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Determination of myristicin in commonly spices applying SPE/GC
► The method of myristicin determination in commonly spices is presented. ► The method is characterized by: high yield (100%); low detection limit 1.35ngg−1. ► High precision (RSD below 2.4%) and excellent linearity R2⩾0.9998. The increasing use of myristicin (a component of nutmeg) as a cheap hallu...
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| Published in: | Food and chemical toxicology 2012-07, Vol.50 (7), p.2362-2367 |
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| Main Authors: | , |
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| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c506t-30075043fba91524d76957ee055f9a49b2c914d510346177f9ce184a8ac4a7c53 |
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| cites | cdi_FETCH-LOGICAL-c506t-30075043fba91524d76957ee055f9a49b2c914d510346177f9ce184a8ac4a7c53 |
| container_end_page | 2367 |
| container_issue | 7 |
| container_start_page | 2362 |
| container_title | Food and chemical toxicology |
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| creator | Dawidowicz, Andrzej L. Dybowski, Michal P. |
| description | ► The method of myristicin determination in commonly spices is presented. ► The method is characterized by: high yield (100%); low detection limit 1.35ngg−1. ► High precision (RSD below 2.4%) and excellent linearity R2⩾0.9998.
The increasing use of myristicin (a component of nutmeg) as a cheap hallucinogenic intoxicant requires from the world of science the elaboration of new methods for determination of this compound in daily-use foodstuffs. The present study describes a fast, simple and sensitive method of myristicin analysis in nutmeg and spices containing it using gas chromatography combined with ultrasonic solvent extraction and solid phase extraction processes. The developed method is characterized by high recovery (almost 100%), a low detection limit 1.35ngg−1 and good repeatability (average RDS value equal 2.39%). The presented analytical approach constitutes a substantial improvement on previously reported methods for myristicin analysis and seems to be the method of choice for determining the amount of the compound in spices containing nutmeg. |
| doi_str_mv | 10.1016/j.fct.2012.04.013 |
| format | article |
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The increasing use of myristicin (a component of nutmeg) as a cheap hallucinogenic intoxicant requires from the world of science the elaboration of new methods for determination of this compound in daily-use foodstuffs. The present study describes a fast, simple and sensitive method of myristicin analysis in nutmeg and spices containing it using gas chromatography combined with ultrasonic solvent extraction and solid phase extraction processes. The developed method is characterized by high recovery (almost 100%), a low detection limit 1.35ngg−1 and good repeatability (average RDS value equal 2.39%). The presented analytical approach constitutes a substantial improvement on previously reported methods for myristicin analysis and seems to be the method of choice for determining the amount of the compound in spices containing nutmeg.</description><identifier>ISSN: 0278-6915</identifier><identifier>EISSN: 1873-6351</identifier><identifier>DOI: 10.1016/j.fct.2012.04.013</identifier><identifier>PMID: 22525861</identifier><identifier>CODEN: FCTOD7</identifier><language>eng</language><publisher>Oxford: Elsevier Ltd</publisher><subject>Benzyl Compounds - analysis ; Biological and medical sciences ; detection limit ; Dioxolanes - analysis ; foods ; gas chromatography ; Gas Chromatography-Mass Spectrometry - methods ; General pharmacology ; Limit of Detection ; Medical sciences ; Miristica fragrans ; Myristicin ; nutmeg ; Nutmeg essential oil ; Pharmacognosy. Homeopathy. Health food ; Pharmacology. Drug treatments ; Pyrogallol - analogs & derivatives ; Pyrogallol - analysis ; solid phase extraction ; Solid Phase Extraction - methods ; solvents ; Spices ; Spices - analysis ; Toxicology ; USE/SPE/GC</subject><ispartof>Food and chemical toxicology, 2012-07, Vol.50 (7), p.2362-2367</ispartof><rights>2012 Elsevier Ltd</rights><rights>2015 INIST-CNRS</rights><rights>Copyright © 2012 Elsevier Ltd. All rights reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c506t-30075043fba91524d76957ee055f9a49b2c914d510346177f9ce184a8ac4a7c53</citedby><cites>FETCH-LOGICAL-c506t-30075043fba91524d76957ee055f9a49b2c914d510346177f9ce184a8ac4a7c53</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=26028962$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/22525861$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Dawidowicz, Andrzej L.</creatorcontrib><creatorcontrib>Dybowski, Michal P.</creatorcontrib><title>Determination of myristicin in commonly spices applying SPE/GC</title><title>Food and chemical toxicology</title><addtitle>Food Chem Toxicol</addtitle><description>► The method of myristicin determination in commonly spices is presented. ► The method is characterized by: high yield (100%); low detection limit 1.35ngg−1. ► High precision (RSD below 2.4%) and excellent linearity R2⩾0.9998.
