A convenient synthesis of cyclopropane malonyl peroxide

Cyclopropane-1,1-dicarbonyl peroxide was prepared in 85% yield by the reaction of diethyl cyclopropane-1,1-dicarboxylate with the urea hydrogen peroxide clathrate in the presence of methanesulfonic acid.

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Bibliographic Details
Published in:Mendeleev communications 2014-11, Vol.24 (6), p.345-345
Main Authors: Terent’ev, Alexander O., Vil’, Vera A., Mulina, Olga M., Pivnitsky, Kazimir K., Nikishin, Gennady I.
Format: Article
Language:English
Subjects:
Clathrates
Cyclopropane
Hydrogen peroxide
Peroxides
Synthesis
Ureas
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Description
Summary:Cyclopropane-1,1-dicarbonyl peroxide was prepared in 85% yield by the reaction of diethyl cyclopropane-1,1-dicarboxylate with the urea hydrogen peroxide clathrate in the presence of methanesulfonic acid.
ISSN:0959-9436
DOI:10.1016/j.mencom.2014.11.010