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Formation of omega and Ti sub(2)Ni phases in a residual Ti-Ni-Ti multilayer between stainless steel and zirconia after bonding at 1173 K

Stainless steel (316L) and 8 mol pct Y sub(2)O sub(3)-stabilized zirconia (8Y-ZrO sub(2)) were bonded using a Ti-Ni-Ti multilayer at 1173 K (900 degree C) for 1 h. Cross-sectional transmission electron microscopy specimens were prepared by an innovative focused ion beam plus lift-out technique. In a...

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Published in:Philosophical magazine letters 2014-10, Vol.94 (10), p.609-619
Main Authors: Wei, Shen-Hung, Lin, Chien-Cheng
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Language:English
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Lin, Chien-Cheng
description Stainless steel (316L) and 8 mol pct Y sub(2)O sub(3)-stabilized zirconia (8Y-ZrO sub(2)) were bonded using a Ti-Ni-Ti multilayer at 1173 K (900 degree C) for 1 h. Cross-sectional transmission electron microscopy specimens were prepared by an innovative focused ion beam plus lift-out technique. In addition to acicular alpha -Ti, the dissolution of Fe, Cr, and Ni diffusing outwards from 316L into beta -Ti led to the precipitation of the omega ( omega ) phase with different variants in the residual Ti foil between 316L and Ni. The omega -phase was not found in the residual Ti foil between Ni and 8Y-ZrO sub(2), while Ti sub(2)Ni precipitates were precipitated in some alpha -Ti grains owing to the exclusion of Ni from the beta -Ti.
doi_str_mv 10.1080/09500839.2014.951705
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source Taylor and Francis Science and Technology Collection
subjects Austenitic stainless steels
Foils
Heat resistant steels
Multilayers
Nickel
Precipitation
Stainless steels
Titanium
Zirconium dioxide
title Formation of omega and Ti sub(2)Ni phases in a residual Ti-Ni-Ti multilayer between stainless steel and zirconia after bonding at 1173 K
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