The increasing use of myristicin (a component of nutmeg) as a cheap hallucinogenic intoxicant requires from the world of science the elaboration of new methods for determination of this compound in daily-use foodstuffs. The present study describes a fast, simple and sensitive method of myristicin analysis in nutmeg and spices containing it using gas chromatography combined with ultrasonic solvent extraction and solid phase extraction processes. The developed method is characterized by high recovery (almost 100%), a low detection limit 1.35ngg−1 and good repeatability (average RDS value equal 2.39%). The presented analytical approach constitutes a substantial improvement on previously reported methods for myristicin analysis and seems to be the method of choice for determining the amount of the compound in spices containing nutmeg.</description><subject>Benzyl Compounds - analysis</subject><subject>Biological and medical sciences</subject><subject>detection limit</subject><subject>Dioxolanes - analysis</subject><subject>foods</subject><subject>gas chromatography</subject><subject>Gas Chromatography-Mass Spectrometry - methods</subject><subject>General pharmacology</subject><subject>Limit of Detection</subject><subject>Medical sciences</subject><subject>Miristica fragrans</subject><subject>Myristicin</subject><subject>nutmeg</subject><subject>Nutmeg essential oil</subject><subject>Pharmacognosy. Homeopathy. Health food</subject><subject>Pharmacology. Drug treatments</subject><subject>Pyrogallol - analogs & derivatives</subject><subject>Pyrogallol - analysis</subject><subject>solid phase extraction</subject><subject>Solid Phase Extraction - methods</subject><subject>solvents</subject><subject>Spices</subject><subject>Spices - analysis</subject><subject>Toxicology</subject><subject>USE/SPE/GC</subject><issn>0278-6915</issn><issn>1873-6351</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqFkEtr3DAUhUVoaKZpf0A2rTeBbuzcK-thUwiEaR6FQAtp1kIjS0GDbbmSpzD_Phpmmu4SEGjznXsOHyFnCBUCiot15cxcUUBaAasA6yOywEbWpag5viMLoLIpRYv8hHxIaQ0AEqV4T04o5ZQ3Ahfk8rudbRz8qGcfxiK4YthGn2Zv_FjkZ8IwhLHfFmnyxqZCT1O_9eNT8fDr-uJ2-ZEcO90n--nwn5LHm-vfy7vy_uftj-XVfWk4iLmsczMHVruVzmso66RoubQWOHetZu2KmhZZxxFqJlBK1xqLDdONNkxLw-tT8nV_d4rhz8amWQ0-Gdv3erRhkxQKKXKUC3gbBQockWKbUdyjJoaUonVqin7QcZshtTOs1iobVjvDCpjKhnPm8-H8ZjXY7iXxT2kGzg-ATkb3LurR-PSfE0CbVtDMfdlzTgeln7J09fiQmzgAyjxxV_VtT9hs9q-3USXj7Whs56PNs7rgXxn6DKs0nuU</recordid><startdate>20120701</startdate><enddate>20120701</enddate><creator>Dawidowicz, Andrzej L.</creator><creator>Dybowski, Michal P.</creator><general>Elsevier Ltd</general><general>Elsevier</general><scope>FBQ</scope><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>7T2</scope><scope>7U2</scope><scope>7U7</scope><scope>C1K</scope></search><sort><creationdate>20120701</creationdate><title>Determination of myristicin in commonly spices applying SPE/GC</title><author>Dawidowicz, Andrzej L. ; Dybowski, Michal P.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c506t-30075043fba91524d76957ee055f9a49b2c914d510346177f9ce184a8ac4a7c53</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Benzyl Compounds - analysis</topic><topic>Biological and medical sciences</topic><topic>detection limit</topic><topic>Dioxolanes - analysis</topic><topic>foods</topic><topic>gas chromatography</topic><topic>Gas Chromatography-Mass Spectrometry - methods</topic><topic>General pharmacology</topic><topic>Limit of Detection</topic><topic>Medical