The influence of the laser scan strategy on grain structure and cracking behaviour in SLM powder-bed fabricated nickel superalloy

• Published in: Journal of alloys and compounds 2014-12, Vol.615, p.338-347
• Main Authors: Carter, Luke N., Martin, Christopher, Withers, Philip J., Attallah, Moataz M.
• Format: Article
• Language: English
• Subjects: Cross-disciplinary physics: materials science; rheology; Electron back scatter diffraction; Exact sciences and technology; Grain structure; Heating; High-temperature alloys; Islands; Laser processing; Lasers; Materials science; Metallography; Microstructure; Nickel base alloys; Phase diagrams and microstructures developed by solidification and solid-solid phase transformations; Physics; Powder metallurgy; Scanning electron microscopy, SEM; Solidification; Strategy
• ISSN: 0925-8388; 1873-4669
• DOI: 10.1016/j.jallcom.2014.06.172

•Laser scanning strategies in Selectively Laser Melted (SLM) of CM247LC were studied.•A bi-modal grain structure has been identified due to the island scan strategy.•EBSD and MicroCT were used to show the influence of the scan strategy.•The island strategy affects the crystrallographic orientation and crack formation.•A possible explanation for this structure is presented based on the microstructural evidence. During the development of a processing route for the Selective Laser Melting (SLM) powder-bed fabrication of the nickel superalloy CM247LC it has been observed that the ‘island’ scan-strategy used as standard by the Concept Laser M2 SLM powder-bed system strongly influences the grain structure of the material. Optical and SEM micrographs are presented to show the observed grain structure in the SLM fabricated and Hot Isostatically Pressed (HIPped) material. The repeating pattern shown in the grain structure has been linked to the overlapping of the ‘island’ pattern used as standard in the Concept Laser M2 powder-bed facility. It is suggested that the formation of this bi-modal grain structure can be linked to the heat transfer away from the solidifying melt pool. The concept of a ‘band’ heating effect across each ‘island’ rather than ‘moving point’ heating has been suggested and has been supported by Electron Back Scattered Diffraction (EBSD) evidence. For comparison an EBSD map from a sample formed using a simple ‘back-and-forth’ strategy has also been presented and reveals a dramatically different grain structure and crystallographic orientation. MicroCT evidence, supported by SEM microscopy, shows that in the as-fabricated material the bimodal structure caused by the ‘island’ scan-strategy translates directly into the macroscopic pattern for the regions of extensive weld cracking associated with the SLM fabrication of γ′ hardenable materials. Similar microCT data has shown that HIPping can effectively close the internal cracks to provide a retro-fix solution.