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Spectroscopic and X-ray Diffraction Investigations into the Specific Features of Crystallization of Potassium Niobium Silicate Glasses

The Raman spectra and X-ray diffraction patterns of initial and crystallized glasses of the composition 25K^sub 2^O · 27.5Nb^sub 2^O^sub 5^ · 47.5SiO^sub 2^ (mol %) are investigated. It is demonstrated that, upon heat treatment at temperatures in the range 740-900°C, nanocrystals similar in composit...

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Bibliographic Details
Published in:Glass physics and chemistry 2004-07, Vol.30 (4), p.311-320
Main Authors: Alekseeva, I. P., Golubkov, V. V., Dymshits, O. S., Zhilin, A. A., Petrov, V. I., Tsenter, M. Ya
Format: Article
Language:English
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Summary:The Raman spectra and X-ray diffraction patterns of initial and crystallized glasses of the composition 25K^sub 2^O · 27.5Nb^sub 2^O^sub 5^ · 47.5SiO^sub 2^ (mol %) are investigated. It is demonstrated that, upon heat treatment at temperatures in the range 740-900°C, nanocrystals similar in composition to the initial glass precipitate in the glass. The sizes of nanocrystals are estimated with the use of both methods.[PUBLICATION ABSTRACT]
ISSN:1087-6596
1608-313X
DOI:10.1023/B:GPAC.0000038702.00600.11