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Quantitative trace analysis of fullerenes in river sediment from Spain and soils from Saudi Arabia
A quantitative method based on ultrasound-assisted toluene extraction followed by liquid chromatography–electrospray ionization–tandem mass spectrometry for the analysis of C 60 and C 70 fullerenes, N -methylfulleropyrrolidine, [6, 6]-phenyl C 61 butyric acid methyl ester and [6, 6]-thienyl C 61 but...
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| Published in: | Analytical and bioanalytical chemistry 2013-07, Vol.405 (18), p.5915-5923 |
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| container_title | Analytical and bioanalytical chemistry |
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| creator | Sanchís, Josep Božović, Dalibor Al-Harbi, Naif A. Silva, Luis F. Farré, Marinella Barceló, Damià |
| description | A quantitative method based on ultrasound-assisted toluene extraction followed by liquid chromatography–electrospray ionization–tandem mass spectrometry for the analysis of C
60
and C
70
fullerenes,
N
-methylfulleropyrrolidine, [6, 6]-phenyl C
61
butyric acid methyl ester and [6, 6]-thienyl C
61
butyric acid methyl ester has been developed. The method was validated using fortified blank river sediments according to the criteria of Commission Decision 2002/657/EC. The method limits of detection ranged from 14 to 290 pg/g, making it suitable for its application in environmental analysis. The method has been applied to investigate fullerene content in 58 soil samples collected from different urban and industrial areas in Saudi Arabia and in river sediment from six different sites in the Llobregat River Basin. In addition, in the case of the Llobregat River, superficial water samples from the same sites of the sediments were collected and analysed using a previous method. In soils from Saudi Arabia, C
60
-fullerene was the only compound that was detected and quantified in 19 % of samples. In the sediments of the Llobregat River, C
60
-fullerene was also the only one detected (33 % of the samples), while in river water, C
70
-fullerene was the most frequent compound, and it was quantified in 67 % of the samples. However, C
60
-fullerene was present in two of the six samples, but at higher concentrations than C
70
-fullerene, ranging from 0.9 to 7.8 ng/L. |
| doi_str_mv | 10.1007/s00216-013-6924-z |
| format | article |
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60
and C
70
fullerenes,
N
-methylfulleropyrrolidine, [6, 6]-phenyl C
61
butyric acid methyl ester and [6, 6]-thienyl C
61
butyric acid methyl ester has been developed. The method was validated using fortified blank river sediments according to the criteria of Commission Decision 2002/657/EC. The method limits of detection ranged from 14 to 290 pg/g, making it suitable for its application in environmental analysis. The method has been applied to investigate fullerene content in 58 soil samples collected from different urban and industrial areas in Saudi Arabia and in river sediment from six different sites in the Llobregat River Basin. In addition, in the case of the Llobregat River, superficial water samples from the same sites of the sediments were collected and analysed using a previous method. In soils from Saudi Arabia, C
60
-fullerene was the only compound that was detected and quantified in 19 % of samples. In the sediments of the Llobregat River, C
60
-fullerene was also the only one detected (33 % of the samples), while in river water, C
70
-fullerene was the most frequent compound, and it was quantified in 67 % of the samples. However, C
60
-fullerene was present in two of the six samples, but at higher concentrations than C
70
-fullerene, ranging from 0.9 to 7.8 ng/L.</description><identifier>ISSN: 1618-2642</identifier><identifier>EISSN: 1618-2650</identifier><identifier>DOI: 10.1007/s00216-013-6924-z</identifier><identifier>PMID: 23545859</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer-Verlag</publisher><subject>Acids ; Analytical Chemistry ; Arabia ; Biochemistry ; Buckminsterfullerene ; Butyric acid ; Characterization and Evaluation of Materials ; Chemical properties ; Chemistry ; Chemistry and Materials Science ; Chemistry, Analytic ; Chromatography ; Composition ; Esters ; Fluvial sediments ; Food Science ; Freshwater ; Fullerenes ; Industrial areas ; Ionization ; Laboratory Medicine ; Liquid chromatography ; Marine sediments ; Mass spectrometry ; Methods ; Monitoring/Environmental Analysis ; Nanomaterials ; Quantitative ; Research Paper ; River basins ; Rivers ; Scientific imaging ; Sediments ; Soil chemistry ; Soils ; Toluene ; Ultrasonic imaging ; Water analysis ; Water sampling</subject><ispartof>Analytical and bioanalytical chemistry, 2013-07, Vol.405 (18), p.5915-5923</ispartof><rights>Springer-Verlag Berlin Heidelberg 2013</rights><rights>COPYRIGHT 2013 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c514t-7ab43ec578258cb18c586ebfa57e233b8801719c26be7131759e68fe7a9594d33</citedby><cites>FETCH-LOGICAL-c514t-7ab43ec578258cb18c586ebfa57e233b8801719c26be7131759e68fe7a9594d33</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,778,782,27911,27912</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/23545859$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Sanchís, Josep</creatorcontrib><creatorcontrib>Božović, Dalibor</creatorcontrib><creatorcontrib>Al-Harbi, Naif A.</creatorcontrib><creatorcontrib>Silva, Luis F.</creatorcontrib><creatorcontrib>Farré, Marinella</creatorcontrib><creatorcontrib>Barceló, Damià</creatorcontrib><title>Quantitative trace analysis of fullerenes in river sediment from Spain and soils from Saudi Arabia</title><title>Analytical and bioanalytical chemistry</title><addtitle>Anal Bioanal Chem</addtitle><addtitle>Anal Bioanal Chem</addtitle><description>A quantitative method based on ultrasound-assisted toluene extraction followed by liquid chromatography–electrospray ionization–tandem mass spectrometry for the analysis of C
60
and C
70
fullerenes,
N
-methylfulleropyrrolidine, [6, 6]-phenyl C
