Flow dynamics in perforated plate liquid extraction columns

• Published in: Chemical engineering research & design 2012-10, Vol.90 (10), p.1417-1424
• Main Authors: Ettouney, R.S., El-Rifai, M.A.
• Format: Article
• Language: English
• Subjects: Applied sciences; Chemical engineering; Constitutive relationships; Dispersion; Dynamics; Exact sciences and technology; Exact solutions; Extraction; Flow rate; Frequency response; Hydrodynamics; Hydrodynamics of contact apparatus; Liquids; Perforated plate columns; Perforated plates; Transient response; Unsteady state
• ISSN: 0263-8762
• DOI: 10.1016/j.cherd.2012.02.014

► Interacting liquid–liquid flow dynamics in perforated plate contactors are studied. ► Analytical solutions enabled to discern the effect of individual system parameters. ► Typical transient and frequency responses of flows and holdups are generated. ► Interesting oscillatory behaviour and inverse response are uncovered. A linearized unsteady state flow model is developed for two counter-currently flowing liquids in an un-agitated perforated plate liquid–liquid column contactor. The model is based on the simultaneous solution of dynamic conservation equations and linearized hydrodynamic constitutive equations relating pressure drops and dispersed phase holdups to flow rates. Analytical expressions are obtained for the dynamic responses of inter-stage continuous and dispersed phase flow rates, inter-stage holdups, and level of the top interface to changes in the light liquid and heavy liquid inflow rates to the column. The system's dynamic behavior is vividly demonstrated through a set of typical frequency and transient response computations. Owing to the interaction between the dynamics associated with the flow of the two liquids, the frequency responses of the flow rates and holdups of the two phases are characterized by resonance peaks and non-minimum phase behavior.