Local structure studies of some cobalt (II) complexes using extended X-ray absorption fine structure

Extended X-ray Absorption Fine Structure (EXAFS) analysis of Cobalt (II) complex as a ligand of 2 -methyl-3-[(bis-aniline(R) phenyl]-3H-l,5 benzodiazepine for finding local structure using conventional method .The Co(II) complexes were prepared by chemical root method. The EXAFS spectra were recorde...

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Bibliographic Details
Published in:Journal of physics. Conference series 2014-01, Vol.534 (1), p.12036-4
Main Authors: Mishra, Ashutosh, Ninama, Samrath, Trivedi, Apurva
Format: Article
Language:English
Subjects:
Aniline
Benzodiazepines
Bonding
Cobalt
Computer programs
Coordination compounds
Fine structure
Fourier analysis
Fourier transforms
Neighbouring
Physics
Synchrotron radiation
Synchrotrons
X ray absorption
X-rays
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Summary:Extended X-ray Absorption Fine Structure (EXAFS) analysis of Cobalt (II) complex as a ligand of 2 -methyl-3-[(bis-aniline(R) phenyl]-3H-l,5 benzodiazepine for finding local structure using conventional method .The Co(II) complexes were prepared by chemical root method. The EXAFS spectra were recorded at Cobalt K-edge i.e.; 7709 eV using Dispersive EXFAS beam line at 2.5GeV Indus-2 Synchrotron Radiation Source(SRS) at RRCAT, Indore, India. The recorded EXAFS data were analysed using the computer software Athena for determine the nearest neighbouring distances (bond lengths) of these complexes with conventional methods and it compared with Fourier transform(FT) analysis. The Fourier Transform convert EXAFS data signal into r-space or k-space. This is useful for visualizing the major contributions to the EXAFS spectrum.
ISSN:1742-6588
1742-6596
DOI:10.1088/1742-6596/534/1/012036