Iodine-catalyzed oxidative system for cyclization of primary alcohols with o-aminobenzamides to quinazolinones using DMSO as the oxidant in dimethyl carbonate

The iodine catalyzed one-pot two-step oxidative system for cyclization of primary alcohols with o-aminobenzamides to quinazolinones using DMSO as the oxidant has been achieved, providing a convenient and efficient method for the synthesis of quinazolinones in good to excellent yields via in situoxid...

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Published in:RSC advances 2013-01, Vol.3 (27), p.10817-10822
Main Authors: Ge, Wenlei, Zhu, Xun, Wei, Yunyang
Format: Article
Language:English
Subjects:
Alcohols
Bulk molding compounds
Carbonates
Dimethyl
Oxidants
Oxidizing agents
Quinazolinones
Solvents
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description The iodine catalyzed one-pot two-step oxidative system for cyclization of primary alcohols with o-aminobenzamides to quinazolinones using DMSO as the oxidant has been achieved, providing a convenient and efficient method for the synthesis of quinazolinones in good to excellent yields via in situoxidation of primary alcohols to aldehydes. The reaction was carried out in the green solvent DMC, under atmospheric conditions. The procedure is suitable for aromatic or alkyl primary alcohols.
doi_str_mv 10.1039/c3ra40872h
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source Royal Society of Chemistry:Jisc Collections:Royal Society of Chemistry Read and Publish 2022-2024 (reading list)
subjects Alcohols
Bulk molding compounds
Carbonates
Dimethyl
Oxidants
Oxidizing agents
Quinazolinones
Solvents
title Iodine-catalyzed oxidative system for cyclization of primary alcohols with o-aminobenzamides to quinazolinones using DMSO as the oxidant in dimethyl carbonate
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