Effect of sample pre-cracking method and notch geometry in plane strain fracture toughness tests as applied to a PMMA resin

• Published in: Polymer testing 2012-09, Vol.31 (6), p.834-840
• Main Authors: de Souza, Joelmir Mariano, Yoshimura, Humberto Naoyuki, Peres, Fabiano Moreno, Schön, Cláudio Geraldo
• Format: Article
• Language: English
• Subjects: Applied sciences; Exact sciences and technology; Fracture toughness; Notches; Photoelasticity; Physicochemistry of polymers; Plane strain; PMMA; Polymer industry, paints, wood; Polymers; Polymethyl methacrylates; Precracking; Pressing; Razor blades; Single-edge notched bending; Tapping; Technology of polymers
• ISSN: 0142-9418; 1873-2348
• DOI: 10.1016/j.polymertesting.2012.06.003

The influence of test method factors (notch shape, square or angular, and pre-cracking method, by tapping onto or pressing a razor blade) on the results obtained in plane strain fracture toughness test according to standard ASTM D5045 using SENB specimens made of a commercial PMMA resin were investigated. Results were analyzed quantitatively by comparing the obtained KIc values and qualitatively by observing their effect on the Moiré fringes observed using photoelasticity, showing that, at 95% significance level, the KIc values are affected by the pre-cracking method, with the most conservative value being obtained when natural pre-cracks were introduced by tapping onto a razor blade (KIc = 1.15 ± 0.11 MPa·m0.5). This correlates with a perturbation in the stress field close to the pre-crack tip observed in the photoelasticity test sample when it was introduced by pressing the razor blade. Surprisingly, notch geometry only slightly affects the results.