Air–particle abrasion on zirconia ceramic using different protocols: Effects on biaxial flexural strength after cyclic loading, phase transformation and surface topography

• Published in: Journal of the mechanical behavior of biomedical materials 2013-10, Vol.26, p.155-163
• Main Authors: Souza, Rodrigo O.A., Valandro, Luiz F., Melo, Renata M., Machado, João P.B., Bottino, Marco A., Özcan, Mutlu
• Format: Article
• Language: English
• Subjects: Abrasion; Abrasion resistance; Air; Air-abrasion; Aluminum oxide; Biaxial flexural strength; Ceramics - chemistry; Cyclic loads; Fatigue (materials); Flexural strength; Hot Temperature; Mechanical Phenomena; Modulus of rupture in bending; Phase Transition; Pressure; Silica coating; Silicon dioxide; Surface Properties; Transformations; Y-TZP; Zirconia; Zirconium - chemistry; Zirconium dioxide
• ISSN: 1751-6161; 1878-0180
• DOI: 10.1016/j.jmbbm.2013.04.018

This study evaluated the effect of different air–particle abrasion protocols on the biaxial flexural strength and structural stability of zirconia ceramics. Zirconia ceramic specimens (ISO 6872) (Lava, 3M ESPE) were obtained (N=336). The specimens (N=118, n=20 per group) were randomly assigned to one of the air-abrasion protocols: Gr1: Control (as-sintered); Gr2: 50 µm Al2O3 (2.5 bar); Gr3: 50 µm Al2O3 (3.5 bar); Gr4: 110 µm Al2O3(2.5 bar); Gr5: 110 µm Al2O3 (3.5 bar); Gr6: 30 µm SiO2 (2.5 bar) (CoJet); Gr7: 30 µm SiO2(3.5 bar); Gr8: 110 µm SiO2 (2.5 bar) (Rocatec Plus); and Gr9: 110 µm SiO2 (3.5 bar) (duration: 20 s, distance: 10 mm). While half of the specimens were tested immediately, the other half was subjected to cyclic loading in water (100,000 cycles; 50 N, 4 Hz, 37 °°C) prior to biaxial flexural strength test (ISO 6872). Phase transformation (t→m), relative amount of transformed monoclinic zirconia (FM), transformed zone depth (TZD) and surface roughness were measured. Particle type (p=0.2746), pressure (p=0.5084) and cyclic loading (p=0.1610) did not influence the flexural strength. Except for the air-abraded group with 110 µm Al2O3 at 3.5 bar, all air-abrasion protocols increased the biaxial flexural strength (MPa) (Controlnon-aged: 1030±153, Controlaged: 1138±138; Experimentalnon-aged: 1307±184–1554±124; Experimentalaged: 1308±118–1451±135) in both non-aged and aged conditions, respectively. Surface roughness (Ra) was the highest with 110 µm Al2O3(0.84 µm. FM values ranged from 0% to 27.21%, higher value for the Rocatec Plus (110 µm SiO2) and 110 µm Al2O3 groups at 3.5 bar pressure. TZD ranged between 0 and 1.43 µm, with the highest values for Rocatec Plus and 110 µm Al2O3 groups at 3.5 bar pressure.