using phosphorus pentasulfide and hexamethyldisiloxane is described. Thionation by this method gave the desired product in higher yield and shorter reaction time as compared to conventional methods.
ISSN:1747-5198
2047-6507
DOI:10.3184/0308234042037149