sciences</topic><topic>Miristica fragrans</topic><topic>Myristicin</topic><topic>nutmeg</topic><topic>Nutmeg essential oil</topic><topic>Pharmacognosy. Homeopathy. Health food</topic><topic>Pharmacology. Drug treatments</topic><topic>Pyrogallol - analogs & derivatives</topic><topic>Pyrogallol - analysis</topic><topic>solid phase extraction</topic><topic>Solid Phase Extraction - methods</topic><topic>solvents</topic><topic>Spices</topic><topic>Spices - analysis</topic><topic>Toxicology</topic><topic>USE/SPE/GC</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Dawidowicz, Andrzej L.</creatorcontrib><creatorcontrib>Dybowski, Michal P.</creatorcontrib><collection>AGRIS</collection><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Health and Safety Science Abstracts (Full archive)</collection><collection>Safety Science and Risk</collection><collection>Toxicology Abstracts</collection><collection>Environmental Sciences and Pollution Management</collection><jtitle>Food and chemical toxicology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Dawidowicz, Andrzej L.</au><au>Dybowski, Michal P.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of myristicin in commonly spices applying SPE/GC</atitle><jtitle>Food and chemical toxicology</jtitle><addtitle>Food Chem Toxicol</addtitle><date>2012-07-01</date><risdate>2012</risdate><volume>50</volume><issue>7</issue><spage>2362</spage><epage>2367</epage><pages>2362-2367</pages><issn>0278-6915</issn><eissn>1873-6351</eissn><coden>FCTOD7</coden><abstract>► The method of myristicin determination in commonly spices is presented. ► The method is characterized by: high yield (100%); low detection limit 1.35ngg−1. ► High precision (RSD below 2.4%) and excellent linearity R2⩾0.9998.
The increasing use of myristicin (a component of nutmeg) as a cheap hallucinogenic intoxicant requires from the world of science the elaboration of new methods for determination of this compound in daily-use foodstuffs. The present study describes a fast, simple and sensitive method of myristicin analysis in nutmeg and spices containing it using gas chromatography combined with ultrasonic solvent extraction and solid phase extraction processes. The developed method is characterized by high recovery (almost 100%), a low detection limit 1.35ngg−1 and good repeatability (average RDS value equal 2.39%). The presented analytical approach constitutes a substantial improvement on previously reported methods for myristicin analysis and seems to be the method of choice for determining the amount of the compound in spices containing nutmeg.</abstract><cop>Oxford</cop><pub>Elsevier Ltd</pub><pmid>22525861</pmid><doi>10.1016/j.fct.2012.04.013</doi><tpages>6</tpages></addata></record> |
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| subjects | Benzyl Compounds - analysis Biological and medical sciences detection limit Dioxolanes - analysis foods gas chromatography Gas Chromatography-Mass Spectrometry - methods General pharmacology Limit of Detection Medical sciences Miristica fragrans Myristicin nutmeg Nutmeg essential oil Pharmacognosy. Homeopathy. Health food Pharmacology. Drug treatments Pyrogallol - analogs & derivatives Pyrogallol - analysis solid phase extraction Solid Phase Extraction - methods solvents Spices Spices - analysis Toxicology USE/SPE/GC |
| title | Determination of myristicin in commonly spices applying SPE/GC |
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