61
butyric acid methyl ester and [6, 6]-thienyl C
61
butyric acid methyl ester has been developed. The method was validated using fortified blank river sediments according to the criteria of Commission Decision 2002/657/EC. The method limits of detection ranged from 14 to 290 pg/g, making it suitable for its application in environmental analysis. The method has been applied to investigate fullerene content in 58 soil samples collected from different urban and industrial areas in Saudi Arabia and in river sediment from six different sites in the Llobregat River Basin. In addition, in the case of the Llobregat River, superficial water samples from the same sites of the sediments were collected and analysed using a previous method. In soils from Saudi Arabia, C
60
-fullerene was the only compound that was detected and quantified in 19 % of samples. In the sediments of the Llobregat River, C
60
-fullerene was also the only one detected (33 % of the samples), while in river water, C
70
-fullerene was the most frequent compound, and it was quantified in 67 % of the samples. However, C
60
-fullerene was present in two of the six samples, but at higher concentrations than C
70
-fullerene, ranging from 0.9 to 7.8 ng/L.</description><subject>Acids</subject><subject>Analytical Chemistry</subject><subject>Arabia</subject><subject>Biochemistry</subject><subject>Buckminsterfullerene</subject><subject>Butyric acid</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical properties</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry, Analytic</subject><subject>Chromatography</subject><subject>Composition</subject><subject>Esters</subject><subject>Fluvial sediments</subject><subject>Food Science</subject><subject>Freshwater</subject><subject>Fullerenes</subject><subject>Industrial areas</subject><subject>Ionization</subject><subject>Laboratory Medicine</subject><subject>Liquid chromatography</subject><subject>Marine sediments</subject><subject>Mass spectrometry</subject><subject>Methods</subject><subject>Monitoring/Environmental Analysis</subject><subject>Nanomaterials</subject><subject>Quantitative</subject><subject>Research Paper</subject><subject>River basins</subject><subject>Rivers</subject><subject>Scientific imaging</subject><subject>Sediments</subject><subject>Soil chemistry</subject><subject>Soils</subject><subject>Toluene</subject><subject>Ultrasonic imaging</subject><subject>Water analysis</subject><subject>Water 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Quality</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) Professional</collection><jtitle>Analytical and bioanalytical chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sanchís, Josep</au><au>Božović, Dalibor</au><au>Al-Harbi, Naif A.</au><au>Silva, Luis F.</au><au>Farré, Marinella</au><au>Barceló, Damià</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Quantitative trace analysis of fullerenes in river sediment from Spain and soils from Saudi Arabia</atitle><jtitle>Analytical and bioanalytical chemistry</jtitle><stitle>Anal Bioanal Chem</stitle><addtitle>Anal Bioanal Chem</addtitle><date>2013-07-01</date><risdate>2013</risdate><volume>405</volume><issue>18</issue><spage>5915</spage><epage>5923</epage><pages>5915-5923</pages><issn>1618-2642</issn><eissn>1618-2650</eissn><abstract>A quantitative method based on ultrasound-assisted toluene extraction followed by liquid chromatography–electrospray ionization–tandem mass spectrometry for the analysis of C
60
and C
70
fullerenes,
N
-methylfulleropyrrolidine, [6, 6]-phenyl C
61
butyric acid methyl ester and [6, 6]-thienyl C
61
butyric acid methyl ester has been developed. The method was validated using fortified blank river sediments according to the criteria of Commission Decision 2002/657/EC. The method limits of detection ranged from 14 to 290 pg/g, making it suitable for its application in environmental analysis. The method has been applied to investigate fullerene content in 58 soil samples collected from different urban and industrial areas in Saudi Arabia and in river sediment from six different sites in the Llobregat River Basin. In addition, in the case of the Llobregat River, superficial water samples from the same sites of the sediments were collected and analysed using a previous method. In soils from Saudi Arabia, C
60
-fullerene was the only compound that was detected and quantified in 19 % of samples. In the sediments of the Llobregat River, C
60
-fullerene was also the only one detected (33 % of the samples), while in river water, C
70
-fullerene was the most frequent compound, and it was quantified in 67 % of the samples. However, C
60
-fullerene was present in two of the six samples, but at higher concentrations than C
70
-fullerene, ranging from 0.9 to 7.8 ng/L.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer-Verlag</pub><pmid>23545859</pmid><doi>10.1007/s00216-013-6924-z</doi><tpages>9</tpages></addata></record> |
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| identifier | ISSN: 1618-2642 |
| ispartof | Analytical and bioanalytical chemistry, 2013-07, Vol.405 (18), p.5915-5923 |
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| language | eng |
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| source | Springer Nature |
| subjects | Acids Analytical Chemistry Arabia Biochemistry Buckminsterfullerene Butyric acid Characterization and Evaluation of Materials Chemical properties Chemistry Chemistry and Materials Science Chemistry, Analytic Chromatography Composition Esters Fluvial sediments Food Science Freshwater Fullerenes Industrial areas Ionization Laboratory Medicine Liquid chromatography Marine sediments Mass spectrometry Methods Monitoring/Environmental Analysis Nanomaterials Quantitative Research Paper River basins Rivers Scientific imaging Sediments Soil chemistry Soils Toluene Ultrasonic imaging Water analysis Water sampling |
| title | Quantitative trace analysis of fullerenes in river sediment from Spain and soils from Saudi Arabia |
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