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One-minute synthesis of crystalline microporous aluminophosphate (AlPO4-5) by combining fast heating with a seed-assisted method

Herein, we report a rapid route for the synthesis of AlPO4-5. By combining fast heating in a tubular reactor with a seed-assisted method, both of which were found to be crucial, the preparation of AlPO4-5 was completed in one minute, making this route the fastest known for the preparation of the cry...

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Bibliographic Details
Published in:Chemical communications (Cambridge, England) England), 2014-03, Vol.50 (19), p.2526-2528
Main Authors: Liu, Zhendong, Wakihara, Toru, Nishioka, Daisuke, Oshima, Kazunori, Takewaki, Takahiko, Okubo, Tatsuya
Format: Article
Language:English
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Summary:Herein, we report a rapid route for the synthesis of AlPO4-5. By combining fast heating in a tubular reactor with a seed-assisted method, both of which were found to be crucial, the preparation of AlPO4-5 was completed in one minute, making this route the fastest known for the preparation of the crystalline microporous materials.
ISSN:1359-7345
1364-548X
DOI:10.1039/c3cc49548e