An efficient method for the preparation of mono α-aryl derivatives of diethyl malonate and ethyl cyanoacetate using ethyl-1-imidazole carbamate (EImC)

An efficient method for the synthesis of mono α-aryl derivatives of diethyl malonate and ethyl cyanoacetate using ethyl-1-imidazole carbamate (EImC) has been described. Using this method many sterically hindered and highly substituted mono α-aryl derivatives of diethyl malonate and ethyl cyanoacetat...

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Bibliographic Details
Published in:Tetrahedron letters 2012-02, Vol.53 (9), p.1060-1062
Main Authors: Behera, Manoranjan, Venkat Ragavan, R., Sambaiah, M., Erugu, Balaiah, Rama Krishna Reddy, J., Mukkanti, K., Yennam, Satyanarayana
Format: Article
Language:English
Subjects:
Derivatives
Ethyl-1-imidazole carbamate
LiHMDS
Mono-α-aryl derivatives of diethyl malonate and ethyl cyanoacetate
Synthesis (chemistry)
Tetrahedrons
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Summary:An efficient method for the synthesis of mono α-aryl derivatives of diethyl malonate and ethyl cyanoacetate using ethyl-1-imidazole carbamate (EImC) has been described. Using this method many sterically hindered and highly substituted mono α-aryl derivatives of diethyl malonate and ethyl cyanoacetate were synthesized in high yield.
ISSN:0040-4039
1873-3581
DOI:10.1016/j.tetlet.2011.12.067