Accelerated CarbonCarbon Bond-Forming Reactions in Preparative Electrospray

From analysis towards synthesis: Charged microdroplets act as microreaction vessels, extending the use of electrospray mass spectrometry from chemical analysis to synthesis. Application of this unique reaction conditions allows microscale carbon–carbon bond forming reactions to be performed rapidly...

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Bibliographic Details
Published in:Angewandte Chemie International Edition 2012-11, Vol.51 (47), p.11832-11835
Main Authors: Müller, Thomas, Badu-Tawiah, Abraham, Cooks, R. Graham
Format: Article
Language:English
Subjects:
analytical methods
Bonding
Carbon-carbon composites
Charging
Chemical analysis
CC coupling
electrospray
Forming
Mass spectrometry
microscale synthesis
Synthesis
Vessels
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Description
Summary:From analysis towards synthesis: Charged microdroplets act as microreaction vessels, extending the use of electrospray mass spectrometry from chemical analysis to synthesis. Application of this unique reaction conditions allows microscale carbon–carbon bond forming reactions to be performed rapidly and in high yields (see picture).
ISSN:1433-7851
1521-3773
DOI:10.1002/anie.201206632